DE2550611A1 - Rauchbares material und verfahren zu seiner herstellung - Google Patents
Rauchbares material und verfahren zu seiner herstellungInfo
- Publication number
- DE2550611A1 DE2550611A1 DE19752550611 DE2550611A DE2550611A1 DE 2550611 A1 DE2550611 A1 DE 2550611A1 DE 19752550611 DE19752550611 DE 19752550611 DE 2550611 A DE2550611 A DE 2550611A DE 2550611 A1 DE2550611 A1 DE 2550611A1
- Authority
- DE
- Germany
- Prior art keywords
- smokable material
- material according
- cellulose acetate
- sheet
- smokable
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Withdrawn
Links
- 239000000463 material Substances 0.000 title claims description 116
- 238000004519 manufacturing process Methods 0.000 title claims description 7
- QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 claims description 60
- 229920002301 cellulose acetate Polymers 0.000 claims description 59
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 38
- 235000019504 cigarettes Nutrition 0.000 claims description 34
- 238000006467 substitution reaction Methods 0.000 claims description 34
- 241000208125 Nicotiana Species 0.000 claims description 32
- 235000002637 Nicotiana tabacum Nutrition 0.000 claims description 32
- 239000000843 powder Substances 0.000 claims description 25
- 239000002002 slurry Substances 0.000 claims description 25
- 239000000203 mixture Substances 0.000 claims description 22
- 238000000034 method Methods 0.000 claims description 19
- 150000002148 esters Chemical class 0.000 claims description 16
- 239000000945 filler Substances 0.000 claims description 15
- 239000010408 film Substances 0.000 claims description 14
- 239000002253 acid Substances 0.000 claims description 13
- 125000001931 aliphatic group Chemical group 0.000 claims description 13
- 230000008569 process Effects 0.000 claims description 11
- 229920002678 cellulose Polymers 0.000 claims description 10
- 239000001913 cellulose Substances 0.000 claims description 10
- 150000001720 carbohydrates Chemical class 0.000 claims description 9
- 235000014633 carbohydrates Nutrition 0.000 claims description 9
- 238000002485 combustion reaction Methods 0.000 claims description 7
- 239000000835 fiber Substances 0.000 claims description 7
- 239000000654 additive Substances 0.000 claims description 6
- 230000003750 conditioning effect Effects 0.000 claims description 6
- 239000003960 organic solvent Substances 0.000 claims description 6
- DPXJVFZANSGRMM-UHFFFAOYSA-N acetic acid;2,3,4,5,6-pentahydroxyhexanal;sodium Chemical compound [Na].CC(O)=O.OCC(O)C(O)C(O)C(O)C=O DPXJVFZANSGRMM-UHFFFAOYSA-N 0.000 claims description 5
- 235000019812 sodium carboxymethyl cellulose Nutrition 0.000 claims description 5
- 239000002904 solvent Substances 0.000 claims description 5
- 239000000126 substance Substances 0.000 claims description 5
- FERIUCNNQQJTOY-UHFFFAOYSA-N Butyric acid Chemical compound CCCC(O)=O FERIUCNNQQJTOY-UHFFFAOYSA-N 0.000 claims description 4
- 229920001218 Pullulan Polymers 0.000 claims description 4
- 239000004373 Pullulan Substances 0.000 claims description 4
- 125000004432 carbon atom Chemical group C* 0.000 claims description 4
- 235000019506 cigar Nutrition 0.000 claims description 4
- XBDQKXXYIPTUBI-UHFFFAOYSA-N dimethylselenoniopropionate Natural products CCC(O)=O XBDQKXXYIPTUBI-UHFFFAOYSA-N 0.000 claims description 4
- 239000003906 humectant Substances 0.000 claims description 4
