DE3629394A1 - Verfahren und vorrichtung zu chromatographischen und/oder elektrophoretischen untersuchungen der zusammensetzung einer stoffprobe in einem planarsystem mit insbesondere durch ueberdruck gezwungener stroemung eines traegermittels - Google Patents
Verfahren und vorrichtung zu chromatographischen und/oder elektrophoretischen untersuchungen der zusammensetzung einer stoffprobe in einem planarsystem mit insbesondere durch ueberdruck gezwungener stroemung eines traegermittelsInfo
- Publication number
- DE3629394A1 DE3629394A1 DE19863629394 DE3629394A DE3629394A1 DE 3629394 A1 DE3629394 A1 DE 3629394A1 DE 19863629394 DE19863629394 DE 19863629394 DE 3629394 A DE3629394 A DE 3629394A DE 3629394 A1 DE3629394 A1 DE 3629394A1
- Authority
- DE
- Germany
- Prior art keywords
- sorbent layer
- carrier
- sorbent
- sample
- unit
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Withdrawn
Links
- 238000000034 method Methods 0.000 title claims description 50
- 239000000203 mixture Substances 0.000 title claims description 21
- 239000000126 substance Substances 0.000 title claims description 18
- 239000002594 sorbent Substances 0.000 claims description 133
- 238000005259 measurement Methods 0.000 claims description 72
- 239000003480 eluent Substances 0.000 claims description 26
- 239000007788 liquid Substances 0.000 claims description 21
- 238000001514 detection method Methods 0.000 claims description 17
- 239000002904 solvent Substances 0.000 claims description 17
- 230000008569 process Effects 0.000 claims description 15
- 238000011835 investigation Methods 0.000 claims description 12
- 238000001962 electrophoresis Methods 0.000 claims description 11
- 238000003780 insertion Methods 0.000 claims description 11
- 230000037431 insertion Effects 0.000 claims description 11
- 230000005684 electric field Effects 0.000 claims description 9
- 230000014759 maintenance of location Effects 0.000 claims description 9
- 230000003287 optical effect Effects 0.000 claims description 7
- 230000001419 dependent effect Effects 0.000 claims description 5
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N silicon dioxide Inorganic materials O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims description 5
- 238000005370 electroosmosis Methods 0.000 claims description 4
- 239000010453 quartz Substances 0.000 claims description 2
- 238000011161 development Methods 0.000 description 29
- 230000018109 developmental process Effects 0.000 description 29
- 238000010586 diagram Methods 0.000 description 12
- 238000000926 separation method Methods 0.000 description 12
- 238000012360 testing method Methods 0.000 description 10
- 238000004587 chromatography analysis Methods 0.000 description 8
- 238000001035 drying Methods 0.000 description 6
- 230000009471 action Effects 0.000 description 4
- 238000003556 assay Methods 0.000 description 4
- 238000004140 cleaning Methods 0.000 description 4
- 230000035945 sensitivity Effects 0.000 description 4
- 238000004809 thin layer chromatography Methods 0.000 description 4
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 4
- 238000004458 analytical method Methods 0.000 description 3
- 239000004744 fabric Substances 0.000 description 3
- 239000000463 material Substances 0.000 description 3
- 230000007246 mechanism Effects 0.000 description 3
- 230000001105 regulatory effect Effects 0.000 description 3
- 230000033228 biological regulation Effects 0.000 description 2
- 150000001875 compounds Chemical class 0.000 description 2
- 238000001816 cooling Methods 0.000 description 2
- 238000005516 engineering process Methods 0.000 description 2
- 238000011156 evaluation Methods 0.000 description 2
- 239000000835 fiber Substances 0.000 description 2
- 238000010438 heat treatment Methods 0.000 description 2
- TWNQGVIAIRXVLR-UHFFFAOYSA-N oxo(oxoalumanyloxy)alumane Chemical compound O=[Al]O[Al]=O TWNQGVIAIRXVLR-UHFFFAOYSA-N 0.000 description 2
- 238000012545 processing Methods 0.000 description 2
- 230000005855 radiation Effects 0.000 description 2
- 239000000741 silica gel Substances 0.000 description 2
- 229910002027 silica gel Inorganic materials 0.000 description 2
- 238000012546 transfer Methods 0.000 description 2
- 235000003363 Cornus mas Nutrition 0.000 description 1
- 240000006766 Cornus mas Species 0.000 description 1
- 102000004190 Enzymes Human genes 0.000 description 1
- 108090000790 Enzymes Proteins 0.000 description 1
- 239000004952 Polyamide Substances 0.000 description 1
- 229910018540 Si C Inorganic materials 0.000 description 1
- 230000001133 acceleration Effects 0.000 description 1
- 239000000654 additive Substances 0.000 description 1
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 description 1
