DE3020075C2 - Verfahren zur Koagulation von Milcheiweiß - Google Patents
Verfahren zur Koagulation von MilcheiweißInfo
- Publication number
- DE3020075C2 DE3020075C2 DE3020075A DE3020075A DE3020075C2 DE 3020075 C2 DE3020075 C2 DE 3020075C2 DE 3020075 A DE3020075 A DE 3020075A DE 3020075 A DE3020075 A DE 3020075A DE 3020075 C2 DE3020075 C2 DE 3020075C2
- Authority
- DE
- Germany
- Prior art keywords
- milk
- coagulation
- protein
- proteins
- polymer
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- 238000005345 coagulation Methods 0.000 title claims description 53
- 230000015271 coagulation Effects 0.000 title claims description 53
- 238000000034 method Methods 0.000 title claims description 53
- 102000014171 Milk Proteins Human genes 0.000 title claims description 31
- 108010011756 Milk Proteins Proteins 0.000 title claims description 31
- 235000021239 milk protein Nutrition 0.000 title claims description 31
- 230000008569 process Effects 0.000 title description 10
- 235000018102 proteins Nutrition 0.000 claims description 93
- 102000004169 proteins and genes Human genes 0.000 claims description 93
- 108090000623 proteins and genes Proteins 0.000 claims description 93
- 235000013336 milk Nutrition 0.000 claims description 81
- 239000008267 milk Substances 0.000 claims description 81
- 210000004080 milk Anatomy 0.000 claims description 81
- 102000011632 Caseins Human genes 0.000 claims description 36
- 108010076119 Caseins Proteins 0.000 claims description 36
- BECPQYXYKAMYBN-UHFFFAOYSA-N casein, tech. Chemical compound NCCCCC(C(O)=O)N=C(O)C(CC(O)=O)N=C(O)C(CCC(O)=N)N=C(O)C(CC(C)C)N=C(O)C(CCC(O)=O)N=C(O)C(CC(O)=O)N=C(O)C(CCC(O)=O)N=C(O)C(C(C)O)N=C(O)C(CCC(O)=N)N=C(O)C(CCC(O)=N)N=C(O)C(CCC(O)=N)N=C(O)C(CCC(O)=O)N=C(O)C(CCC(O)=O)N=C(O)C(COP(O)(O)=O)N=C(O)C(CCC(O)=N)N=C(O)C(N)CC1=CC=CC=C1 BECPQYXYKAMYBN-UHFFFAOYSA-N 0.000 claims description 36
- 235000021240 caseins Nutrition 0.000 claims description 36
- 239000005018 casein Substances 0.000 claims description 32
- 239000005862 Whey Substances 0.000 claims description 26
- 102000007544 Whey Proteins Human genes 0.000 claims description 26
- 108010046377 Whey Proteins Proteins 0.000 claims description 26
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 23
- 229920000642 polymer Polymers 0.000 claims description 18
- 239000000203 mixture Substances 0.000 claims description 16
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 14
- 239000000843 powder Substances 0.000 claims description 14
- 239000000126 substance Substances 0.000 claims description 13
- 125000003178 carboxy group Chemical group [H]OC(*)=O 0.000 claims description 7
- 102000007327 Protamines Human genes 0.000 claims description 6
- 108010007568 Protamines Proteins 0.000 claims description 6
- 239000007864 aqueous solution Substances 0.000 claims description 6
- 125000000524 functional group Chemical group 0.000 claims description 6
- 229940048914 protamine Drugs 0.000 claims description 6
- 235000008939 whole milk Nutrition 0.000 claims description 6
- 235000020183 skimmed milk Nutrition 0.000 claims description 5
- 102000035118 modified proteins Human genes 0.000 claims description 4
- 108091005573 modified proteins Proteins 0.000 claims description 4
- 229920005615 natural polymer Polymers 0.000 claims description 4
- 238000001704 evaporation Methods 0.000 claims description 3
- 230000008020 evaporation Effects 0.000 claims description 3
- 229920001059 synthetic polymer Polymers 0.000 claims description 3
- 108010082495 Dietary Plant Proteins Proteins 0.000 claims description 2
- 241001465754 Metazoa Species 0.000 claims description 2
