DE3641756C2 - - Google Patents
Info
- Publication number
- DE3641756C2 DE3641756C2 DE3641756A DE3641756A DE3641756C2 DE 3641756 C2 DE3641756 C2 DE 3641756C2 DE 3641756 A DE3641756 A DE 3641756A DE 3641756 A DE3641756 A DE 3641756A DE 3641756 C2 DE3641756 C2 DE 3641756C2
- Authority
- DE
- Germany
- Prior art keywords
- ketoximosilanes
- general formula
- group
- preparation
- ketoxime
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- 238000000034 method Methods 0.000 claims description 10
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 5
- 229910052783 alkali metal Inorganic materials 0.000 claims description 4
- 150000001340 alkali metals Chemical class 0.000 claims description 4
- 229910052747 lanthanoid Inorganic materials 0.000 claims description 3
- 150000002602 lanthanoids Chemical class 0.000 claims description 3
- 125000000217 alkyl group Chemical group 0.000 claims description 2
- 150000004649 carbonic acid derivatives Chemical class 0.000 claims description 2
- 150000004679 hydroxides Chemical class 0.000 claims description 2
- 150000002736 metal compounds Chemical class 0.000 claims 2
- 150000007514 bases Chemical class 0.000 claims 1
- 229910052751 metal Inorganic materials 0.000 claims 1
- 239000002184 metal Substances 0.000 claims 1
- 150000002739 metals Chemical class 0.000 claims 1
- 230000000737 periodic effect Effects 0.000 claims 1
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 description 12
- 238000004821 distillation Methods 0.000 description 5
- 125000003545 alkoxy group Chemical group 0.000 description 4
- 238000009835 boiling Methods 0.000 description 4
- 238000004519 manufacturing process Methods 0.000 description 4
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 description 3
- 238000006243 chemical reaction Methods 0.000 description 3
- 238000000354 decomposition reaction Methods 0.000 description 3
- 125000002496 methyl group Chemical group [H]C([H])([H])* 0.000 description 3
- WHIVNJATOVLWBW-UHFFFAOYSA-N n-butan-2-ylidenehydroxylamine Chemical compound CCC(C)=NO WHIVNJATOVLWBW-UHFFFAOYSA-N 0.000 description 3
- 150000003377 silicon compounds Chemical class 0.000 description 3
- 239000002904 solvent Substances 0.000 description 3
- 239000000126 substance Substances 0.000 description 3
- 239000007983 Tris buffer Substances 0.000 description 2
- 230000002378 acidificating effect Effects 0.000 description 2
- 238000004132 cross linking Methods 0.000 description 2
- 238000004880 explosion Methods 0.000 description 2
- 239000002360 explosive Substances 0.000 description 2
- 239000000047 product Substances 0.000 description 2
- 229910000077 silane Inorganic materials 0.000 description 2
- 229910021578 Iron(III) chloride Inorganic materials 0.000 description 1
- BLRPTPMANUNPDV-UHFFFAOYSA-N Silane Chemical compound [SiH4] BLRPTPMANUNPDV-UHFFFAOYSA-N 0.000 description 1
- 229910001854 alkali hydroxide Inorganic materials 0.000 description 1
- 229910000288 alkali metal carbonate Inorganic materials 0.000 description 1
- 150000008041 alkali metal carbonates Chemical class 0.000 description 1
- BRPQOXSCLDDYGP-UHFFFAOYSA-N calcium oxide Chemical compound [O-2].[Ca+2] BRPQOXSCLDDYGP-UHFFFAOYSA-N 0.000 description 1
- ODINCKMPIJJUCX-UHFFFAOYSA-N calcium oxide Inorganic materials [Ca]=O ODINCKMPIJJUCX-UHFFFAOYSA-N 0.000 description 1
- 239000000292 calcium oxide Substances 0.000 description 1
- 125000004432 carbon atom Chemical group C* 0.000 description 1
- 239000003054 catalyst Substances 0.000 description 1
- 230000003197 catalytic effect Effects 0.000 description 1
- 239000007795 chemical reaction product Substances 0.000 description 1
- 239000012043 crude product Substances 0.000 description 1
- 229920005645 diorganopolysiloxane polymer Polymers 0.000 description 1
- 229920001971 elastomer Polymers 0.000 description 1
- 239000000806 elastomer Substances 0.000 description 1
- 125000001495 ethyl group Chemical group [H]C([H])([H])C([H])([H])* 0.000 description 1
- -1 ethyl methyl Chemical group 0.000 description 1
- 238000011049 filling Methods 0.000 description 1