- 229910052782 aluminium Inorganic materials 0.000 description 1
- 125000000129 anionic group Chemical group 0.000 description 1
- 239000000969 carrier Substances 0.000 description 1
- 125000002091 cationic group Chemical group 0.000 description 1
- 239000001913 cellulose Substances 0.000 description 1
- 229920002678 cellulose Polymers 0.000 description 1
- 238000010276 construction Methods 0.000 description 1
- 238000011109 contamination Methods 0.000 description 1
- 230000003111 delayed effect Effects 0.000 description 1
- 150000002009 diols Chemical class 0.000 description 1
- 238000004090 dissolution Methods 0.000 description 1
- 238000009826 distribution Methods 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 239000012634 fragment Substances 0.000 description 1
- 238000005184 irreversible process Methods 0.000 description 1
- 238000011068 loading method Methods 0.000 description 1
- HCWCAKKEBCNQJP-UHFFFAOYSA-N magnesium orthosilicate Chemical compound [Mg+2].[Mg+2].[O-][Si]([O-])([O-])[O-] HCWCAKKEBCNQJP-UHFFFAOYSA-N 0.000 description 1
- 239000000391 magnesium silicate Substances 0.000 description 1
- 229910052919 magnesium silicate Inorganic materials 0.000 description 1
- 235000019792 magnesium silicate Nutrition 0.000 description 1
- 239000011159 matrix material Substances 0.000 description 1
- 238000013508 migration Methods 0.000 description 1
- 230000005012 migration Effects 0.000 description 1
- 238000002156 mixing Methods 0.000 description 1
- 125000000449 nitro group Chemical group [O-][N+](*)=O 0.000 description 1
- 239000005416 organic matter Substances 0.000 description 1
- 239000004033 plastic Substances 0.000 description 1
- 229920002647 polyamide Polymers 0.000 description 1
- 239000011148 porous material Substances 0.000 description 1
- 238000002360 preparation method Methods 0.000 description 1
- 125000002924 primary amino group Chemical group [H]N([H])* 0.000 description 1
- 102000004196 processed proteins & peptides Human genes 0.000 description 1
- 108090000765 processed proteins & peptides Proteins 0.000 description 1
- 230000009467 reduction Effects 0.000 description 1
- 229920005989 resin Polymers 0.000 description 1
- 239000011347 resin Substances 0.000 description 1
- 238000004904 shortening Methods 0.000 description 1
- 229910010271 silicon carbide Inorganic materials 0.000 description 1
- 238000005245 sintering Methods 0.000 description 1
- 238000005507 spraying Methods 0.000 description 1
- 238000013517 stratification Methods 0.000 description 1
- 229920003002 synthetic resin Polymers 0.000 description 1
- 239000000057 synthetic resin Substances 0.000 description 1
- 239000000454 talc Substances 0.000 description 1
- 229910052623 talc Inorganic materials 0.000 description 1
- 239000010409 thin film Substances 0.000 description 1
Classifications
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N30/00—Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
- G01N30/90—Plate chromatography, e.g. thin layer or paper chromatography
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N27/00—Investigating or analysing materials by the use of electric, electrochemical, or magnetic means
- G01N27/26—Investigating or analysing materials by the use of electric, electrochemical, or magnetic means by investigating electrochemical variables; by using electrolysis or electrophoresis
- G01N27/416—Systems
- G01N27/447—Systems using electrophoresis
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N27/00—Investigating or analysing materials by the use of electric, electrochemical, or magnetic means
- G01N27/26—Investigating or analysing materials by the use of electric, electrochemical, or magnetic means by investigating electrochemical variables; by using electrolysis or electrophoresis
- G01N27/416—Systems
- G01N27/447—Systems using electrophoresis
- G01N27/44704—Details; Accessories
- G01N27/44717—Arrangements for investigating the separated zones, e.g. localising zones
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N30/00—Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
- G01N30/90—Plate chromatography, e.g. thin layer or paper chromatography
- G01N2030/906—Plate chromatography, e.g. thin layer or paper chromatography pressurised fluid phase
Landscapes
- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Chemical & Material Sciences (AREA)
- Molecular Biology (AREA)
- Pathology (AREA)
- Physics & Mathematics (AREA)
- Analytical Chemistry (AREA)
- Biochemistry (AREA)
- General Health & Medical Sciences (AREA)
- General Physics & Mathematics (AREA)
- Immunology (AREA)
- Electrochemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Treatment Of Liquids With Adsorbents In General (AREA)
