DE3137765A1 - Verfahren und vorrichtung zur schnellen detektion, identifikation und quantifikation von spurenelementen in gasen, fluessigkeiten und festkoerpern - Google Patents

Verfahren und vorrichtung zur schnellen detektion, identifikation und quantifikation von spurenelementen in gasen, fluessigkeiten und festkoerpern

Info

Publication number
DE3137765A1
DE3137765A1 DE19813137765 DE3137765A DE3137765A1 DE 3137765 A1 DE3137765 A1 DE 3137765A1 DE 19813137765 DE19813137765 DE 19813137765 DE 3137765 A DE3137765 A DE 3137765A DE 3137765 A1 DE3137765 A1 DE 3137765A1
Authority
DE
Germany
Prior art keywords
contact membrane
collecting surface
membrane
contact
carrier gas
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
DE19813137765
Other languages
German (de)
English (en)
Other versions
DE3137765C2 (OSRAM
Inventor
Bernhard Dipl.-Chem. 3042 Munster Odernheimer
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Bruker Daltonics GmbH and Co KG
Original Assignee
Bundesministerium der Verteidigung
Federal Government of Germany
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Bundesministerium der Verteidigung, Federal Government of Germany filed Critical Bundesministerium der Verteidigung
Priority to DE19813137765 priority Critical patent/DE3137765A1/de
Priority to PCT/DE1982/000189 priority patent/WO1983001110A1/de
Priority to JP57502855A priority patent/JPS58501595A/ja
Priority to US06/504,688 priority patent/US4541268A/en
Priority to EP82902900A priority patent/EP0089356B1/de
Publication of DE3137765A1 publication Critical patent/DE3137765A1/de
Application granted granted Critical
Publication of DE3137765C2 publication Critical patent/DE3137765C2/de
Granted legal-status Critical Current

Links

Classifications

    • G—PHYSICS
    • G01—MEASURING; TESTING
    • G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N30/00—Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
    • G—PHYSICS
    • G01—MEASURING; TESTING
    • G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N1/00—Sampling; Preparing specimens for investigation
    • G01N1/02—Devices for withdrawing samples
    • G01N1/10—Devices for withdrawing samples in the liquid or fluent state
    • G—PHYSICS
    • G01—MEASURING; TESTING
    • G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N1/00—Sampling; Preparing specimens for investigation
    • G01N1/02—Devices for withdrawing samples
    • G01N1/22—Devices for withdrawing samples in the gaseous state
    • G01N1/2202—Devices for withdrawing samples in the gaseous state involving separation of sample components during sampling
    • G01N1/2214—Devices for withdrawing samples in the gaseous state involving separation of sample components during sampling by sorption
    • G—PHYSICS
    • G01—MEASURING; TESTING
    • G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N1/00—Sampling; Preparing specimens for investigation
    • G01N1/28—Preparing specimens for investigation including physical details of (bio-)chemical methods covered elsewhere, e.g. G01N33/50, C12Q
    • G01N1/40—Concentrating samples
    • G01N1/405—Concentrating samples by adsorption or absorption
    • G—PHYSICS
    • G01—MEASURING; TESTING
    • G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N1/00—Sampling; Preparing specimens for investigation
    • G01N1/02—Devices for withdrawing samples
    • G01N1/10—Devices for withdrawing samples in the liquid or fluent state
    • G01N1/14—Suction devices, e.g. pumps; Ejector devices
    • G01N2001/1472—Devices not actuated by pressure difference
    • G01N2001/149—Capillaries; Sponges
    • G—PHYSICS
    • G01—MEASURING; TESTING
    • G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N1/00—Sampling; Preparing specimens for investigation
    • G01N1/28—Preparing specimens for investigation including physical details of (bio-)chemical methods covered elsewhere, e.g. G01N33/50, C12Q
    • G01N1/2813—Producing thin layers of samples on a substrate, e.g. smearing, spinning-on
    • G01N2001/2826—Collecting by adsorption or absorption
    • G—PHYSICS
    • G01—MEASURING; TESTING
    • G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N1/00—Sampling; Preparing specimens for investigation
    • G01N1/28—Preparing specimens for investigation including physical details of (bio-)chemical methods covered elsewhere, e.g. G01N33/50, C12Q
    • G01N1/38—Diluting, dispersing or mixing samples
    • G01N2001/383—Diluting, dispersing or mixing samples collecting and diluting in a flow of liquid

