DE2457218C2 - Verfahren zur Herstellung von pilierter Seife - Google Patents
Verfahren zur Herstellung von pilierter SeifeInfo
- Publication number
- DE2457218C2 DE2457218C2 DE19742457218 DE2457218A DE2457218C2 DE 2457218 C2 DE2457218 C2 DE 2457218C2 DE 19742457218 DE19742457218 DE 19742457218 DE 2457218 A DE2457218 A DE 2457218A DE 2457218 C2 DE2457218 C2 DE 2457218C2
- Authority
- DE
- Germany
- Prior art keywords
- soap
- mixture
- saponification
- bath
- oil
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- 239000000344 soap Substances 0.000 title claims description 97
- 238000000034 method Methods 0.000 title claims description 26
- 238000004519 manufacturing process Methods 0.000 title claims description 10
- 230000008569 process Effects 0.000 title claims description 9
- 239000003921 oil Substances 0.000 claims description 51
- 239000000203 mixture Substances 0.000 claims description 23
- 239000013078 crystal Substances 0.000 claims description 15
- 238000007127 saponification reaction Methods 0.000 claims description 15
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 15
- 235000014113 dietary fatty acids Nutrition 0.000 claims description 11
- 239000000194 fatty acid Substances 0.000 claims description 11
- 229930195729 fatty acid Natural products 0.000 claims description 11
- 150000004665 fatty acids Chemical class 0.000 claims description 11
- POULHZVOKOAJMA-UHFFFAOYSA-N methyl undecanoic acid Natural products CCCCCCCCCCCC(O)=O POULHZVOKOAJMA-UHFFFAOYSA-N 0.000 claims description 10
- HIQIXEFWDLTDED-UHFFFAOYSA-N 4-hydroxy-1-piperidin-4-ylpyrrolidin-2-one Chemical compound O=C1CC(O)CN1C1CCNCC1 HIQIXEFWDLTDED-UHFFFAOYSA-N 0.000 claims description 8
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 claims description 8
- 150000001298 alcohols Chemical class 0.000 claims description 8
- 239000007787 solid Substances 0.000 claims description 8
- 239000005639 Lauric acid Substances 0.000 claims description 6
- 238000001816 cooling Methods 0.000 claims description 5
- 235000021355 Stearic acid Nutrition 0.000 claims description 4
- 235000011187 glycerol Nutrition 0.000 claims description 4
- -1 lauric acid ester Chemical class 0.000 claims description 4
- 239000002480 mineral oil Substances 0.000 claims description 4
- QIQXTHQIDYTFRH-UHFFFAOYSA-N octadecanoic acid Chemical compound CCCCCCCCCCCCCCCCCC(O)=O QIQXTHQIDYTFRH-UHFFFAOYSA-N 0.000 claims description 4
- OQCDKBAXFALNLD-UHFFFAOYSA-N octadecanoic acid Natural products CCCCCCCC(C)CCCCCCCCC(O)=O OQCDKBAXFALNLD-UHFFFAOYSA-N 0.000 claims description 4
- 239000008117 stearic acid Substances 0.000 claims description 4
- IAYPIBMASNFSPL-UHFFFAOYSA-N Ethylene oxide Chemical compound C1CO1 IAYPIBMASNFSPL-UHFFFAOYSA-N 0.000 claims description 3
- 239000004359 castor oil Substances 0.000 claims description 3
- 235000019438 castor oil Nutrition 0.000 claims description 3
- 125000005456 glyceride group Chemical group 0.000 claims description 3
- ZEMPKEQAKRGZGQ-XOQCFJPHSA-N glycerol triricinoleate Natural products CCCCCC[C@@H](O)CC=CCCCCCCCC(=O)OC[C@@H](COC(=O)CCCCCCCC=CC[C@@H](O)CCCCCC)OC(=O)CCCCCCCC=CC[C@H](O)CCCCCC ZEMPKEQAKRGZGQ-XOQCFJPHSA-N 0.000 claims description 3
- 235000019388 lanolin Nutrition 0.000 claims description 3
- 239000007788 liquid Substances 0.000 claims description 3
- IPCSVZSSVZVIGE-UHFFFAOYSA-N n-hexadecanoic acid Natural products CCCCCCCCCCCCCCCC(O)=O IPCSVZSSVZVIGE-UHFFFAOYSA-N 0.000 claims description 3
- 239000001993 wax Substances 0.000 claims description 3
- 239000004166 Lanolin Substances 0.000 claims description 2
- 235000021314 Palmitic acid Nutrition 0.000 claims description 2
- 229940039717 lanolin Drugs 0.000 claims description 2
- WQEPLUUGTLDZJY-UHFFFAOYSA-N n-Pentadecanoic acid Natural products CCCCCCCCCCCCCCC(O)=O WQEPLUUGTLDZJY-UHFFFAOYSA-N 0.000 claims description 2
- 239000003513 alkali Substances 0.000 claims 2
- 235000010446 mineral oil Nutrition 0.000 claims 1
- 239000012071 phase Substances 0.000 description 33
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 15
- 238000002474 experimental method Methods 0.000 description 7
- 150000002148 esters Chemical class 0.000 description 6
- 238000005187 foaming Methods 0.000 description 5
- 238000010521 absorption reaction Methods 0.000 description 4
- 230000000694 effects Effects 0.000 description 4
- 239000004615 ingredient Substances 0.000 description 4
- 239000000463 material Substances 0.000 description 4
- 239000003094 microcapsule Substances 0.000 description 4