- 210000004369 blood Anatomy 0.000 claims description 2
- 239000008280 blood Substances 0.000 claims description 2
- 238000000108 ultra-filtration Methods 0.000 claims description 2
- 108010033040 Histones Proteins 0.000 claims 1
- 108010058846 Ovalbumin Proteins 0.000 claims 1
- 125000001495 ethyl group Chemical group [H]C([H])([H])C([H])([H])* 0.000 claims 1
- 150000004702 methyl esters Chemical class 0.000 claims 1
- 229920000768 polyamine Polymers 0.000 claims 1
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 96
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 description 61
- 229910052757 nitrogen Inorganic materials 0.000 description 48
- 239000000243 solution Substances 0.000 description 35
- HEMHJVSKTPXQMS-UHFFFAOYSA-M sodium hydroxide Inorganic materials [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 18
- 239000000047 product Substances 0.000 description 12
- 210000002966 serum Anatomy 0.000 description 10
- 102000009027 Albumins Human genes 0.000 description 9
- 108010088751 Albumins Proteins 0.000 description 9
- 229920002873 Polyethylenimine Polymers 0.000 description 7
- 230000008859 change Effects 0.000 description 7
- 235000019441 ethanol Nutrition 0.000 description 7
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 description 6
- 238000003756 stirring Methods 0.000 description 6
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 description 5
- 230000002378 acidificating effect Effects 0.000 description 5
- 238000004458 analytical method Methods 0.000 description 5
- 239000007787 solid Substances 0.000 description 5
- 229940021722 caseins Drugs 0.000 description 4
- 230000001112 coagulating effect Effects 0.000 description 4
- 239000003456 ion exchange resin Substances 0.000 description 4
- 229920003303 ion-exchange polymer Polymers 0.000 description 4
- 150000002500 ions Chemical class 0.000 description 4
- 239000000693 micelle Substances 0.000 description 4
- 229920000729 poly(L-lysine) polymer Polymers 0.000 description 4
- 239000000725 suspension Substances 0.000 description 4
- CDBYLPFSWZWCQE-UHFFFAOYSA-L Sodium Carbonate Chemical compound [Na+].[Na+].[O-]C([O-])=O CDBYLPFSWZWCQE-UHFFFAOYSA-L 0.000 description 3
- 239000002253 acid Substances 0.000 description 3
- 238000006243 chemical reaction Methods 0.000 description 3
- 230000032050 esterification Effects 0.000 description 3
- 238000005886 esterification reaction Methods 0.000 description 3
- 238000001914 filtration Methods 0.000 description 3
- 238000011084 recovery Methods 0.000 description 3
- 229940108461 rennet Drugs 0.000 description 3
- 108010058314 rennet Proteins 0.000 description 3
- 239000000377 silicon dioxide Substances 0.000 description 3
- 238000005406 washing Methods 0.000 description 3
- NWUYHJFMYQTDRP-UHFFFAOYSA-N 1,2-bis(ethenyl)benzene;1-ethenyl-2-ethylbenzene;styrene Chemical compound C=CC1=CC=CC=C1.CCC1=CC=CC=C1C=C.C=CC1=CC=CC=C1C=C NWUYHJFMYQTDRP-UHFFFAOYSA-N 0.000 description 2
- HZAXFHJVJLSVMW-UHFFFAOYSA-N 2-Aminoethan-1-ol Chemical compound NCCO HZAXFHJVJLSVMW-UHFFFAOYSA-N 0.000 description 2
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 description 2
- 238000007696 Kjeldahl method Methods 0.000 description 2
- NBIIXXVUZAFLBC-UHFFFAOYSA-N Phosphoric acid Chemical compound OP(O)(O)=O NBIIXXVUZAFLBC-UHFFFAOYSA-N 0.000 description 2
- 238000013019 agitation Methods 0.000 description 2
- -1 aminoethoxy Chemical class 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- 238000002474 experimental method Methods 0.000 description 2
- 239000012458 free base Substances 0.000 description 2
- 238000010438 heat treatment Methods 0.000 description 2
