DE2531646A1 - Verfahren und vorrichtung zur herstellung von tonerde - Google Patents
Verfahren und vorrichtung zur herstellung von tonerdeInfo
- Publication number
- DE2531646A1 DE2531646A1 DE19752531646 DE2531646A DE2531646A1 DE 2531646 A1 DE2531646 A1 DE 2531646A1 DE 19752531646 DE19752531646 DE 19752531646 DE 2531646 A DE2531646 A DE 2531646A DE 2531646 A1 DE2531646 A1 DE 2531646A1
- Authority
- DE
- Germany
- Prior art keywords
- stirrer
- product
- stirring
- agitator
- crystals
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Withdrawn
Links
- 238000000034 method Methods 0.000 title claims description 97
- 238000004519 manufacturing process Methods 0.000 title description 10
- 239000004927 clay Substances 0.000 title description 9
- 239000013078 crystal Substances 0.000 claims description 153
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 claims description 145
- 238000003756 stirring Methods 0.000 claims description 81
- 230000008569 process Effects 0.000 claims description 43
- 239000012452 mother liquor Substances 0.000 claims description 37
- PNEYBMLMFCGWSK-UHFFFAOYSA-N aluminium oxide Inorganic materials [O-2].[O-2].[O-2].[Al+3].[Al+3] PNEYBMLMFCGWSK-UHFFFAOYSA-N 0.000 claims description 34
- 239000000243 solution Substances 0.000 claims description 29
- WNROFYMDJYEPJX-UHFFFAOYSA-K aluminium hydroxide Chemical compound [OH-].[OH-].[OH-].[Al+3] WNROFYMDJYEPJX-UHFFFAOYSA-K 0.000 claims description 26
- 229910001570 bauxite Inorganic materials 0.000 claims description 13
- 238000011081 inoculation Methods 0.000 claims description 10
- 238000002255 vaccination Methods 0.000 claims description 10
- 239000000725 suspension Substances 0.000 claims description 9
- 239000007787 solid Substances 0.000 claims description 8
- 239000012535 impurity Substances 0.000 claims description 5
- 230000015572 biosynthetic process Effects 0.000 claims description 3
- 239000000463 material Substances 0.000 claims description 3
- 239000012047 saturated solution Substances 0.000 claims description 3
- 229910018072 Al 2 O 3 Inorganic materials 0.000 claims 1
- 238000001816 cooling Methods 0.000 claims 1
- 238000001704 evaporation Methods 0.000 claims 1
- 230000008020 evaporation Effects 0.000 claims 1
- 235000011121 sodium hydroxide Nutrition 0.000 description 52
- 239000000047 product Substances 0.000 description 51
- TWNQGVIAIRXVLR-UHFFFAOYSA-N oxo(oxoalumanyloxy)alumane Chemical compound O=[Al]O[Al]=O TWNQGVIAIRXVLR-UHFFFAOYSA-N 0.000 description 12
- 239000000203 mixture Substances 0.000 description 8
- 239000003518 caustics Substances 0.000 description 7
- 239000000706 filtrate Substances 0.000 description 7
- 238000013019 agitation Methods 0.000 description 6
- 239000003513 alkali Substances 0.000 description 6
- 238000010899 nucleation Methods 0.000 description 6
- 239000010802 sludge Substances 0.000 description 5
- 239000002562 thickening agent Substances 0.000 description 5
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 description 4
- 229910052782 aluminium Inorganic materials 0.000 description 4