Landscapes

  • Life Sciences & Earth Sciences (AREA)
  • Health & Medical Sciences (AREA)
  • General Physics & Mathematics (AREA)
  • Immunology (AREA)
  • Chemical & Material Sciences (AREA)
  • Analytical Chemistry (AREA)
  • Biochemistry (AREA)
  • General Health & Medical Sciences (AREA)
  • Pathology (AREA)
  • Physics & Mathematics (AREA)
  • Hydrology & Water Resources (AREA)
  • Engineering & Computer Science (AREA)
  • Biomedical Technology (AREA)
  • Molecular Biology (AREA)
  • Sampling And Sample Adjustment (AREA)
  • Other Investigation Or Analysis Of Materials By Electrical Means (AREA)
  • Treatment Of Liquids With Adsorbents In General (AREA)
DE19813137765 1981-09-23 1981-09-23 Verfahren und vorrichtung zur schnellen detektion, identifikation und quantifikation von spurenelementen in gasen, fluessigkeiten und festkoerpern Granted DE3137765A1 (de)

Priority Applications (5)

Application Number Priority Date Filing Date Title
DE19813137765 DE3137765A1 (de) 1981-09-23 1981-09-23 Verfahren und vorrichtung zur schnellen detektion, identifikation und quantifikation von spurenelementen in gasen, fluessigkeiten und festkoerpern
PCT/DE1982/000189 WO1983001110A1 (fr) 1981-09-23 1982-09-22 Procede et dispositif pour le prelevement des elements de trace dans les gaz, liquides, solides ou dans les couches superficielles
JP57502855A JPS58501595A (ja) 1981-09-23 1982-09-22 気体、液体、固体または表面層中の痕跡成分のサンプリング法および装置
US06/504,688 US4541268A (en) 1981-09-23 1982-09-22 Method and device for the sampling of trace elements in gases, liquids, solids or in surface layers
EP82902900A EP0089356B1 (de) 1981-09-23 1982-09-22 Verfahren und vorrichtung zur probenahme von spurenkomponenten in gasen, flüssigkeiten an festkörpern oder in oberflächenschichten

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
DE19813137765 DE3137765A1 (de) 1981-09-23 1981-09-23 Verfahren und vorrichtung zur schnellen detektion, identifikation und quantifikation von spurenelementen in gasen, fluessigkeiten und festkoerpern

Publications (2)

Publication Number Publication Date
DE3137765A1 true DE3137765A1 (de) 1983-03-31
DE3137765C2 DE3137765C2 (OSRAM) 1989-04-27

Family

ID=6142365

Family Applications (1)

Application Number Title Priority Date Filing Date
DE19813137765 Granted DE3137765A1 (de) 1981-09-23 1981-09-23 Verfahren und vorrichtung zur schnellen detektion, identifikation und quantifikation von spurenelementen in gasen, fluessigkeiten und festkoerpern

Country Status (5)

Country Link
US (1) US4541268A (OSRAM)
EP (1) EP0089356B1 (OSRAM)
JP (1) JPS58501595A (OSRAM)
DE (1) DE3137765A1 (OSRAM)
WO (1) WO1983001110A1 (OSRAM)