- 235000019423 pullulan Nutrition 0.000 claims description 4
- SNICXCGAKADSCV-JTQLQIEISA-N (-)-Nicotine Chemical compound CN1CCC[C@H]1C1=CC=CN=C1 SNICXCGAKADSCV-JTQLQIEISA-N 0.000 claims description 3
- QTBSBXVTEAMEQO-UHFFFAOYSA-M Acetate Chemical compound CC([O-])=O QTBSBXVTEAMEQO-UHFFFAOYSA-M 0.000 claims description 3
- 229920002472 Starch Polymers 0.000 claims description 3
- 238000002156 mixing Methods 0.000 claims description 3
- 229960002715 nicotine Drugs 0.000 claims description 3
- SNICXCGAKADSCV-UHFFFAOYSA-N nicotine Natural products CN1CCCC1C1=CC=CN=C1 SNICXCGAKADSCV-UHFFFAOYSA-N 0.000 claims description 3
- 238000002360 preparation method Methods 0.000 claims description 3
- 239000008107 starch Substances 0.000 claims description 3
- 235000019698 starch Nutrition 0.000 claims description 3
- 229920002307 Dextran Polymers 0.000 claims description 2
- 150000007513 acids Chemical class 0.000 claims description 2
- 230000015572 biosynthetic process Effects 0.000 claims description 2
- 239000001768 carboxy methyl cellulose Substances 0.000 claims description 2
- 239000003607 modifier Substances 0.000 claims description 2
- 235000019260 propionic acid Nutrition 0.000 claims description 2
- IUVKMZGDUIUOCP-BTNSXGMBSA-N quinbolone Chemical compound O([C@H]1CC[C@H]2[C@H]3[C@@H]([C@]4(C=CC(=O)C=C4CC3)C)CC[C@@]21C)C1=CCCC1 IUVKMZGDUIUOCP-BTNSXGMBSA-N 0.000 claims description 2
- 239000010409 thin film Substances 0.000 claims description 2
- 239000011888 foil Substances 0.000 claims 3
- 229920000881 Modified starch Polymers 0.000 claims 1
- 230000000996 additive effect Effects 0.000 claims 1
- 125000003118 aryl group Chemical group 0.000 claims 1
- 239000012765 fibrous filler Substances 0.000 claims 1
- 235000019426 modified starch Nutrition 0.000 claims 1
- 238000007493 shaping process Methods 0.000 claims 1
- 229920001027 sodium carboxymethylcellulose Polymers 0.000 claims 1
- 229940081735 acetylcellulose Drugs 0.000 description 54
- 206010013911 Dysgeusia Diseases 0.000 description 29
- CSCPPACGZOOCGX-UHFFFAOYSA-N Acetone Chemical compound CC(C)=O CSCPPACGZOOCGX-UHFFFAOYSA-N 0.000 description 24
- 229960000583 acetic acid Drugs 0.000 description 19
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 description 18
- 229920001131 Pulp (paper) Polymers 0.000 description 13
- 230000002650 habitual effect Effects 0.000 description 13
- 230000000391 smoking effect Effects 0.000 description 13
- KFZMGEQAYNKOFK-UHFFFAOYSA-N Isopropanol Chemical compound CC(C)O KFZMGEQAYNKOFK-UHFFFAOYSA-N 0.000 description 12
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 description 11
- 231100000344 non-irritating Toxicity 0.000 description 11
- WFDIJRYMOXRFFG-UHFFFAOYSA-N acetic acid anhydride Natural products CC(=O)OC(C)=O WFDIJRYMOXRFFG-UHFFFAOYSA-N 0.000 description 10
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 description 9
- 239000011521 glass Substances 0.000 description 9
- 238000003756 stirring Methods 0.000 description 8
- 230000001143 conditioned effect Effects 0.000 description 7
- 239000003085 diluting agent Substances 0.000 description 7
- 238000012360 testing method Methods 0.000 description 7
- 239000012744 reinforcing agent Substances 0.000 description 6
- 239000011230 binding agent Substances 0.000 description 5
- 235000011187 glycerol Nutrition 0.000 description 5
- 230000007794 irritation Effects 0.000 description 5