- Sampling And Sample Adjustment (AREA)
- Analysing Materials By The Use Of Radiation (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| HU325885A HU196509B (en) | 1985-08-29 | 1985-08-29 | Method and apparatus for carrying out forced-flowing expediently overpressurized separating technical testings in planar system |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| DE3629394A1 true DE3629394A1 (de) | 1987-03-05 |
Family
ID=10963357
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DE19863629394 Withdrawn DE3629394A1 (de) | 1985-08-29 | 1986-08-29 | Verfahren und vorrichtung zu chromatographischen und/oder elektrophoretischen untersuchungen der zusammensetzung einer stoffprobe in einem planarsystem mit insbesondere durch ueberdruck gezwungener stroemung eines traegermittels |
Country Status (6)
| Country | Link |
|---|---|
| JP (1) | JPS6291859A (enrdf_load_stackoverflow) |
| CH (1) | CH673779A5 (enrdf_load_stackoverflow) |
| DE (1) | DE3629394A1 (enrdf_load_stackoverflow) |
| FR (1) | FR2586812B1 (enrdf_load_stackoverflow) |
| GB (1) | GB2179564B (enrdf_load_stackoverflow) |
| HU (1) | HU196509B (enrdf_load_stackoverflow) |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE4017805A1 (de) * | 1989-08-22 | 1991-03-07 | Finnigan Mat Gmbh | Verfahren, praeparat und vorrichtung zur bereitstellung eines analytes fuer eine untersuchung |
| DE4017804A1 (de) * | 1989-08-22 | 1991-03-14 | Finnigan Mat Gmbh | Verfahren und vorrichtung zur laserdesorption von analytmolekuelionen, insbesondere von biomolekuelen |
| WO1992003726A1 (en) * | 1990-08-28 | 1992-03-05 | Laboratóriumi Mu^'szergyár Rt. | Method of, arrangement and separation unit for carrying out separation analysis investigations in a planar system with forced flow of a fluid carrier medium, especially by the means of overpressurized layer chromatography |
Families Citing this family (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| GB2191110B (en) * | 1986-06-06 | 1989-12-06 | Plessey Co Plc | Chromatographic separation device |
| DE4407675C1 (de) * | 1994-03-08 | 1995-06-14 | Merck Patent Gmbh | Trennmaterialien für die DC-RAMAN Kopplung |
| JP2012093092A (ja) * | 2009-11-05 | 2012-05-17 | Nagoya Institute Of Technology | 平板型カラム、それを用いた分離システムおよび分離方法 |
| JPWO2018123575A1 (ja) * | 2016-12-26 | 2019-10-31 | パナソニックＩｐマネジメント株式会社 | 薄層クロマトグラフィープレート及びそれを用いた試料の分析方法 |
Family Cites Families (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4139458A (en) * | 1977-10-03 | 1979-02-13 | Shuyen Harrison | Preparative centrifugal chromatography device |
| US4469601A (en) * | 1981-03-17 | 1984-09-04 | Varex Corporation | System and apparatus for multi-dimensional real-time chromatography |
| US4346001A (en) * | 1981-06-12 | 1982-08-24 | Labor Muszeripari Muvek | Linear overpressured thin-layer chromatographic apparatus |
| CH670160A5 (enrdf_load_stackoverflow) * | 1985-04-04 | 1989-05-12 | Mueszeripari Muevek Lab |
-
1985
- 1985-08-29 HU HU325885A patent/HU196509B/hu not_active IP Right Cessation
-
1986
- 1986-08-25 CH CH344786A patent/CH673779A5/de not_active IP Right Cessation
- 1986-08-26 GB GB8620632A patent/GB2179564B/en not_active Expired - Fee Related
- 1986-08-28 FR FR8612165A patent/FR2586812B1/fr not_active Expired - Lifetime
- 1986-08-28 JP JP61200228A patent/JPS6291859A/ja active Pending
- 1986-08-29 DE DE19863629394 patent/DE3629394A1/de not_active Withdrawn
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE4017805A1 (de) * | 1989-08-22 | 1991-03-07 | Finnigan Mat Gmbh | Verfahren, praeparat und vorrichtung zur bereitstellung eines analytes fuer eine untersuchung |
| DE4017804A1 (de) * | 1989-08-22 | 1991-03-14 | Finnigan Mat Gmbh | Verfahren und vorrichtung zur laserdesorption von analytmolekuelionen, insbesondere von biomolekuelen |
| DE4017805C2 (de) * | 1989-08-22 | 1998-03-26 | Finnigan Mat Gmbh | Verfahren, Präparat und Vorrichtung zur Bereitstellung eines Analytes für eine Untersuchung |
| WO1992003726A1 (en) * | 1990-08-28 | 1992-03-05 | Laboratóriumi Mu^'szergyár Rt. | Method of, arrangement and separation unit for carrying out separation analysis investigations in a planar system with forced flow of a fluid carrier medium, especially by the means of overpressurized layer chromatography |
Also Published As
| Publication number | Publication date |
|---|---|
| GB8620632D0 (en) | 1986-10-01 |
| FR2586812A1 (fr) | 1987-03-06 |
| FR2586812B1 (fr) | 1990-07-20 |
| GB2179564B (en) | 1990-04-25 |
| JPS6291859A (ja) | 1987-04-27 |
| CH673779A5 (enrdf_load_stackoverflow) | 1990-04-12 |
| HUT43964A (en) | 1988-01-28 |
| GB2179564A (en) | 1987-03-11 |
| HU196509B (en) | 1988-11-28 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| 8141 | Disposal/no request for examination |