Cited By (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP0145449A3 (en) * 1983-12-07 1987-05-20 Roger C. Eyler The detection of chemical agent droplets
DE3835207C1 (OSRAM) * 1988-10-15 1989-08-03 Bruker - Franzen Analytik Gmbh, 2800 Bremen, De
DE3818210C1 (OSRAM) * 1988-05-28 1989-11-23 Bundesrepublik Deutschland, Vertreten Durch Den Bundesminister Der Verteidigung, Dieser Vertreten Durch Den Praesidenten Des Bundesamtes Fuer Wehrtechnik Und Beschaffung, 5400 Koblenz, De
EP0501955A4 (en) * 1987-07-08 1993-06-30 Thermedics, Inc. Selective detection of vapors
DE19617964A1 (de) * 1996-05-06 1997-11-13 Trace Analysensysteme Gmbh Verfahren zum Nachweis und zur quantitativen Bestimmung gasförmiger oder in Lösung befindlicher Substanzen durch Fließdiffusionsanalyse (FDA) und Meßvorrichtung, insbesondere zur Durchführung dieses Verfahrens
US6183418B1 (en) 1996-05-06 2001-02-06 Trace Analysensysteme Gmbh Process and measuring system for detection of substances emitted or perspired through the skin
DE20303747U1 (de) * 2003-03-10 2003-07-03 Sensobi Sensoren GmbH, 06120 Halle Probenehmer und Anordnung zur Probenahme für Analysen zur Bestimmung von Kontaminationen
DE10302220A1 (de) * 2003-01-20 2004-08-05 Biotechnologie Kempe Gmbh Sonde zur Messung von Ethanol in einer wässrigen Lösung
US7488449B2 (en) 2003-01-20 2009-02-10 Biotechnologie Kempe (Gmbh) Probe device for measuring ethanol concentrations in an aqueous solution