- 239000007788 liquid Substances 0.000 description 5
- 238000005406 washing Methods 0.000 description 5
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 description 4
- 238000006243 chemical reaction Methods 0.000 description 4
- 239000003795 chemical substances by application Substances 0.000 description 4
- 238000010438 heat treatment Methods 0.000 description 4
- 238000006460 hydrolysis reaction Methods 0.000 description 4
- 230000007935 neutral effect Effects 0.000 description 4
- 230000003472 neutralizing effect Effects 0.000 description 4
- 230000000704 physical effect Effects 0.000 description 4
- FGIUAXJPYTZDNR-UHFFFAOYSA-N potassium nitrate Chemical compound [K+].[O-][N+]([O-])=O FGIUAXJPYTZDNR-UHFFFAOYSA-N 0.000 description 4
- 239000000779 smoke Substances 0.000 description 4
- 229920002134 Carboxymethyl cellulose Polymers 0.000 description 3
- VMHLLURERBWHNL-UHFFFAOYSA-M Sodium acetate Chemical compound [Na+].CC([O-])=O VMHLLURERBWHNL-UHFFFAOYSA-M 0.000 description 3
- 125000000218 acetic acid group Chemical group C(C)(=O)* 0.000 description 3
- -1 cellulose and starch Chemical class 0.000 description 3
- 230000008859 change Effects 0.000 description 3
- 239000000796 flavoring agent Substances 0.000 description 3
- 239000001632 sodium acetate Substances 0.000 description 3
- 235000017281 sodium acetate Nutrition 0.000 description 3
- 239000000725 suspension Substances 0.000 description 3
- 229920001747 Cellulose diacetate Polymers 0.000 description 2
- 230000002378 acidificating effect Effects 0.000 description 2
- 239000007795 chemical reaction product Substances 0.000 description 2
- 238000007796 conventional method Methods 0.000 description 2
- 230000007423 decrease Effects 0.000 description 2
- 235000019634 flavors Nutrition 0.000 description 2
- 239000012362 glacial acetic acid Substances 0.000 description 2
- LEQAOMBKQFMDFZ-UHFFFAOYSA-N glyoxal Chemical compound O=CC=O LEQAOMBKQFMDFZ-UHFFFAOYSA-N 0.000 description 2
- 230000007062 hydrolysis Effects 0.000 description 2
- 239000002245 particle Substances 0.000 description 2
- 235000021395 porridge Nutrition 0.000 description 2
- 239000004323 potassium nitrate Substances 0.000 description 2
- 235000010333 potassium nitrate Nutrition 0.000 description 2
- 230000005070 ripening Effects 0.000 description 2
- 238000005096 rolling process Methods 0.000 description 2
- 239000011122 softwood Substances 0.000 description 2
- 239000007787 solid Substances 0.000 description 2
- 229920002284 Cellulose triacetate Polymers 0.000 description 1
- 229920000742 Cotton Polymers 0.000 description 1
- 244000043261 Hevea brasiliensis Species 0.000 description 1
- SMEGJBVQLJJKKX-HOTMZDKISA-N [(2R,3S,4S,5R,6R)-5-acetyloxy-3,4,6-trihydroxyoxan-2-yl]methyl acetate Chemical compound CC(=O)OC[C@@H]1[C@H]([C@@H]([C@H]([C@@H](O1)O)OC(=O)C)O)O SMEGJBVQLJJKKX-HOTMZDKISA-N 0.000 description 1
- NNLVGZFZQQXQNW-ADJNRHBOSA-N [(2r,3r,4s,5r,6s)-4,5-diacetyloxy-3-[(2s,3r,4s,5r,6r)-3,4,5-triacetyloxy-6-(acetyloxymethyl)oxan-2-yl]oxy-6-[(2r,3r,4s,5r,6s)-4,5,6-triacetyloxy-2-(acetyloxymethyl)oxan-3-yl]oxyoxan-2-yl]methyl acetate Chemical compound O([C@@H]1O[C@@H]([C@H]([C@H](OC(C)=O)[C@H]1OC(C)=O)O[C@H]1[C@@H]([C@@H](OC(C)=O)[C@H](OC(C)=O)[C@@H](COC(C)=O)O1)OC(C)=O)COC(=O)C)[C@@H]1[C@@H](COC(C)=O)O[C@@H](OC(C)=O)[C@H](OC(C)=O)[C@H]1OC(C)=O NNLVGZFZQQXQNW-ADJNRHBOSA-N 0.000 description 1