- 239000007788 liquid Substances 0.000 description 2
- 239000002244 precipitate Substances 0.000 description 2
- 235000012239 silicon dioxide Nutrition 0.000 description 2
- QCVGEOXPDFCNHA-UHFFFAOYSA-N 5,5-dimethyl-2,4-dioxo-1,3-oxazolidine-3-carboxamide Chemical compound CC1(C)OC(=O)N(C(N)=O)C1=O QCVGEOXPDFCNHA-UHFFFAOYSA-N 0.000 description 1
- GUBGYTABKSRVRQ-XLOQQCSPSA-N Alpha-Lactose Chemical compound O[C@@H]1[C@@H](O)[C@@H](O)[C@@H](CO)O[C@H]1O[C@@H]1[C@@H](CO)O[C@H](O)[C@H](O)[C@H]1O GUBGYTABKSRVRQ-XLOQQCSPSA-N 0.000 description 1
- 241000208199 Buxus sempervirens Species 0.000 description 1
- VEXZGXHMUGYJMC-UHFFFAOYSA-M Chloride anion Chemical compound [Cl-] VEXZGXHMUGYJMC-UHFFFAOYSA-M 0.000 description 1
- 102000002322 Egg Proteins Human genes 0.000 description 1
- 108010000912 Egg Proteins Proteins 0.000 description 1
- 102000006395 Globulins Human genes 0.000 description 1
- 108010044091 Globulins Proteins 0.000 description 1
- WQZGKKKJIJFFOK-GASJEMHNSA-N Glucose Natural products OC[C@H]1OC(O)[C@H](O)[C@@H](O)[C@@H]1O WQZGKKKJIJFFOK-GASJEMHNSA-N 0.000 description 1
- 102000001554 Hemoglobins Human genes 0.000 description 1
- 108010054147 Hemoglobins Proteins 0.000 description 1
- GUBGYTABKSRVRQ-QKKXKWKRSA-N Lactose Natural products OC[C@H]1O[C@@H](O[C@H]2[C@H](O)[C@@H](O)C(O)O[C@@H]2CO)[C@H](O)[C@@H](O)[C@H]1O GUBGYTABKSRVRQ-QKKXKWKRSA-N 0.000 description 1
- 240000007594 Oryza sativa Species 0.000 description 1
- 235000007164 Oryza sativa Nutrition 0.000 description 1
- 102000057297 Pepsin A Human genes 0.000 description 1
- 108090000284 Pepsin A Proteins 0.000 description 1
- 108091005804 Peptidases Proteins 0.000 description 1
- 102000035195 Peptidases Human genes 0.000 description 1
- 108010039918 Polylysine Proteins 0.000 description 1
- 102100034750 Protamine-2 Human genes 0.000 description 1
- 229920002472 Starch Polymers 0.000 description 1
- 230000009471 action Effects 0.000 description 1
- 239000000853 adhesive Substances 0.000 description 1
- 230000001070 adhesive effect Effects 0.000 description 1
- 150000001298 alcohols Chemical class 0.000 description 1
- 229910000147 aluminium phosphate Inorganic materials 0.000 description 1
- 235000013405 beer Nutrition 0.000 description 1
- WQZGKKKJIJFFOK-VFUOTHLCSA-N beta-D-glucose Chemical compound OC[C@H]1O[C@@H](O)[C@H](O)[C@@H](O)[C@@H]1O WQZGKKKJIJFFOK-VFUOTHLCSA-N 0.000 description 1
- 230000033228 biological regulation Effects 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 239000012888 bovine serum Substances 0.000 description 1
- 244000309466 calf Species 0.000 description 1
- 235000013339 cereals Nutrition 0.000 description 1
- 239000003795 chemical substances by application Substances 0.000 description 1
- OEYIOHPDSNJKLS-UHFFFAOYSA-N choline Chemical compound C[N+](C)(C)CCO OEYIOHPDSNJKLS-UHFFFAOYSA-N 0.000 description 1
- 229960001231 choline Drugs 0.000 description 1
- 239000013065 commercial product Substances 0.000 description 1
- 230000006378 damage Effects 0.000 description 1
- 238000004925 denaturation Methods 0.000 description 1
- 230000036425 denaturation Effects 0.000 description 1
- 239000012153 distilled water Substances 0.000 description 1
- 238000001035 drying Methods 0.000 description 1
- 235000014103 egg white Nutrition 0.000 description 1
- 210000000969 egg white Anatomy 0.000 description 1
- 238000006911 enzymatic reaction Methods 0.000 description 1
- 238000000605 extraction Methods 0.000 description 1
- 235000013305 food Nutrition 0.000 description 1
- 239000008103 glucose Substances 0.000 description 1
- 150000004676 glycans Chemical class 0.000 description 1