- 239000011521 glass Substances 0.000 description 1
- RBTARNINKXHZNM-UHFFFAOYSA-K iron trichloride Chemical compound Cl[Fe](Cl)Cl RBTARNINKXHZNM-UHFFFAOYSA-K 0.000 description 1
- 125000001449 isopropyl group Chemical group [H]C([H])([H])C([H])(*)C([H])([H])[H] 0.000 description 1
- BFXIKLCIZHOAAZ-UHFFFAOYSA-N methyltrimethoxysilane Chemical compound CO[Si](C)(OC)OC BFXIKLCIZHOAAZ-UHFFFAOYSA-N 0.000 description 1
- 238000002156 mixing Methods 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- 238000012856 packing Methods 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
- 239000000376 reactant Substances 0.000 description 1
- 238000010992 reflux Methods 0.000 description 1
- 238000000926 separation method Methods 0.000 description 1
- 150000004756 silanes Chemical class 0.000 description 1
- 230000001960 triggered effect Effects 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
- C07F7/00—Compounds containing elements of Groups 4 or 14 of the Periodic Table
- C07F7/02—Silicon compounds
- C07F7/08—Compounds having one or more C—Si linkages
- C07F7/0834—Compounds having one or more O-Si linkage
- C07F7/0892—Compounds with a Si-O-N linkage
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
- C07F7/00—Compounds containing elements of Groups 4 or 14 of the Periodic Table
- C07F7/02—Silicon compounds
- C07F7/08—Compounds having one or more C—Si linkages
- C07F7/18—Compounds having one or more C—Si linkages as well as one or more C—O—Si linkages
- C07F7/1804—Compounds having Si-O-C linkages
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
Priority Applications (4)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE19863641756 DE3641756A1 (de) | 1986-12-06 | 1986-12-06 | Verfahren zur herstellung von ketoximosilanen |
| EP87117188A EP0273189A1 (de) | 1986-12-06 | 1987-11-21 | Verfahren zur Herstellung von Ketoximosilanen |
| JP62304693A JPS63156795A (ja) | 1986-12-06 | 1987-12-03 | ケトキシモシランの製造方法 |
| US07/128,879 US4766231A (en) | 1986-12-06 | 1987-12-04 | Process for the preparation of ketoximosilanes |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE19863641756 DE3641756A1 (de) | 1986-12-06 | 1986-12-06 | Verfahren zur herstellung von ketoximosilanen |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| DE3641756A1 DE3641756A1 (de) | 1988-08-11 |
| DE3641756C2 true DE3641756C2 (enExample) | 1989-03-09 |
Family
ID=6315631
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DE19863641756 Granted DE3641756A1 (de) | 1986-12-06 | 1986-12-06 | Verfahren zur herstellung von ketoximosilanen |
Country Status (4)
| Country | Link |
|---|---|
| US (1) | US4766231A (enExample) |
| EP (1) | EP0273189A1 (enExample) |
| JP (1) | JPS63156795A (enExample) |
| DE (1) | DE3641756A1 (enExample) |
Families Citing this family (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| FR2611719B1 (fr) * | 1987-03-05 | 1989-06-09 | Rhone Poulenc Chimie | Procede de preparation en continu d'oximinosilanes |
| US5359108A (en) * | 1992-09-17 | 1994-10-25 | Alliedsignal Inc. | Di-, tri- and tetrafunctional methyl isobutyl and methyl amyl ketoxime-based silanes |
| US5717052A (en) * | 1992-09-17 | 1998-02-10 | Alliedsignal Inc. | Di-, tri- and tetrafunctional methyl isobutyl and methyl amyl ketoxime-based silanes |
| US5405930A (en) * | 1992-09-17 | 1995-04-11 | Alliedsignal Inc. | Di-, tri- and tetrafunctional methyl isobutyl and methyl amyl ketoxime-based silanes |
| CN102532186B (zh) * | 2012-01-05 | 2015-07-15 | 北京天山新材料技术有限公司 | 一种肟基有机硅化合物的制备方法 |
| CN103833783B (zh) * | 2014-02-26 | 2016-09-14 | 湖北新蓝天新材料股份有限公司 | 二月桂酸二丁基锡催化合成甲氧基肟酮基硅烷的方法 |
| CN105732687B (zh) * | 2016-03-15 | 2018-08-10 | 荆州市江汉精细化工有限公司 | 一种甲基三丁酮肟基硅烷的制备方法 |
| WO2018013900A1 (en) * | 2016-07-15 | 2018-01-18 | Momentive Performance Materials Inc. | Method of stabilizing imino-functional silane |
| CN114591358B (zh) * | 2021-11-26 | 2024-03-08 | 浙江衢州硅宝化工有限公司 | 一种甲基丙烯酰氧丙基三酮肟基硅烷的制备方法 |
Family Cites Families (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| GB975603A (en) * | 1961-02-27 | 1964-11-18 | Dow Corning | Improvements in or relating to organosilicon compounds |