- 125000000217 alkyl group Chemical group 0.000 description 1
- 230000002238 attenuated effect Effects 0.000 description 1
- 230000008901 benefit Effects 0.000 description 1
- 125000003178 carboxy group Chemical group [H]OC(*)=O 0.000 description 1
- 235000010948 carboxy methyl cellulose Nutrition 0.000 description 1
- 239000008112 carboxymethyl-cellulose Substances 0.000 description 1
- 239000003054 catalyst Substances 0.000 description 1
- 238000007385 chemical modification Methods 0.000 description 1
- 230000000052 comparative effect Effects 0.000 description 1
- 238000001514 detection method Methods 0.000 description 1
- 239000006185 dispersion Substances 0.000 description 1
- 238000011156 evaluation Methods 0.000 description 1
- 239000005454 flavour additive Substances 0.000 description 1
- 235000013355 food flavoring agent Nutrition 0.000 description 1
- 150000004676 glycans Chemical class 0.000 description 1
- 229940015043 glyoxal Drugs 0.000 description 1
- 230000003301 hydrolyzing effect Effects 0.000 description 1
- 125000002887 hydroxy group Chemical group [H]O* 0.000 description 1
- 238000007654 immersion Methods 0.000 description 1
- 238000009413 insulation Methods 0.000 description 1
- 238000004898 kneading Methods 0.000 description 1
- TWNIBLMWSKIRAT-VFUOTHLCSA-N levoglucosan Chemical group O[C@@H]1[C@@H](O)[C@H](O)[C@H]2CO[C@@H]1O2 TWNIBLMWSKIRAT-VFUOTHLCSA-N 0.000 description 1
- GMDNUWQNDQDBNQ-UHFFFAOYSA-L magnesium;diformate Chemical compound [Mg+2].[O-]C=O.[O-]C=O GMDNUWQNDQDBNQ-UHFFFAOYSA-L 0.000 description 1
- 230000035800 maturation Effects 0.000 description 1
- 230000010198 maturation time Effects 0.000 description 1
- 229920000609 methyl cellulose Polymers 0.000 description 1
- 239000001923 methylcellulose Substances 0.000 description 1
- 235000010981 methylcellulose Nutrition 0.000 description 1
- 229920003052 natural elastomer Polymers 0.000 description 1
- 229920001194 natural rubber Polymers 0.000 description 1
- 229920001282 polysaccharide Polymers 0.000 description 1
- 239000005017 polysaccharide Substances 0.000 description 1
- 239000012716 precipitator Substances 0.000 description 1
- 239000000047 product Substances 0.000 description 1
- 230000001105 regulatory effect Effects 0.000 description 1
- 230000000717 retained effect Effects 0.000 description 1
- 238000007372 rollout process Methods 0.000 description 1
- 150000003839 salts Chemical class 0.000 description 1
- 238000007613 slurry method Methods 0.000 description 1
- 159000000000 sodium salts Chemical class 0.000 description 1
- 239000007858 starting material Substances 0.000 description 1
- 238000004809 thin layer chromatography Methods 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/10—Chemical features of tobacco products or tobacco substitutes
- A24B15/12—Chemical features of tobacco products or tobacco substitutes of reconstituted tobacco
- A24B15/14—Chemical features of tobacco products or tobacco substitutes of reconstituted tobacco made of tobacco and a binding agent not derived from tobacco
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/10—Chemical features of tobacco products or tobacco substitutes
- A24B15/16—Chemical features of tobacco products or tobacco substitutes of tobacco substitutes
Landscapes
