DE3104737A1 - Verfahren zur herstellung von zinn-(iv)-chlorid - Google Patents
Verfahren zur herstellung von zinn-(iv)-chloridInfo
- Publication number
- DE3104737A1 DE3104737A1 DE19813104737 DE3104737A DE3104737A1 DE 3104737 A1 DE3104737 A1 DE 3104737A1 DE 19813104737 DE19813104737 DE 19813104737 DE 3104737 A DE3104737 A DE 3104737A DE 3104737 A1 DE3104737 A1 DE 3104737A1
- Authority
- DE
- Germany
- Prior art keywords
- tin
- chloride
- chlorine
- reaction
- space
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Withdrawn
Links
- 229910021627 Tin(IV) chloride Inorganic materials 0.000 title claims description 163
- HPGGPRDJHPYFRM-UHFFFAOYSA-J tin(iv) chloride Chemical compound Cl[Sn](Cl)(Cl)Cl HPGGPRDJHPYFRM-UHFFFAOYSA-J 0.000 title claims description 162
- 238000004519 manufacturing process Methods 0.000 title claims description 6
- ZAMOUSCENKQFHK-UHFFFAOYSA-N Chlorine atom Chemical compound [Cl] ZAMOUSCENKQFHK-UHFFFAOYSA-N 0.000 claims description 136
- 229910052801 chlorine Inorganic materials 0.000 claims description 136
- 239000000460 chlorine Substances 0.000 claims description 136
- 238000006243 chemical reaction Methods 0.000 claims description 131
- ATJFFYVFTNAWJD-UHFFFAOYSA-N Tin Chemical compound [Sn] ATJFFYVFTNAWJD-UHFFFAOYSA-N 0.000 claims description 110
- 239000007788 liquid Substances 0.000 claims description 57
- 239000007789 gas Substances 0.000 claims description 44
- 238000000034 method Methods 0.000 claims description 39
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 claims description 16
- 238000001816 cooling Methods 0.000 claims description 15
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 claims description 12
- 229910052757 nitrogen Inorganic materials 0.000 claims description 8
- 239000007787 solid Substances 0.000 claims description 4
- 239000003795 chemical substances by application Substances 0.000 claims 1
- 239000011521 glass Substances 0.000 description 61
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 10
- 238000002474 experimental method Methods 0.000 description 9
- 239000000047 product Substances 0.000 description 8
- 238000003860 storage Methods 0.000 description 7
- 238000005406 washing Methods 0.000 description 7
- KZBUYRJDOAKODT-UHFFFAOYSA-N Chlorine Chemical compound ClCl KZBUYRJDOAKODT-UHFFFAOYSA-N 0.000 description 6
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 6
- 239000013078 crystal Substances 0.000 description 5
- 238000002844 melting Methods 0.000 description 5
- 230000008018 melting Effects 0.000 description 5
- 230000015572 biosynthetic process Effects 0.000 description 4
- 238000009833 condensation Methods 0.000 description 4
- 230000005494 condensation Effects 0.000 description 4
- 238000011049 filling Methods 0.000 description 4
- VEXZGXHMUGYJMC-UHFFFAOYSA-M Chloride anion Chemical compound [Cl-] VEXZGXHMUGYJMC-UHFFFAOYSA-M 0.000 description 3
- 239000003463 adsorbent Substances 0.000 description 3
- VMPVEPPRYRXYNP-UHFFFAOYSA-I antimony(5+);pentachloride Chemical compound Cl[Sb](Cl)(Cl)(Cl)Cl VMPVEPPRYRXYNP-UHFFFAOYSA-I 0.000 description 3
- 238000009835 boiling Methods 0.000 description 3
- 230000000694 effects Effects 0.000 description 3
- 238000001914 filtration Methods 0.000 description 3
- 239000008187 granular material Substances 0.000 description 3
- 239000000463 material Substances 0.000 description 3
- 239000000203 mixture Substances 0.000 description 3
- CURLTUGMZLYLDI-UHFFFAOYSA-N Carbon dioxide Chemical compound O=C=O CURLTUGMZLYLDI-UHFFFAOYSA-N 0.000 description 2
- 229910021626 Tin(II) chloride Inorganic materials 0.000 description 2
- 230000009286 beneficial effect Effects 0.000 description 2
- 238000005260 corrosion Methods 0.000 description 2
- 230000007797 corrosion Effects 0.000 description 2
- 239000000155 melt Substances 0.000 description 2
- 229910052751 metal Inorganic materials 0.000 description 2
- 239000002184 metal Substances 0.000 description 2
