DE2441447C3 - Verfahren zur adsorptiven Trennung von neben Stickstoff wenigstens Sauerstoff enthaltenden Gasgemischen - Google Patents

Verfahren zur adsorptiven Trennung von neben Stickstoff wenigstens Sauerstoff enthaltenden Gasgemischen

Info

Publication number
DE2441447C3
DE2441447C3 DE2441447A DE2441447A DE2441447C3 DE 2441447 C3 DE2441447 C3 DE 2441447C3 DE 2441447 A DE2441447 A DE 2441447A DE 2441447 A DE2441447 A DE 2441447A DE 2441447 C3 DE2441447 C3 DE 2441447C3
Authority
DE
Germany
Prior art keywords
nitrogen
gas
molecular sieve
adsorber
stage
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired
Application number
DE2441447A
Other languages
German (de)
English (en)
Other versions
DE2441447A1 (de
DE2441447B2 (de
Inventor
Hugo Horbel
Harald Prof. Dipl.-Chem. Dr. Juentgen
Karl Dipl.- Ing. Dr. Knoblauch
Werner 4330 Muelheim Koerbaecher
Heinrich Dipl.- Chem. Dr. 4300 Essen Muenzner
Werner Prof. Dr. 4640 Wattenscheid Peters
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Bergwerksverband GmbH
Original Assignee
Bergwerksverband GmbH
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Bergwerksverband GmbH filed Critical Bergwerksverband GmbH
Priority to DE2441447A priority Critical patent/DE2441447C3/de
Priority to IT50220/75A priority patent/IT1040717B/it
Priority to BE158689A priority patent/BE831821A/xx
Priority to ZA00755356A priority patent/ZA755356B/xx
Priority to CA234,075A priority patent/CA1084421A/en
Priority to BR7505509*A priority patent/BR7505509A/pt
Priority to AU84368/75A priority patent/AU503999B2/en
Priority to JP50104190A priority patent/JPS5150298A/ja
Priority to NLAANVRAGE7510234,A priority patent/NL181559C/xx
Priority to GB35833/75A priority patent/GB1480866A/en
Priority to FR7526653A priority patent/FR2283094A1/fr
Publication of DE2441447A1 publication Critical patent/DE2441447A1/de
Publication of DE2441447B2 publication Critical patent/DE2441447B2/de
Application granted granted Critical
Publication of DE2441447C3 publication Critical patent/DE2441447C3/de
Expired legal-status Critical Current

Links

Classifications

    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D53/00—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols
    • B01D53/02—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols by adsorption, e.g. preparative gas chromatography
    • B01D53/04—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols by adsorption, e.g. preparative gas chromatography with stationary adsorbents
    • B01D53/047—Pressure swing adsorption
    • B01D53/0476—Vacuum pressure swing adsorption
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D53/00—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols
    • B01D53/02—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols by adsorption, e.g. preparative gas chromatography
    • B01D53/04—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols by adsorption, e.g. preparative gas chromatography with stationary adsorbents
    • B01D53/047—Pressure swing adsorption
    • B01D53/0473—Rapid pressure swing adsorption
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B21/00—Nitrogen; Compounds thereof
    • C01B21/04—Purification or separation of nitrogen
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D2253/00—Adsorbents used in seperation treatment of gases and vapours
    • B01D2253/10—Inorganic adsorbents
    • B01D2253/116—Molecular sieves other than zeolites
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D2253/00—Adsorbents used in seperation treatment of gases and vapours
    • B01D2253/25—Coated, impregnated or composite adsorbents
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D2256/00—Main component in the product gas stream after treatment
    • B01D2256/10—Nitrogen
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D2257/00—Components to be removed
    • B01D2257/10—Single element gases other than halogens
    • B01D2257/104—Oxygen
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D2257/00—Components to be removed
    • B01D2257/50—Carbon oxides
    • B01D2257/502—Carbon monoxide
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D2257/00—Components to be removed
    • B01D2257/80—Water
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D2259/00—Type of treatment
    • B01D2259/40—Further details for adsorption processes and devices
    • B01D2259/40001—Methods relating to additional, e.g. intermediate, treatment of process gas
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D2259/00—Type of treatment
    • B01D2259/40—Further details for adsorption processes and devices
    • B01D2259/40011—Methods relating to the process cycle in pressure or temperature swing adsorption
    • B01D2259/40035—Equalization
    • B01D2259/40037—Equalization with two sub-steps
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D2259/00—Type of treatment
    • B01D2259/40—Further details for adsorption processes and devices
    • B01D2259/40011—Methods relating to the process cycle in pressure or temperature swing adsorption
    • B01D2259/40058—Number of sequence steps, including sub-steps, per cycle
    • B01D2259/40062—Four
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D2259/00—Type of treatment
    • B01D2259/40—Further details for adsorption processes and devices
    • B01D2259/40011—Methods relating to the process cycle in pressure or temperature swing adsorption
    • B01D2259/40058—Number of sequence steps, including sub-steps, per cycle
    • B01D2259/40064—Five
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D2259/00—Type of treatment
    • B01D2259/40—Further details for adsorption processes and devices
    • B01D2259/402—Further details for adsorption processes and devices using two beds
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D53/00—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols
    • B01D53/26—Drying gases or vapours
    • B01D53/261—Drying gases or vapours by adsorption