- 239000000243 solution Substances 0.000 description 4
- LYCAIKOWRPUZTN-UHFFFAOYSA-N Ethylene glycol Chemical compound OCCO LYCAIKOWRPUZTN-UHFFFAOYSA-N 0.000 description 3
- 239000000654 additive Substances 0.000 description 3
- 239000000975 dye Substances 0.000 description 3
- 238000001125 extrusion Methods 0.000 description 3
- 238000010348 incorporation Methods 0.000 description 3
- 229940105132 myristate Drugs 0.000 description 3
- TUNFSRHWOTWDNC-UHFFFAOYSA-N tetradecanoic acid Chemical compound CCCCCCCCCCCCCC(O)=O TUNFSRHWOTWDNC-UHFFFAOYSA-N 0.000 description 3
- 230000007704 transition Effects 0.000 description 3
- 238000007792 addition Methods 0.000 description 2
- 230000002411 adverse Effects 0.000 description 2
- 230000015572 biosynthetic process Effects 0.000 description 2
- 230000008859 change Effects 0.000 description 2
- 238000006243 chemical reaction Methods 0.000 description 2
- 238000004140 cleaning Methods 0.000 description 2
- 239000002131 composite material Substances 0.000 description 2
- 238000001035 drying Methods 0.000 description 2
- 239000006260 foam Substances 0.000 description 2
- 238000004898 kneading Methods 0.000 description 2
- 235000013575 mashed potatoes Nutrition 0.000 description 2
- 238000002156 mixing Methods 0.000 description 2
- 235000012149 noodles Nutrition 0.000 description 2
- 239000002304 perfume Substances 0.000 description 2
- 230000000704 physical effect Effects 0.000 description 2
- 239000000049 pigment Substances 0.000 description 2
- 239000000126 substance Substances 0.000 description 2
- 230000008961 swelling Effects 0.000 description 2
- 244000215068 Acacia senegal Species 0.000 description 1
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 1
- 108010010803 Gelatin Proteins 0.000 description 1
- 229920000084 Gum arabic Polymers 0.000 description 1
- 235000010489 acacia gum Nutrition 0.000 description 1
- 239000000205 acacia gum Substances 0.000 description 1
- 238000000429 assembly Methods 0.000 description 1
- 230000000712 assembly Effects 0.000 description 1
- 238000003287 bathing Methods 0.000 description 1
- 230000005540 biological transmission Effects 0.000 description 1
- 239000003795 chemical substances by application Substances 0.000 description 1
- 238000005354 coacervation Methods 0.000 description 1
- 229940110456 cocoa butter Drugs 0.000 description 1
- 235000019868 cocoa butter Nutrition 0.000 description 1
- 238000002485 combustion reaction Methods 0.000 description 1
- 239000000470 constituent Substances 0.000 description 1
- 239000002537 cosmetic Substances 0.000 description 1
- 238000001493 electron microscopy Methods 0.000 description 1
- 239000003974 emollient agent Substances 0.000 description 1
- 238000007046 ethoxylation reaction Methods 0.000 description 1
- 235000019197 fats Nutrition 0.000 description 1
- 239000003205 fragrance Substances 0.000 description 1
- 235000021588 free fatty acids Nutrition 0.000 description 1
- 229920000159 gelatin Polymers 0.000 description 1
- 239000008273 gelatin Substances 0.000 description 1
- 235000019322 gelatine Nutrition 0.000 description 1
- 235000011852 gelatine desserts Nutrition 0.000 description 1
- 239000008187 granular material Substances 0.000 description 1
- 230000001771 impaired effect Effects 0.000 description 1
- 230000006872 improvement Effects 0.000 description 1
- 238000011065 in-situ storage Methods 0.000 description 1
- 239000007791 liquid phase Substances 0.000 description 1
- 238000012423 maintenance Methods 0.000 description 1
- 230000007257 malfunction Effects 0.000 description 1
- 239000003605 opacifier Substances 0.000 description 1
- 230000035515 penetration Effects 0.000 description 1
- 238000001556 precipitation Methods 0.000 description 1
- 230000002028 premature Effects 0.000 description 1
- 238000003825 pressing Methods 0.000 description 1
- 150000003138 primary alcohols Chemical class 0.000 description 1
- 238000012545 processing Methods 0.000 description 1
- 230000001681 protective effect Effects 0.000 description 1
- 230000001007 puffing effect Effects 0.000 description 1
- 230000009257 reactivity Effects 0.000 description 1
- 238000007493 shaping process Methods 0.000 description 1
- 239000006104 solid solution Substances 0.000 description 1
- 238000007711 solidification Methods 0.000 description 1
- 230000008023 solidification Effects 0.000 description 1
- 230000002269 spontaneous effect Effects 0.000 description 1
- 238000003756 stirring Methods 0.000 description 1