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US4759210A (en) * 1986-06-06 1988-07-26 Microsensor Systems, Inc. Apparatus for gas-monitoring and method of conducting same
KR900005223B1 (ko) * 1986-12-11 1990-07-21 가부시끼가이샤 호리바 세이사꾸쇼 이온농도등의 측정방법과 그 측정에 사용하는 계측기의 교정용시이트 및 교정방법
US5205178A (en) * 1988-05-28 1993-04-27 Bruker-Franzen Analytik Gmbh Method for non-intrusive continuous and automatic taking of samples, storing and supplying of samples and data for a possible evaluation
EP0360901A1 (de) * 1988-09-29 1990-04-04 Leybold Aktiengesellschaft Verfahren und Vorrichtung zur Probennahme und Analyse von Kohlenwasserstoffen
FR2637685B1 (fr) * 1988-10-06 1991-01-04 Berger Produits Dispositif pour l'injection d'un echantillon gazeux dans une colonne de chromatographie en phase gazeuse
FR2648227B1 (fr) * 1989-06-09 1994-01-21 Etat Francais Delegue Armement Appareillage portatif et autonome pour l'analyse in situ d'une substance liquide ou solide se presentant sous la forme de depots superficiels
GB2242141A (en) * 1990-03-24 1991-09-25 Ion Track Instr Method and apparatus for detecting low volatility atmospheric vapors
GB9008630D0 (en) * 1990-04-17 1990-06-13 Graseby Ionics Ltd Vapouriser
EP0458622A3 (en) * 1990-05-22 1992-01-22 Barringer Technologies Inc. Method and apparatus for collection and analysis of desquamated skin particulates or other tissue
CA2060729A1 (en) * 1991-03-20 1992-09-21 Stephen E. O'brien Detection method for checking surfaces for specific compounds
EP0734516A4 (en) * 1993-11-19 1997-11-19 Commw Scient Ind Res Org DIFFUSION CELL
EP0665054A1 (de) * 1994-01-27 1995-08-02 SECURETEC GmbH Adsorbermaterial zur Anreicherung und Gewinnung von Spurenstoffen aus der Gasphase
DE4443755A1 (de) * 1994-01-27 1995-08-03 Boehringer Mannheim Gmbh Adsorbermaterial, Vorrichtung und Verfahren zur Anreicherung und Gewinnung von Spurenstoffen aus der Gasphase
AUPM707494A0 (en) * 1994-07-26 1994-08-18 Crc For Waste Management And Pollution Control Limited A method and apparatus for environmental monitoring of low concentration levels of organic compounds
DE19710525C2 (de) * 1997-03-14 1999-11-11 Cammann Karl Passiv-Diffusionssammler für in Gasen enthaltene Analyte sowie Verfahren zur passiven Probenahme und Analyse
US6186012B1 (en) 1997-12-30 2001-02-13 Battelle Memorial Institute Hand held sample tube manipulator, system and method
EP1136808A1 (en) * 2000-03-20 2001-09-26 Carlo Squicciarini A system for automatically extracting and analysing residual solvents in material samples
AU2003206583A1 (en) * 2002-02-26 2003-09-09 Biosensor Applications Sweden Ab (Publ) Thermostable coated filter disk.
DE112004000253T5 (de) * 2003-02-10 2006-02-02 Waters Investments Ltd., New Castle Adsorption, Detektion und Identifikation von Komponenten der Umgebungsluft mit Desorption/Ionisation auf Silizium und Massenspektrometrie (DIOS-MS)
JP3673789B2 (ja) * 2003-03-31 2005-07-20 株式会社日立製作所 気化ガス検出方法および気化ガス検出装置
US8123834B2 (en) 2005-10-06 2012-02-28 The Board Of Trustees Of The University Of Illinois High gain selective metal organic framework preconcentrators
GB0606346D0 (en) * 2006-03-30 2006-05-10 Smiths Group Plc Preconcentrator and detector apparatus
US7880026B2 (en) * 2006-04-14 2011-02-01 The Board Of Trustees Of The University Of Illinois MOF synthesis method
US8152908B2 (en) 2008-01-16 2012-04-10 The Board Of Trustees Of The University Of Illinois Micromachined gas chromatography columns for fast separation of Organophosphonate and Organosulfur compounds and methods for deactivating same
US8269029B2 (en) 2008-04-08 2012-09-18 The Board Of Trustees Of The University Of Illinois Water repellent metal-organic frameworks, process for making and uses regarding same
ITRM20090581A1 (it) * 2009-11-11 2011-05-12 Istituto Naz Per La Ricerca S Ul Cancro Dispositivo di rilevazione di sostanze volatili, apparato utilizzante tale dispositivo e relativo metodo di funzionamento.
US8402842B2 (en) * 2009-12-30 2013-03-26 Morpho Detection, Inc Surface sampling mobile chemical detection probe
BR112013015141B1 (pt) 2010-12-17 2021-06-29 Biomerieux, Inc. Dispositivo de transferência de amostra e filtração integrado, montagem de transferência de amostra e filtração, e método de isolamento e identificação de um microorganismo de uma amostra de teste
US9150756B2 (en) 2011-08-10 2015-10-06 Hamilton Space Systems International, Inc. Sampling device for substance detection instrument
FR3065807A1 (fr) * 2017-04-26 2018-11-02 Tamas Gabor Palfy Procede d'echantillonage consistant en une separation des solides et a la congelation pour une longue stabilite les echantillons
CN112122140A (zh) * 2019-07-22 2020-12-25 浙江啄云智能科技有限公司 一种用于快递包裹爆炸物及剧毒物的安检方法及系统

Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE2022958A1 (de) * 1969-06-16 1970-12-23 Varian Associates Verfahren und Vorrichtung zum Detektieren von Stoffen in einer Fluessigkeit
DE2139992A1 (de) * 1971-08-10 1973-02-22 Bodenseewerk Perkin Elmer Co Verfahren und vorrichtung zur probenahme und zum aufgeben einer probe in ein analysengeraet

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FR1573147A (OSRAM) * 1967-05-31 1969-07-04
US3638401A (en) * 1969-03-24 1972-02-01 Varian Associates Vacuum connector for connecting replaceable evacuated devices to an evacuated system
GB1309549A (en) * 1969-06-13 1973-03-14 Atomic Energy Authority Uk Carbon content analysis
US3929003A (en) * 1969-06-16 1975-12-30 Varian Associates Method and apparatus for detecing materials in a liquid
US3950980A (en) * 1974-03-27 1976-04-20 Minnesota Mining And Manufacturing Company Vapor sampling device
GB1454602A (en) * 1974-05-02 1976-11-03 Jenkins A Apparatus for checking the contents of closed containers
US3985017A (en) * 1975-01-02 1976-10-12 Abcor, Inc. Gaseous contaminate dosimeter and method
JPS5194294A (OSRAM) * 1975-02-17 1976-08-18
DE3009069C2 (de) * 1980-03-10 1982-10-21 Bundesrepublik Deutschland, Vertreten Durch Den Bundesminister Der Verteidigung, 5300 Bonn Eingangs-Kopf eines Meß/Nachweissystems für chemische Agentien