- 230000029087 digestion Effects 0.000 description 4
- 239000012065 filter cake Substances 0.000 description 4
- 239000007789 gas Substances 0.000 description 4
- 239000002002 slurry Substances 0.000 description 4
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 4
- YCKRFDGAMUMZLT-UHFFFAOYSA-N Fluorine atom Chemical compound [F] YCKRFDGAMUMZLT-UHFFFAOYSA-N 0.000 description 3
- WMWXXXSCZVGQAR-UHFFFAOYSA-N dialuminum;oxygen(2-);hydrate Chemical class O.[O-2].[O-2].[O-2].[Al+3].[Al+3] WMWXXXSCZVGQAR-UHFFFAOYSA-N 0.000 description 3
- 239000011737 fluorine Substances 0.000 description 3
- 229910052731 fluorine Inorganic materials 0.000 description 3
- 239000007788 liquid Substances 0.000 description 3
- 229920006395 saturated elastomer Polymers 0.000 description 3
- 239000011734 sodium Substances 0.000 description 3
- 238000005406 washing Methods 0.000 description 3
- 239000002699 waste material Substances 0.000 description 3
- 238000004131 Bayer process Methods 0.000 description 2
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 description 2
- CDBYLPFSWZWCQE-UHFFFAOYSA-L Sodium Carbonate Chemical compound [Na+].[Na+].[O-]C([O-])=O CDBYLPFSWZWCQE-UHFFFAOYSA-L 0.000 description 2
- 238000005868 electrolysis reaction Methods 0.000 description 2
- 238000001914 filtration Methods 0.000 description 2
- 239000002054 inoculum Substances 0.000 description 2
- 230000004048 modification Effects 0.000 description 2
- 238000012986 modification Methods 0.000 description 2
- 230000006911 nucleation Effects 0.000 description 2
- 239000002245 particle Substances 0.000 description 2
- 230000002093 peripheral effect Effects 0.000 description 2
- 239000000126 substance Substances 0.000 description 2
- RYGMFSIKBFXOCR-UHFFFAOYSA-N Copper Chemical compound [Cu] RYGMFSIKBFXOCR-UHFFFAOYSA-N 0.000 description 1
- RTAQQCXQSZGOHL-UHFFFAOYSA-N Titanium Chemical compound [Ti] RTAQQCXQSZGOHL-UHFFFAOYSA-N 0.000 description 1
- 229910052770 Uranium Inorganic materials 0.000 description 1
- HCHKCACWOHOZIP-UHFFFAOYSA-N Zinc Chemical compound [Zn] HCHKCACWOHOZIP-UHFFFAOYSA-N 0.000 description 1
- XFBXDGLHUSUNMG-UHFFFAOYSA-N alumane;hydrate Chemical class O.[AlH3] XFBXDGLHUSUNMG-UHFFFAOYSA-N 0.000 description 1
- RREGISFBPQOLTM-UHFFFAOYSA-N alumane;trihydrate Chemical class O.O.O.[AlH3] RREGISFBPQOLTM-UHFFFAOYSA-N 0.000 description 1
- 230000033228 biological regulation Effects 0.000 description 1
- 238000001354 calcination Methods 0.000 description 1
- 230000001914 calming effect Effects 0.000 description 1
- 230000008859 change Effects 0.000 description 1
- 238000006243 chemical reaction Methods 0.000 description 1
- 238000010276 construction Methods 0.000 description 1
- 238000011109 contamination Methods 0.000 description 1
- 229910052802 copper Inorganic materials 0.000 description 1
- 239000010949 copper Substances 0.000 description 1
- 229910052593 corundum Inorganic materials 0.000 description 1
- 230000007423 decrease Effects 0.000 description 1
- 238000010586 diagram Methods 0.000 description 1