- 238000006467 substitution reaction Methods 0.000 description 1
- 238000012360 testing method Methods 0.000 description 1
- 230000009466 transformation Effects 0.000 description 1
- 238000009736 wetting Methods 0.000 description 1
- 238000012982 x-ray structure analysis Methods 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D9/00—Compositions of detergents based essentially on soap
- C11D9/04—Compositions of detergents based essentially on soap containing compounding ingredients other than soaps
- C11D9/48—Superfatting agents
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D13/00—Making of soap or soap solutions in general; Apparatus therefor
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D13/00—Making of soap or soap solutions in general; Apparatus therefor
- C11D13/02—Boiling soap; Refining
Landscapes
- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Detergent Compositions (AREA)
- Cosmetics (AREA)
Priority Applications (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| GB2448474A GB1447435A (en) | 1974-06-03 | 1974-06-03 | Soap composition and process of producing such |
| FR7419142A FR2273865A1 (fr) | 1974-06-03 | 1974-06-04 | Composition pour savon et le procede de preparation correspondant |
| DE19742457218 DE2457218C2 (de) | 1974-06-03 | 1974-12-04 | Verfahren zur Herstellung von pilierter Seife |
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| GB2448474A GB1447435A (en) | 1974-06-03 | 1974-06-03 | Soap composition and process of producing such |
| FR7419142A FR2273865A1 (fr) | 1974-06-03 | 1974-06-04 | Composition pour savon et le procede de preparation correspondant |
| DE19742457218 DE2457218C2 (de) | 1974-06-03 | 1974-12-04 | Verfahren zur Herstellung von pilierter Seife |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| DE2457218A1 DE2457218A1 (de) | 1976-06-10 |
| DE2457218C2 true DE2457218C2 (de) | 1982-09-23 |
Family
ID=27186178
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DE19742457218 Expired DE2457218C2 (de) | 1974-06-03 | 1974-12-04 | Verfahren zur Herstellung von pilierter Seife |
Country Status (3)
| Country | Link |
|---|---|
| DE (1) | DE2457218C2 (enExample) |
| FR (1) | FR2273865A1 (enExample) |
| GB (1) | GB1447435A (enExample) |
Families Citing this family (10)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE3272256D1 (en) * | 1981-04-07 | 1986-09-04 | Mitsubishi Chem Ind | Soap composition |
| US4474683A (en) * | 1981-08-10 | 1984-10-02 | Armour-Dial, Inc. | Soap making process |
| US4680132A (en) * | 1982-03-26 | 1987-07-14 | Lever Brothers Company | Processing detergent bars with a cavity transfer mixer to reduce grittiness |
| IN157133B (enExample) * | 1982-03-29 | 1986-01-25 | Lever Hindustan Ltd | |
| PH22031A (en) * | 1982-03-29 | 1988-05-13 | Unilever Nv | Detergent bar processing |
| US4840810A (en) * | 1985-03-27 | 1989-06-20 | Lever Brothers Company | Process for the preparation of an edible fat-containing product |
| US4844928A (en) * | 1985-03-27 | 1989-07-04 | Lever Brothers Company | Process for the preparation of an edible fat-containing product |
| WO1995016022A1 (en) * | 1991-12-04 | 1995-06-15 | Colgate-Palmolive Company | Process for toilet bars and resulting bar |
| US7737097B2 (en) | 2003-06-27 | 2010-06-15 | Lam Research Corporation | Method for removing contamination from a substrate and for making a cleaning solution |
| EP2428557A1 (en) * | 2005-12-30 | 2012-03-14 | LAM Research Corporation | Cleaning solution |
-
1974
- 1974-06-03 GB GB2448474A patent/GB1447435A/en not_active Expired
- 1974-06-04 FR FR7419142A patent/FR2273865A1/fr active Granted
- 1974-12-04 DE DE19742457218 patent/DE2457218C2/de not_active Expired
Non-Patent Citations (1)
| Title |
|---|
| NICHTS-ERMITTELT |
Also Published As
| Publication number | Publication date |
|---|---|
| GB1447435A (en) | 1976-08-25 |
| FR2273865A1 (fr) | 1976-01-02 |
| DE2457218A1 (de) | 1976-06-10 |
| FR2273865B1 (enExample) | 1977-10-14 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| OD | Request for examination | ||
| D2 | Grant after examination | ||
| 8327 | Change in the person/name/address of the patent owner |
Owner name: FERRARA, PETER J., CORNWALL, N.Y., US |
|
| 8381 | Inventor (new situation) |
Free format text: FERRARA, PETER J., CORNWALL, N.Y., US DALBY, GASTON, ST. GERMAIN DU SALEMBRE, NEUVIC-SUR-L ISLE, FRBARNES JUN., CLARENCE A. GORDON, ROY, NEW YORK, N.Y., US |
|
| 8339 | Ceased/non-payment of the annual fee |