- 235000011187 glycerol Nutrition 0.000 description 1
- 239000008187 granular material Substances 0.000 description 1
- 229910052500 inorganic mineral Inorganic materials 0.000 description 1
- 239000008101 lactose Substances 0.000 description 1
- 239000007791 liquid phase Substances 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- VNWKTOKETHGBQD-UHFFFAOYSA-N methane Natural products C VNWKTOKETHGBQD-UHFFFAOYSA-N 0.000 description 1
- 239000011707 mineral Substances 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000020477 pH reduction Effects 0.000 description 1
- 239000003973 paint Substances 0.000 description 1
- 239000002245 particle Substances 0.000 description 1
- 229940111202 pepsin Drugs 0.000 description 1
- 229920003023 plastic Polymers 0.000 description 1
- 239000004033 plastic Substances 0.000 description 1
- 229920000656 polylysine Polymers 0.000 description 1
- 229920002714 polyornithine Polymers 0.000 description 1
- 108010055896 polyornithine Proteins 0.000 description 1
- 229920001282 polysaccharide Polymers 0.000 description 1
- 239000005017 polysaccharide Substances 0.000 description 1
- 229920002717 polyvinylpyridine Polymers 0.000 description 1
- 235000008476 powdered milk Nutrition 0.000 description 1
- 230000001376 precipitating effect Effects 0.000 description 1
- 108010076339 protamine 2 Proteins 0.000 description 1
- 229940024999 proteolytic enzymes for treatment of wounds and ulcers Drugs 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
- 230000008929 regeneration Effects 0.000 description 1
- 238000011069 regeneration method Methods 0.000 description 1
- 235000009566 rice Nutrition 0.000 description 1
- 150000003839 salts Chemical class 0.000 description 1
- 238000000926 separation method Methods 0.000 description 1
- 230000007928 solubilization Effects 0.000 description 1
- 238000005063 solubilization Methods 0.000 description 1
- 239000008107 starch Substances 0.000 description 1
- 235000019698 starch Nutrition 0.000 description 1
- 238000004448 titration Methods 0.000 description 1
- YNJBWRMUSHSURL-UHFFFAOYSA-N trichloroacetic acid Chemical compound OC(=O)C(Cl)(Cl)Cl YNJBWRMUSHSURL-UHFFFAOYSA-N 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23J—PROTEIN COMPOSITIONS FOR FOODSTUFFS; WORKING-UP PROTEINS FOR FOODSTUFFS; PHOSPHATIDE COMPOSITIONS FOR FOODSTUFFS
- A23J1/00—Obtaining protein compositions for foodstuffs; Bulk opening of eggs and separation of yolks from whites
- A23J1/20—Obtaining protein compositions for foodstuffs; Bulk opening of eggs and separation of yolks from whites from milk, e.g. casein; from whey
- A23J1/207—Co-precipitates of casein and lactalbumine
Landscapes
- Life Sciences & Earth Sciences (AREA)
- Chemical & Material Sciences (AREA)
- Biochemistry (AREA)
- Engineering & Computer Science (AREA)
- Food Science & Technology (AREA)
- Polymers & Plastics (AREA)
- Dairy Products (AREA)
- Peptides Or Proteins (AREA)
- Paints Or Removers (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| IT7923079A IT1165079B (it) | 1979-05-29 | 1979-05-29 | Metodo di coagulazione del latte |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| DE3020075A1 DE3020075A1 (de) | 1980-12-04 |
| DE3020075C2 true DE3020075C2 (de) | 1982-10-14 |
Family
ID=11203545
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DE3020075A Expired DE3020075C2 (de) | 1979-05-29 | 1980-05-27 | Verfahren zur Koagulation von Milcheiweiß |
Country Status (4)
| Country | Link |
|---|---|
| DE (1) | DE3020075C2 (it) |
| FR (1) | FR2457642B1 (it) |
| IT (1) | IT1165079B (it) |
| NL (1) | NL190691C (it) |