- UOCIZHQMWNPGEN-UHFFFAOYSA-N dialuminum;oxygen(2-);trihydrate Chemical compound O.O.O.[O-2].[O-2].[O-2].[Al+3].[Al+3] UOCIZHQMWNPGEN-UHFFFAOYSA-N 0.000 description 1
- 239000000428 dust Substances 0.000 description 1
- 230000007613 environmental effect Effects 0.000 description 1
- 229910052742 iron Inorganic materials 0.000 description 1
- 238000002156 mixing Methods 0.000 description 1
- 150000004682 monohydrates Chemical class 0.000 description 1
- 239000002244 precipitate Substances 0.000 description 1
- 230000000717 retained effect Effects 0.000 description 1
- 238000004062 sedimentation Methods 0.000 description 1
- 229910000029 sodium carbonate Inorganic materials 0.000 description 1
- 239000007858 starting material Substances 0.000 description 1
- 239000013589 supplement Substances 0.000 description 1
- 230000008719 thickening Effects 0.000 description 1
- 229910052719 titanium Inorganic materials 0.000 description 1
- 239000010936 titanium Substances 0.000 description 1
- 150000004684 trihydrates Chemical class 0.000 description 1
- WFKWXMTUELFFGS-UHFFFAOYSA-N tungsten Chemical compound [W] WFKWXMTUELFFGS-UHFFFAOYSA-N 0.000 description 1
- 229910052721 tungsten Inorganic materials 0.000 description 1
- 239000010937 tungsten Substances 0.000 description 1
- 230000007306 turnover Effects 0.000 description 1
- JFALSRSLKYAFGM-UHFFFAOYSA-N uranium(0) Chemical compound [U] JFALSRSLKYAFGM-UHFFFAOYSA-N 0.000 description 1
- 229910001845 yogo sapphire Inorganic materials 0.000 description 1
- 239000011701 zinc Substances 0.000 description 1
- 229910052725 zinc Inorganic materials 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01F—COMPOUNDS OF THE METALS BERYLLIUM, MAGNESIUM, ALUMINIUM, CALCIUM, STRONTIUM, BARIUM, RADIUM, THORIUM, OR OF THE RARE-EARTH METALS
- C01F7/00—Compounds of aluminium
- C01F7/02—Aluminium oxide; Aluminium hydroxide; Aluminates
- C01F7/04—Preparation of alkali metal aluminates; Aluminium oxide or hydroxide therefrom
- C01F7/14—Aluminium oxide or hydroxide from alkali metal aluminates
- C01F7/144—Aluminium oxide or hydroxide from alkali metal aluminates from aqueous aluminate solutions by precipitation due to cooling, e.g. as part of the Bayer process
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01F—COMPOUNDS OF THE METALS BERYLLIUM, MAGNESIUM, ALUMINIUM, CALCIUM, STRONTIUM, BARIUM, RADIUM, THORIUM, OR OF THE RARE-EARTH METALS
- C01F7/00—Compounds of aluminium
- C01F7/02—Aluminium oxide; Aluminium hydroxide; Aluminates
- C01F7/04—Preparation of alkali metal aluminates; Aluminium oxide or hydroxide therefrom
- C01F7/14—Aluminium oxide or hydroxide from alkali metal aluminates
- C01F7/144—Aluminium oxide or hydroxide from alkali metal aluminates from aqueous aluminate solutions by precipitation due to cooling, e.g. as part of the Bayer process
- C01F7/147—Apparatus for precipitation
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Life Sciences & Earth Sciences (AREA)
- Geology (AREA)
- Inorganic Chemistry (AREA)
- Compounds Of Alkaline-Earth Elements, Aluminum Or Rare-Earth Metals (AREA)
- Mixers Of The Rotary Stirring Type (AREA)