Landscapes

  • Chemical & Material Sciences (AREA)
  • Analytical Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • General Chemical & Material Sciences (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Chemistry (AREA)
  • Inorganic Chemistry (AREA)
  • Separation Of Gases By Adsorption (AREA)
  • Oxygen, Ozone, And Oxides In General (AREA)
DE2441447A 1974-08-29 1974-08-29 Verfahren zur adsorptiven Trennung von neben Stickstoff wenigstens Sauerstoff enthaltenden Gasgemischen Expired DE2441447C3 (de)

Priority Applications (11)

Application Number Priority Date Filing Date Title
DE2441447A DE2441447C3 (de) 1974-08-29 1974-08-29 Verfahren zur adsorptiven Trennung von neben Stickstoff wenigstens Sauerstoff enthaltenden Gasgemischen
IT50220/75A IT1040717B (it) 1974-08-29 1975-06-25 Procedimento per la produzione di gas ricchi d azoto da gas contenenti oltre ad azoto almento ossigeno come per esempio l aria
BE158689A BE831821A (fr) 1974-08-29 1975-07-28 Procede pour l'obtention de gaz riches en azote
ZA00755356A ZA755356B (en) 1974-08-29 1975-08-21 Process for obtaining nitrogen-rich gases, such as for example air, which in addition to n, contain at least o2
CA234,075A CA1084421A (en) 1974-08-29 1975-08-25 Recovery of gases from gaseous mixtures
AU84368/75A AU503999B2 (en) 1974-08-29 1975-08-28 N2-enrichment/adsorption
BR7505509*A BR7505509A (pt) 1974-08-29 1975-08-28 Processo para a obtencao de gases ricos em nitrogenio a partir de gases contendo-alem de n2-pelo menos o2,como por exemplo,ar
JP50104190A JPS5150298A (en) 1974-08-29 1975-08-29 Chitsusofukagasuno seiho
NLAANVRAGE7510234,A NL181559C (nl) 1974-08-29 1975-08-29 Werkwijze voor het adsorptief scheiden van gasmengsels die naast stikstof ten minste zuurstof bevatten.
GB35833/75A GB1480866A (en) 1974-08-29 1975-08-29 Process for obtaining nitrogen-rich gases from gases containing oxygen and nitrogen
FR7526653A FR2283094A1 (fr) 1974-08-29 1975-08-29 Procede de preparation de gaz riches en azote a partir de gaz contenant, outre l'azote, au moins de l'oxygene, tels que l'air

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
DE2441447A DE2441447C3 (de) 1974-08-29 1974-08-29 Verfahren zur adsorptiven Trennung von neben Stickstoff wenigstens Sauerstoff enthaltenden Gasgemischen

Publications (3)

Publication Number Publication Date
DE2441447A1 DE2441447A1 (de) 1976-03-18
DE2441447B2 DE2441447B2 (de) 1979-09-06
DE2441447C3 true DE2441447C3 (de) 1980-05-22

Family

ID=5924411

Family Applications (1)

Application Number Title Priority Date Filing Date
DE2441447A Expired DE2441447C3 (de) 1974-08-29 1974-08-29 Verfahren zur adsorptiven Trennung von neben Stickstoff wenigstens Sauerstoff enthaltenden Gasgemischen