- 239000002245 particle Substances 0.000 description 2
- 230000001105 regulatory effect Effects 0.000 description 2
- 238000005245 sintering Methods 0.000 description 2
- 235000011150 stannous chloride Nutrition 0.000 description 2
- TXUICONDJPYNPY-UHFFFAOYSA-N (1,10,13-trimethyl-3-oxo-4,5,6,7,8,9,11,12,14,15,16,17-dodecahydrocyclopenta[a]phenanthren-17-yl) heptanoate Chemical compound C1CC2CC(=O)C=C(C)C2(C)C2C1C1CCC(OC(=O)CCCCCC)C1(C)CC2 TXUICONDJPYNPY-UHFFFAOYSA-N 0.000 description 1
- WKBOTKDWSSQWDR-UHFFFAOYSA-N Bromine atom Chemical compound [Br] WKBOTKDWSSQWDR-UHFFFAOYSA-N 0.000 description 1
- 239000002250 absorbent Substances 0.000 description 1
- 230000002745 absorbent Effects 0.000 description 1
- 239000003513 alkali Substances 0.000 description 1
- 229910052787 antimony Inorganic materials 0.000 description 1
- WATWJIUSRGPENY-UHFFFAOYSA-N antimony atom Chemical compound [Sb] WATWJIUSRGPENY-UHFFFAOYSA-N 0.000 description 1
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 1
- CMLMFNACXHHYRY-UHFFFAOYSA-N azanylidynetin Chemical compound [N].[Sn] CMLMFNACXHHYRY-UHFFFAOYSA-N 0.000 description 1
- 239000002585 base Substances 0.000 description 1
- GDTBXPJZTBHREO-UHFFFAOYSA-N bromine Substances BrBr GDTBXPJZTBHREO-UHFFFAOYSA-N 0.000 description 1
- 229910052794 bromium Inorganic materials 0.000 description 1
- 229910052799 carbon Inorganic materials 0.000 description 1
- 239000001569 carbon dioxide Substances 0.000 description 1
- 229910002092 carbon dioxide Inorganic materials 0.000 description 1
- 239000003054 catalyst Substances 0.000 description 1
- 239000007795 chemical reaction product Substances 0.000 description 1
- 238000005660 chlorination reaction Methods 0.000 description 1
- 238000004140 cleaning Methods 0.000 description 1
- 238000004891 communication Methods 0.000 description 1
- 230000000052 comparative effect Effects 0.000 description 1
- 238000010276 construction Methods 0.000 description 1
- 238000011109 contamination Methods 0.000 description 1
- 239000002826 coolant Substances 0.000 description 1
- 238000000354 decomposition reaction Methods 0.000 description 1
- 238000009826 distribution Methods 0.000 description 1
- 230000003670 easy-to-clean Effects 0.000 description 1
- 239000004744 fabric Substances 0.000 description 1
- 239000012530 fluid Substances 0.000 description 1
- 238000005194 fractionation Methods 0.000 description 1
- 229910052736 halogen Inorganic materials 0.000 description 1
- 150000002367 halogens Chemical class 0.000 description 1
- 238000010438 heat treatment Methods 0.000 description 1
- 239000011261 inert gas Substances 0.000 description 1
- 229910052754 neon Inorganic materials 0.000 description 1
- GKAOGPIIYCISHV-UHFFFAOYSA-N neon atom Chemical compound [Ne] GKAOGPIIYCISHV-UHFFFAOYSA-N 0.000 description 1
- 239000001301 oxygen Substances 0.000 description 1
- 229910052760 oxygen Inorganic materials 0.000 description 1
- 238000003825 pressing Methods 0.000 description 1
- 238000005086 pumping Methods 0.000 description 1
- 238000000746 purification Methods 0.000 description 1
- 239000011541 reaction mixture Substances 0.000 description 1
- 238000010992 reflux Methods 0.000 description 1
- 238000005201 scrubbing Methods 0.000 description 1
- 238000005507 spraying Methods 0.000 description 1
- 239000001119 stannous chloride Substances 0.000 description 1
- 229910052718 tin Inorganic materials 0.000 description 1
- IUTCEZPPWBHGIX-UHFFFAOYSA-N tin(2+) Chemical compound [Sn+2] IUTCEZPPWBHGIX-UHFFFAOYSA-N 0.000 description 1
- SYRHIZPPCHMRIT-UHFFFAOYSA-N tin(4+) Chemical compound [Sn+4] SYRHIZPPCHMRIT-UHFFFAOYSA-N 0.000 description 1
- AXZWODMDQAVCJE-UHFFFAOYSA-L tin(II) chloride (anhydrous) Chemical compound [Cl-].[Cl-].[Sn+2] AXZWODMDQAVCJE-UHFFFAOYSA-L 0.000 description 1
- JOQGJRQKCIJIDB-UHFFFAOYSA-M tin;chloride Chemical compound [Cl-].[Sn] JOQGJRQKCIJIDB-UHFFFAOYSA-M 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