Priority Applications (8)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE19752531646 DE2531646A1 (de) | 1975-07-15 | 1975-07-15 | Verfahren und vorrichtung zur herstellung von tonerde |
| FR7610767A FR2318113A1 (fr) | 1975-07-15 | 1976-04-13 | Procede pour la fabrication d'alumine et dispositif pour sa mise en oeuvre |
| CH465576A CH618948A5 (en, 2012) | 1975-07-15 | 1976-04-13 | |
| AU14056/76A AU504874B2 (en) | 1975-07-15 | 1976-05-18 | Process and apparatus for producing alumina |
| JP51081085A JPS5231999A (en) | 1975-07-15 | 1976-07-09 | Process for preparing aluminium oxide and apparatus therefore |
| CA256,707A CA1098284A (en) | 1975-07-15 | 1976-07-09 | Method of and apparatus for extracting alumina from bauxite |
| SU762379606A SU708988A3 (ru) | 1975-07-15 | 1976-07-13 | Смеситель дл получени глинозема |
| US06/026,061 US4238159A (en) | 1975-07-15 | 1979-04-02 | Apparatus for extracting alumina from bauxite |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE19752531646 DE2531646A1 (de) | 1975-07-15 | 1975-07-15 | Verfahren und vorrichtung zur herstellung von tonerde |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| DE2531646A1 true DE2531646A1 (de) | 1977-02-03 |
Family
ID=5951578
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DE19752531646 Withdrawn DE2531646A1 (de) | 1975-07-15 | 1975-07-15 | Verfahren und vorrichtung zur herstellung von tonerde |
Country Status (8)
| Country | Link |
|---|---|
| US (1) | US4238159A (en, 2012) |
| JP (1) | JPS5231999A (en, 2012) |
| AU (1) | AU504874B2 (en, 2012) |
| CA (1) | CA1098284A (en, 2012) |
| CH (1) | CH618948A5 (en, 2012) |
| DE (1) | DE2531646A1 (en, 2012) |
| FR (1) | FR2318113A1 (en, 2012) |
| SU (1) | SU708988A3 (en, 2012) |
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE2909986A1 (de) * | 1978-07-31 | 1980-02-21 | Eurallumina Spa | Verfahren zur beseitigung von bauxitaufbereitungsabfaellen und aufnahmebassin hierfuer |
| DE3131088A1 (de) * | 1981-08-06 | 1983-02-24 | Vereinigte Aluminium-Werke Ag, 5300 Bonn | Verfahren zur herstellung von aluminiumhydroxid |
| DE3324378A1 (de) * | 1982-07-08 | 1984-01-12 | Aluminium Pechiney, 75008 Paris | Verfahren zur herstellung eines aluminiumtrihydroxids grober korngroesse |
| DE3432473A1 (de) * | 1983-09-05 | 1985-03-21 | Aluminium Pechiney, Paris | Verfahren zur erzeugung eines aluminiumtrihydroxids grober und regelmaessiger korngroesse |
Families Citing this family (36)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS6043468B2 (ja) * | 1978-03-22 | 1985-09-28 | 竹本油脂株式会社 | 繊維処理用油剤 |
| DE2852273C3 (de) * | 1978-12-02 | 1986-07-31 | Vereinigte Aluminium-Werke AG, 1000 Berlin und 5300 Bonn | Schwerentflammbare, Aluminiumtrihydroxid enthaltende Harzmasse auf der Basis polymerer Stoffe |
| JPS5658001A (en) * | 1979-10-18 | 1981-05-20 | Kao Corp | Disposable diaper |
| FI73148C (fi) * | 1982-08-24 | 1987-09-10 | Outokumpu Oy | Saett att dispergera en gas i en vaetska innehaollande fast material och en anordning daerfoer. |
| EP0102403B1 (de) * | 1982-09-02 | 1986-03-05 | Alcoa Chemie GmbH | Verbessertes Verfahren zur Gewinnung von Tonerde |