Patent Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE2022958A1 (de) * 1969-06-16 1970-12-23 Varian Associates Verfahren und Vorrichtung zum Detektieren von Stoffen in einer Fluessigkeit
DE2139992A1 (de) * 1971-08-10 1973-02-22 Bodenseewerk Perkin Elmer Co Verfahren und vorrichtung zur probenahme und zum aufgeben einer probe in ein analysengeraet

Cited By (11)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP0145449A3 (en) * 1983-12-07 1987-05-20 Roger C. Eyler The detection of chemical agent droplets
EP0501955A4 (en) * 1987-07-08 1993-06-30 Thermedics, Inc. Selective detection of vapors
DE3818210C1 (OSRAM) * 1988-05-28 1989-11-23 Bundesrepublik Deutschland, Vertreten Durch Den Bundesminister Der Verteidigung, Dieser Vertreten Durch Den Praesidenten Des Bundesamtes Fuer Wehrtechnik Und Beschaffung, 5400 Koblenz, De
DE3835207C1 (OSRAM) * 1988-10-15 1989-08-03 Bruker - Franzen Analytik Gmbh, 2800 Bremen, De
EP0364687A3 (en) * 1988-10-15 1990-11-28 Bruker-Franzen Analytik Gmbh Sampling device for survey vehicles
DE19617964A1 (de) * 1996-05-06 1997-11-13 Trace Analysensysteme Gmbh Verfahren zum Nachweis und zur quantitativen Bestimmung gasförmiger oder in Lösung befindlicher Substanzen durch Fließdiffusionsanalyse (FDA) und Meßvorrichtung, insbesondere zur Durchführung dieses Verfahrens
DE19617964C2 (de) * 1996-05-06 1998-07-09 Trace Analysensysteme Gmbh Verfahren und Meßvorrichtung zum Nachweis von durch die Haut abgegebenen oder ausgedunsteten Substanzen und zugehörige Meßvorrichtung
US6183418B1 (en) 1996-05-06 2001-02-06 Trace Analysensysteme Gmbh Process and measuring system for detection of substances emitted or perspired through the skin
DE10302220A1 (de) * 2003-01-20 2004-08-05 Biotechnologie Kempe Gmbh Sonde zur Messung von Ethanol in einer wässrigen Lösung
US7488449B2 (en) 2003-01-20 2009-02-10 Biotechnologie Kempe (Gmbh) Probe device for measuring ethanol concentrations in an aqueous solution
DE20303747U1 (de) * 2003-03-10 2003-07-03 Sensobi Sensoren GmbH, 06120 Halle Probenehmer und Anordnung zur Probenahme für Analysen zur Bestimmung von Kontaminationen

Also Published As

Publication number Publication date
US4541268A (en) 1985-09-17
EP0089356B1 (de) 1986-08-27
WO1983001110A1 (fr) 1983-03-31
JPS58501595A (ja) 1983-09-22
EP0089356A1 (de) 1983-09-28
DE3137765C2 (OSRAM) 1989-04-27

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Legal Events

Date Code Title Description
8110 Request for examination paragraph 44
8127 New person/name/address of the applicant

Owner name: BRUKER - FRANZEN ANALYTIK GMBH, 2800 BREMEN, DE

D2 Grant after examination
8364 No opposition during term of opposition
8327 Change in the person/name/address of the patent owner

Owner name: BRUKER DALTONIK GMBH, 28359 BREMEN, DE

8339 Ceased/non-payment of the annual fee