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Manufacture Of Tobacco Products (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP49129699A JPS5154997A (en) | 1974-11-11 | 1974-11-11 | Tabakososeibutsuno seizohoho |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| DE2550611A1 true DE2550611A1 (de) | 1976-05-13 |
Family
ID=15015997
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DE19752550611 Withdrawn DE2550611A1 (de) | 1974-11-11 | 1975-11-11 | Rauchbares material und verfahren zu seiner herstellung |
Country Status (5)
| Country | Link |
|---|---|
| US (1) | US4068670A (enExample) |
| JP (1) | JPS5154997A (enExample) |
| DE (1) | DE2550611A1 (enExample) |
| FR (1) | FR2290165A1 (enExample) |
| GB (1) | GB1528786A (enExample) |
Families Citing this family (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| FR2582571B1 (fr) * | 1985-05-30 | 1987-07-17 | Tabacs & Allumettes Ind | Procede de fabrication d'un materiau a fumer et materiau a fumer |
| IE873108L (en) * | 1986-12-12 | 1988-06-12 | Huels Chemische Werke Ag | Impact modifying agent for use with smoking articles |
| CN105518059B (zh) * | 2013-09-02 | 2019-01-01 | 捷恩智株式会社 | 多孔性纤维素粒子的制造方法、多孔性纤维素粒子及色谱法用填充剂 |
| JP7653446B2 (ja) * | 2020-10-02 | 2025-03-28 | 日本たばこ産業株式会社 | たばこシート |
| CN113729260B (zh) * | 2021-09-20 | 2022-12-27 | 河南中烟工业有限责任公司 | 一种焦甜香韵潜香物质及潜香型再造烟叶的制备方法 |
Family Cites Families (13)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| FR644117A (fr) * | 1926-12-30 | 1928-10-02 | Procédé de préparation de feuilles et d'enveloppes au moyen de tabac et de déchets de tabac | |
| US2797689A (en) * | 1955-04-11 | 1957-07-02 | Gen Cigar Co | Tobacco products and process therefor |
| FR1180022A (fr) * | 1957-05-17 | 1959-06-01 | Gen Cigar Co | Procédé de préparation de produits à base de tabac et produits conformes à ceuxobtenus |
| US3012562A (en) * | 1957-06-12 | 1961-12-12 | American Mach & Foundry | Manufacture of tobacco sheet |
| US3012561A (en) * | 1957-06-12 | 1961-12-12 | American Mach & Foundry | Manufacture of tobacco sheet |
| US2976873A (en) * | 1959-04-06 | 1961-03-28 | American Mach & Foundry | Tobacco sheet |
| DE1517237C3 (de) * | 1960-08-17 | 1975-02-13 | Amf Inc., New York, N.Y. (V.St.A.) | Verfahren zum Herstellen von Tabakfolien |
| NL6501218A (enExample) * | 1964-01-31 | 1965-08-02 | ||
| BE687507A (enExample) * | 1966-09-28 | 1967-03-01 | ||
| FR1546092A (fr) * | 1966-12-01 | 1968-11-15 | Gen Cigar Co | Procédé de fabrication de produits à partir de tabac et produits ainsi obtenus |
| US3404691A (en) * | 1967-10-11 | 1968-10-08 | American Mach & Foundry | Tobacco product and process for making same |
| UST912011I4 (en) | 1972-06-30 | 1973-07-24 | Defensive publication | |
| US3931824A (en) * | 1973-09-10 | 1976-01-13 | Celanese Corporation | Smoking materials |
-
1974
- 1974-11-11 JP JP49129699A patent/JPS5154997A/ja active Pending
-
1975
- 1975-11-07 GB GB46145/75A patent/GB1528786A/en not_active Expired
- 1975-11-10 US US05/630,272 patent/US4068670A/en not_active Expired - Lifetime
- 1975-11-10 FR FR7534305A patent/FR2290165A1/fr active Granted
- 1975-11-11 DE DE19752550611 patent/DE2550611A1/de not_active Withdrawn
Also Published As
| Publication number | Publication date |
|---|---|
| US4068670A (en) | 1978-01-17 |
| FR2290165A1 (fr) | 1976-06-04 |
| GB1528786A (en) | 1978-10-18 |
| JPS5154997A (en) | 1976-05-14 |
| FR2290165B1 (enExample) | 1977-12-16 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| 8139 | Disposal/non-payment of the annual fee |