| JPS6099027A (ja) * | 1983-10-31 | 1985-06-01 | 帝人株式会社 | ポリエステル捲縮繊維及びその製造方法 |
| FR2573414B1 (fr) * | 1984-11-22 | 1989-12-01 | Pechiney Aluminium | Procede de mise en oeuvre d'un amorcage en deux temps pour l'obtention d'alumine a gros grains |
| JPH0763601B2 (ja) * | 1989-01-13 | 1995-07-12 | 鐘淵化学工業株式会社 | 粘性物質の撹拌反応装置 |
| US5167449A (en) * | 1991-12-12 | 1992-12-01 | Corning Incorporated | Paddle shaft assembly with adjustable-pitch paddles |
| DE4429244A1 (de) * | 1994-08-18 | 1996-02-22 | Laeis & Bucher Gmbh | Verfahren und Vorrichtung zur Materialaufbereitung |
| US5738439A (en) * | 1996-11-20 | 1998-04-14 | Flower; Arnold B. | Mixing apparatus |
| FR2771081B1 (fr) | 1997-11-17 | 1999-12-17 | Pechiney Aluminium | Production de trihydrate d'alumine avec controle separe de la teneur en sodium et de la granulometrie |
| RU2147012C1 (ru) * | 1998-04-30 | 2000-03-27 | Акционерное общество "Богословский алюминиевый завод" | Способ нагрева бокситовой пульпы |
| RU2158223C2 (ru) * | 1998-11-06 | 2000-10-27 | ОАО "Богословский алюминиевый завод" | Способ выщелачивания боксита |
| RU2158222C2 (ru) * | 1998-11-06 | 2000-10-27 | ОАО "Богословский алюминиевый завод" | Способ переработки боксита |
| RU2158224C2 (ru) * | 1998-12-01 | 2000-10-27 | ОАО "Богословский алюминиевый завод" | Способ нагрева бокситовой пульпы |
| RU2175640C2 (ru) * | 1999-02-02 | 2001-11-10 | ОАО "Богословский алюминиевый завод" | Способ выщелачивания боксита |
| RU2181695C2 (ru) * | 1999-08-18 | 2002-04-27 | Акционерное общество открытого типа "Всероссийский алюминиево-магниевый институт" | Способ переработки бокситов на глинозем |
| RU2183193C2 (ru) * | 1999-10-11 | 2002-06-10 | Открытое акционерное общество "Алюминий Казахстана" | Способ переработки на глинозем низкокачественного боксита |
| RU2193524C2 (ru) * | 2000-08-08 | 2002-11-27 | Открытое акционерное общество "Богословский алюминиевый завод" | Способ выщелачивания боксита |
| RU2189356C2 (ru) * | 2000-09-29 | 2002-09-20 | ОАО "Богословский алюминиевый завод" | Способ выщелачивания боксита |
| AU2002301811B2 (en) * | 2001-11-07 | 2007-08-23 | Sumitomo Chemical Company, Limited | Aluminum hydroxide aggregated particles, process for producing the same, vessel used therefor, and process for producing aluminum hydroxide powder |
| RU2224716C2 (ru) * | 2001-11-08 | 2004-02-27 | Открытое акционерное общество "Сибирско-Уральская алюминиевая компания" | Способ выщелачивания боксита |
| US6796707B2 (en) * | 2002-02-26 | 2004-09-28 | Spx Corporation | Dual direction mixing impeller and method |
| RU2226175C1 (ru) * | 2002-08-30 | 2004-03-27 | Открытое акционерное общество "Всероссийский алюминиево-магниевый институт" | Аппарат для карбонизации алюминатных растворов |
| RU2302375C2 (ru) * | 2005-05-26 | 2007-07-10 | Закрытое акционерное общество "ЭКОНЭФ" | Способ химической переработки золошлаковых материалов с получением глинозема и кремнезема |
| RU2355637C1 (ru) * | 2007-10-11 | 2009-05-20 | Открытое акционерное общество "РУСАЛ Всероссийский Алюминиево-магниевый Институт" | Карбонизатор алюминатных растворов |