| JPS4939967A (enExample) * | 1972-08-25 | 1974-04-15 | ||
| SU435243A1 (enExample) * | 1972-11-30 | 1974-07-05 | ||
| SU724514A1 (ru) * | 1977-11-21 | 1980-03-30 | Предприятие П/Я Г-4236 | Способ получени силиловых эфиров оксимов |
| US4400527A (en) * | 1981-12-17 | 1983-08-23 | Allied Corporation | Producing oximinosilanes, oximinogermanes and oximinostannanes |
| US4380660A (en) * | 1982-07-01 | 1983-04-19 | Allied Corporation | Producing alkoxysilanes and alkoxy-oximinosilanes |
| US4384131A (en) * | 1982-07-13 | 1983-05-17 | Union Carbide Corporation | Process for the preparation of oximatohydridosilanes and aminoxyhydridosilanes |
| US4705878A (en) * | 1987-02-25 | 1987-11-10 | Dow Corning Corporation | Method for preparing aminohydrocarbyl-substituted ketoximosilanes |
| US4705877A (en) * | 1987-02-25 | 1987-11-10 | Dow Corning Corporation | Novel aminohydrocarbyl-substituted ketoximosilanes |
-
1986
- 1986-12-06 DE DE19863641756 patent/DE3641756A1/de active Granted
-
1987
- 1987-11-21 EP EP87117188A patent/EP0273189A1/de not_active Withdrawn
- 1987-12-03 JP JP62304693A patent/JPS63156795A/ja active Pending
- 1987-12-04 US US07/128,879 patent/US4766231A/en not_active Expired - Lifetime
Also Published As
| Publication number | Publication date |
|---|---|
| US4766231A (en) | 1988-08-23 |
| JPS63156795A (ja) | 1988-06-29 |
| DE3641756A1 (de) | 1988-08-11 |
| EP0273189A1 (de) | 1988-07-06 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| DE2552907A1 (de) | Verfahren zur herstellung von aromatischen carbonaten | |
| DE3641756C2 (enExample) | ||
| DE2521399A1 (de) | Verfahren zur herstellung von aminoalkylsilanen | |
| EP0003317B1 (de) | Verfahren zum Herstellen von Acyloxysilanen und gegebenenfalls Acyloxysiloxanen | |
| DE2828604C2 (de) | Verfahren zur Reduktion von Phosphinoxiden | |
| DE2263819B2 (de) | Verfahren zur Herstellung von a- Alkoxy w-siloxanolen | |
| EP0277642B1 (de) | Verfahren zur Herstellung von Oximosilanen | |
| EP0845469A2 (de) | Verfahren zur Herstellung von Organocarbonoyloxysilanen | |
| CH661928A5 (de) | Verfahren zur herstellung funktionell substituierter silane. | |
| EP0159599A2 (de) | Verfahren zur Herstellung von Alkoxymethylenverbindungen von Essigestern und substituierten Essigestern | |
| DE2101207A1 (de) | Cyclische Stickstoff enthaltende Organosihciumverbindungen | |
| DD298403A5 (de) | Verfahren zur herstellung von ketoximosilanen | |
| EP0130439B1 (de) | Verfahren zur Herstellung von Derivaten der Vinylphosphon-, oder Vinylpyrophosphonsäure | |
| EP0157270A2 (de) | Verfahren zur Herstellung von tetrachlorierten Benzo-1,4-dioxenen | |
| EP0074582B1 (de) | Verfahren zur Herstellung von Dialkylphosphinsäurehalogeniden | |
| DE3903985A1 (de) | Verfahren zur herstellung von ketoximosilanen | |
| EP0182168B1 (de) | Verfahren zur Herstellung von Hydroxymethylen-alkoxyessigsäureestern | |
| EP0329595B1 (de) | Verfahren zur Herstellung von Alkenylphosphinsäurealkylestern | |
| DE3641100C2 (enExample) | ||
| DE3540216C2 (de) | Verfahren zur Herstellung von N-Methylphosphonsäurediestern von Acryl- bzw. Methacrylsäureamiden aus Methylolverbindungen | |
| DE69314813T2 (de) | Verfahren zur Isolierung von N,O-Dialkyl-hydroxycarbamin-Säureestern | |
| DE1235914B (de) | Verfahren zur Herstellung von Hexaalkyldistannanen | |
| DE60005614T2 (de) | Hydrosilylierung von 4-Vinyl-1-Cyclohexen | |
| EP0018540B1 (de) | Ester des Isocamphyl-guajakols, Verfahren zu ihrer Herstellung und ihre Verwendung zur Herstellung von 3-(Iso-camphyl-(5))-cyclohexanol | |
| EP0258805B1 (de) | Verfahren zur Herstellung von 2-Chlorethanphosphonsäuredichlorid |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| OP8 | Request for examination as to paragraph 44 patent law | ||
| D2 | Grant after examination | ||
| 8327 | Change in the person/name/address of the patent owner |
Owner name: HUELS AG, 4370 MARL, DE |
|
| 8364 | No opposition during term of opposition | ||
| 8339 | Ceased/non-payment of the annual fee |