- C01G19/00—Compounds of tin
- C01G19/04—Halides
- C01G19/08—Stannic chloride
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Inorganic Compounds Of Heavy Metals (AREA)
- Catalysts (AREA)
Priority Applications (5)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE19813104737 DE3104737A1 (de) | 1981-02-11 | 1981-02-11 | Verfahren zur herstellung von zinn-(iv)-chlorid |
| US06/346,299 US4396593A (en) | 1981-02-11 | 1982-02-05 | Process for the production of tin(IV) chloride |
| EP82100884A EP0057929B1 (de) | 1981-02-11 | 1982-02-08 | Verfahren zur Herstellung von Zinn-(IV)-chlorid |
| DE8282100884T DE3260152D1 (en) | 1981-02-11 | 1982-02-08 | Process for the production of tin (iv) chloride |
| JP57018995A JPS57188416A (en) | 1981-02-11 | 1982-02-10 | Manufacture of stannic chloride |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE19813104737 DE3104737A1 (de) | 1981-02-11 | 1981-02-11 | Verfahren zur herstellung von zinn-(iv)-chlorid |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| DE3104737A1 true DE3104737A1 (de) | 1982-08-19 |
Family
ID=6124513
Family Applications (2)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DE19813104737 Withdrawn DE3104737A1 (de) | 1981-02-11 | 1981-02-11 | Verfahren zur herstellung von zinn-(iv)-chlorid |
| DE8282100884T Expired DE3260152D1 (en) | 1981-02-11 | 1982-02-08 | Process for the production of tin (iv) chloride |
Family Applications After (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DE8282100884T Expired DE3260152D1 (en) | 1981-02-11 | 1982-02-08 | Process for the production of tin (iv) chloride |
Country Status (4)
Families Citing this family (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE3217143A1 (de) * | 1982-05-07 | 1983-11-10 | Hoechst Ag, 6230 Frankfurt | Verfahren zur herstellung von zinn-(iv)-chlorid |
| DE3929300C3 (de) * | 1989-09-04 | 1998-10-22 | Elektro Chemie Ibbenbueren | Verfahren zur kontinuierlichen Herstellung von Zinntetrachlorid |
| DE19739155A1 (de) * | 1997-09-06 | 1999-03-11 | Vinnolit Monomer Gmbh & Co Kg | Verfahren zur Herstellung von Zinntetrachlorid |
| WO2001012556A1 (en) * | 1999-08-13 | 2001-02-22 | Anglo American Corporation Of South Africa Limited | Titanium tetrachloride production |
| CN105668620B (zh) * | 2016-01-27 | 2017-11-21 | 柳州豪祥特科技有限公司 | 一种制备四氯化锡的工艺 |
| CN105645466B (zh) * | 2016-01-27 | 2017-11-21 | 柳州豪祥特科技有限公司 | 一种四氯化锡的合成方法 |
Family Cites Families (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US887262A (en) * | 1908-05-12 | Miner Co W H | Antifriction center-bearing for railway-cars. | |
| US1897360A (en) * | 1929-07-09 | 1933-02-14 | Vulcan Detinning Company | Manufacture of stannic chloride |
| US2047545A (en) * | 1929-07-09 | 1936-07-14 | Vulcan Detinning Company | Manufacture of stannic chloride |
| US2061816A (en) * | 1932-05-14 | 1936-11-24 | Gen Chemical Corp | Process of making tin tetrachloride |
| US3848052A (en) * | 1973-05-17 | 1974-11-12 | Vulcan Materials Co | Process for the preparation of stannic chloride |
-
1981
- 1981-02-11 DE DE19813104737 patent/DE3104737A1/de not_active Withdrawn
-
1982
- 1982-02-05 US US06/346,299 patent/US4396593A/en not_active Expired - Lifetime
- 1982-02-08 EP EP82100884A patent/EP0057929B1/de not_active Expired
- 1982-02-08 DE DE8282100884T patent/DE3260152D1/de not_active Expired
- 1982-02-10 JP JP57018995A patent/JPS57188416A/ja active Granted
Also Published As
| Publication number | Publication date |
|---|---|
| EP0057929B1 (de) | 1984-05-16 |
| EP0057929A1 (de) | 1982-08-18 |
| US4396593A (en) | 1983-08-02 |
| JPS57188416A (en) | 1982-11-19 |
| JPH0310574B2 (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html) | 1991-02-14 |
| DE3260152D1 (en) | 1984-06-20 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| AG | Has addition no. |
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| AG | Has addition no. |
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| 8130 | Withdrawal |