| RU2402423C2 (ru) * | 2009-01-19 | 2010-10-27 | Джемакулов Тимур Заурович | Смесительная машина для производства стеновых изделий |
| CN101704539B (zh) * | 2009-09-11 | 2013-12-25 | 中铝国际技术发展有限公司 | 氧化铝厂母液蒸发的方法及装置 |
| RU2450066C1 (ru) * | 2011-03-11 | 2012-05-10 | Виктор Григорьевич Оголь | Способ переработки нефелиновых руд для получения глинозема и содопродуктов |
| IN2012DE00390A (en, 2012) * | 2012-02-13 | 2015-06-05 | Council Scient Ind Res | |
| CN102764624A (zh) * | 2012-08-08 | 2012-11-07 | 确成硅化学股份有限公司 | 生产二氧化硅的沉淀反应器 |
| CN106573209B (zh) * | 2014-08-13 | 2020-01-03 | 维尔萨利斯股份公司 | 转子以及搅拌设备 |
| RU2572322C1 (ru) * | 2014-10-14 | 2016-01-10 | Общество с ограниченной ответственностью "Объединенная Компания РУСАЛ Инженерно-технологический центр" | Аппарат для сгущения суспензии белитового шлама |
| CN105363403A (zh) * | 2015-12-11 | 2016-03-02 | 茂名市兴煌化工有限公司 | 干式氨化无机矿物粘土的设备及氨化方法 |
| CN112774230A (zh) * | 2021-01-11 | 2021-05-11 | 中铝山东有限公司 | 一种蒸发器机组及蒸发工艺方法 |
Family Cites Families (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| AT265214B (de) * | 1964-12-29 | 1968-10-10 | Erich Karl Todtenhaupt | Vorrichtung zur Herstellung gleichmäßiger Dispersionen |
| US3671019A (en) * | 1970-12-10 | 1972-06-20 | Rietz Mfg Co | Apparatus for material fluffing |
-
1975
- 1975-07-15 DE DE19752531646 patent/DE2531646A1/de not_active Withdrawn
-
1976
- 1976-04-13 CH CH465576A patent/CH618948A5/de not_active IP Right Cessation
- 1976-04-13 FR FR7610767A patent/FR2318113A1/fr active Granted
- 1976-05-18 AU AU14056/76A patent/AU504874B2/en not_active Expired
- 1976-07-09 CA CA256,707A patent/CA1098284A/en not_active Expired
- 1976-07-09 JP JP51081085A patent/JPS5231999A/ja active Pending
- 1976-07-13 SU SU762379606A patent/SU708988A3/ru active
-
1979
- 1979-04-02 US US06/026,061 patent/US4238159A/en not_active Expired - Lifetime
Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE2909986A1 (de) * | 1978-07-31 | 1980-02-21 | Eurallumina Spa | Verfahren zur beseitigung von bauxitaufbereitungsabfaellen und aufnahmebassin hierfuer |
| DE3131088A1 (de) * | 1981-08-06 | 1983-02-24 | Vereinigte Aluminium-Werke Ag, 5300 Bonn | Verfahren zur herstellung von aluminiumhydroxid |
| DE3324378A1 (de) * | 1982-07-08 | 1984-01-12 | Aluminium Pechiney, 75008 Paris | Verfahren zur herstellung eines aluminiumtrihydroxids grober korngroesse |
| DE3432473A1 (de) * | 1983-09-05 | 1985-03-21 | Aluminium Pechiney, Paris | Verfahren zur erzeugung eines aluminiumtrihydroxids grober und regelmaessiger korngroesse |
| DE3432473C3 (de) * | 1983-09-05 | 1998-02-12 | Pechiney Aluminium | Verfahren zur Herstellung eines Aluminiumtrihydroxids grober Kerngröße |
Also Published As
| Publication number | Publication date |
|---|---|
| SU708988A3 (ru) | 1980-01-05 |
| CH618948A5 (en, 2012) | 1980-08-29 |
| FR2318113A1 (fr) | 1977-02-11 |
| US4238159A (en) | 1980-12-09 |
| JPS5231999A (en) | 1977-03-10 |
| FR2318113B1 (en, 2012) | 1981-08-21 |
| AU1405676A (en) | 1977-11-24 |
| AU504874B2 (en) | 1979-11-01 |
| CA1098284A (en) | 1981-03-31 |
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