Country Status (11)

Country Link
JP (1) JPS5150298A (enExample)
AU (1) AU503999B2 (enExample)
BE (1) BE831821A (enExample)
BR (1) BR7505509A (enExample)
CA (1) CA1084421A (enExample)
DE (1) DE2441447C3 (enExample)
FR (1) FR2283094A1 (enExample)
GB (1) GB1480866A (enExample)
IT (1) IT1040717B (enExample)
NL (1) NL181559C (enExample)
ZA (1) ZA755356B (enExample)

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP0082948A1 (de) * 1981-11-21 1983-07-06 Leybold-Heraeus GmbH Verfahren zum Betrieb einer Druckwechselanlage und nach diesem Verfahren arbeitende Druckwechselanlage
EP0075663A3 (en) * 1981-09-22 1983-10-26 Leybold-Heraeus Gmbh Process and apparatus for producing highly pure nitrogen

Families Citing this family (12)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE2652486C2 (de) * 1976-11-18 1987-01-08 Bergwerksverband Gmbh, 4300 Essen Verfahren zur Gewinnung von stickstoffreichen Gasen aus neben N↓2↓ wenigstens O↓2↓ enthaltenden Gasen, wie z.B. Luft
US4256469A (en) * 1978-11-06 1981-03-17 Linde Aktiengesellschaft Repressurization technique for pressure swing adsorption
DE2923325A1 (de) * 1979-06-08 1980-12-11 Linde Ag Zyklisches adsorptionsverfahren zum zerlegen eines gasgemisches
DE2932333C2 (de) * 1979-08-09 1986-08-07 Bergwerksverband Gmbh, 4300 Essen Verfahren zur adsorptiven Trennung von neben Stickstoff wenigstens Sauerstoff enthaltenden Gasgemischen
ZA811931B (en) 1980-03-31 1982-05-26 African Oxygen Ltd Process and apparatus for the separation of gaseous mixture
JPS5745320A (en) * 1980-08-31 1982-03-15 Ishikawaken Method and equipment of production for concentration- adjustable oxygen-enriched air
GB2086258A (en) * 1980-10-30 1982-05-12 Boc Ltd Process and apparatus for separation of a gaseous mixture
DE3132572A1 (de) * 1981-08-18 1983-03-10 Linde Ag, 6200 Wiesbaden Verfahren zur adsorptiven zerlegung eines gasgemisches
JPS607920A (ja) * 1983-06-29 1985-01-16 Hitachi Ltd 非凝縮性混合ガスの分離方法
GB2152834B (en) * 1983-07-23 1987-01-28 Derek Edward Ward Producing nitrogen from air
JP2634015B2 (ja) * 1993-02-25 1997-07-23 東洋エンジニアリング株式会社 アンモニア分離用の圧力スイング分離装置およびアンモニア分離方法
JP5902920B2 (ja) 2011-11-10 2016-04-13 大陽日酸株式会社 窒素ガス製造方法、ガス分離方法および窒素ガス製造装置

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP0075663A3 (en) * 1981-09-22 1983-10-26 Leybold-Heraeus Gmbh Process and apparatus for producing highly pure nitrogen
EP0082948A1 (de) * 1981-11-21 1983-07-06 Leybold-Heraeus GmbH Verfahren zum Betrieb einer Druckwechselanlage und nach diesem Verfahren arbeitende Druckwechselanlage

Also Published As

Publication number Publication date
FR2283094A1 (fr) 1976-03-26
ZA755356B (en) 1976-07-28
FR2283094B1 (enExample) 1980-04-25
JPS5150298A (en) 1976-05-01
AU8436875A (en) 1977-03-03
BE831821A (fr) 1976-01-28
BR7505509A (pt) 1976-08-03
NL181559B (nl) 1987-04-16
DE2441447A1 (de) 1976-03-18
GB1480866A (en) 1977-07-27
DE2441447B2 (de) 1979-09-06
IT1040717B (it) 1979-12-20
NL7510234A (nl) 1976-03-02
JPS5417595B2 (enExample) 1979-06-30
CA1084421A (en) 1980-08-26
NL181559C (nl) 1987-09-16
AU503999B2 (en) 1979-09-27

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Legal Events

Date Code Title Description
C3 Grant after two publication steps (3rd publication)