Family Cites Families (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DD97815A3 (it) * | 1970-08-04 | 1973-05-21 | ||
| BE791350A (nl) * | 1971-11-15 | 1973-05-14 | Stichting Bedrijven Van Het | Werkwijze voor de bereiding van een melkeiwit-coprecipitaat |
| US4100149A (en) * | 1975-08-28 | 1978-07-11 | Rhone-Poulenc Industries | Method of separating proteins by ion exchange |
| FR2399214A2 (fr) * | 1977-08-05 | 1979-03-02 | Rhone Poulenc Ind | Procede d'extraction des proteines du lait |
-
1979
- 1979-05-29 IT IT7923079A patent/IT1165079B/it active
-
1980
- 1980-05-27 DE DE3020075A patent/DE3020075C2/de not_active Expired
- 1980-05-28 FR FR808011856A patent/FR2457642B1/fr not_active Expired
- 1980-05-29 NL NL8003129A patent/NL190691C/xx not_active IP Right Cessation
Also Published As
| Publication number | Publication date |
|---|---|
| NL190691B (nl) | 1994-02-01 |
| FR2457642A1 (fr) | 1980-12-26 |
| IT1165079B (it) | 1987-04-22 |
| NL190691C (nl) | 1994-07-01 |
| NL8003129A (nl) | 1980-12-02 |
| IT7923079A0 (it) | 1979-05-29 |
| FR2457642B1 (fr) | 1985-07-26 |
| DE3020075A1 (de) | 1980-12-04 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| DE3008900C2 (it) | ||
| DE3043691A1 (de) | Modifizierte molkeproteinzusammensetzungen | |
| DE2718046C2 (it) | ||
| CH666992A5 (de) | Verfahren zur herstellung eines sojaproteinisolates mit einem niederen phytat-gehalt. | |
| DE4134854C2 (it) | ||
| DE2354195B2 (de) | Teigentwicklungs- und konditionierungsmittel | |
| DE3447576A1 (de) | Faserige serum-milch-protein-komplexe | |
| DE10010113A1 (de) | Verfahren zur Isolierung von Schwammkollagen sowie Herstellung von nanoparikulärem Kollagen | |
| DE2557782A1 (de) | Verfahren zur herstellung eines waermekoagulierbaren viskosen proteinproduktes | |
| DE2725711A1 (de) | Verfahren zur herstellung von antithrombin iii | |
| DE1667959B2 (de) | Verfahren zur Herstellung von Sojaproteinen mit hoher Gelbildungs fahigkeit | |
| DE3024356A1 (de) | Verfahren zur senkung der geliertemperatur von aus milch erhaltenen molkeproteinen | |
| DE69632561T2 (de) | Verfahren zur Herstellung von fraktionierten Sojaproteinen und Verwendung derselben in Nahrungsmitteln | |
| DE2260119B2 (de) | Essbare Proteinfaser auf Kaseinbasis und Verfahren zur Herstellung derselben | |
| DE3020075C2 (de) | Verfahren zur Koagulation von Milcheiweiß | |
| DE2419308C3 (de) | Verfahren zur Isolierung und Reinigung von Protein aus Käsemolke | |
| DE1965438A1 (de) | Modifizierte Proteine,diese enthaltende Loesungen und Emulsionen und Verfahren zu deren Herstellung | |
| DE2355850C2 (de) | Proteinzusammensetzung und Verfahren zu deren Herstellung | |
| DE2413194A1 (de) | Verfahren zur herstellung von kaese | |
| DE2803039A1 (de) | Verfahren zur entfernung von eisenverbindungen aus einem waessrigen bluthydrolysat | |
| DE2323298A1 (de) | Verfahren zur herstellung eines oelsaatenproteins mit vorbestimmtem loeslichkeitsgrad | |
| DE2536899A1 (de) | Verfahren zur gewinnung von kasein und molke bzw. molkeprodukten aus magermilch oder deren gemischen mit anderen fluessigen milchprodukten | |
| DE2213956A1 (de) | Verfahren zur Herstellung von trockenen Sojaproteingemischen | |
| DE2326483C3 (de) | Verfahren zur Strukturierung von Globulinen und Albuminen | |
| DE2512934A1 (de) | Verfahren zur herstellung von wasserdispergierbaren, stabilisierten reaktionsprodukten aus protein und alkylenglykolalginaten |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| OD | Request for examination | ||
| 8125 | Change of the main classification | ||
| D2 | Grant after examination | ||
| 8339 | Ceased/non-payment of the annual fee |