DE2403427A1 - Verfahren zur herstellung von pesticiden praeparaten - Google Patents
Verfahren zur herstellung von pesticiden praeparatenInfo
- Publication number
- DE2403427A1 DE2403427A1 DE2403427A DE2403427A DE2403427A1 DE 2403427 A1 DE2403427 A1 DE 2403427A1 DE 2403427 A DE2403427 A DE 2403427A DE 2403427 A DE2403427 A DE 2403427A DE 2403427 A1 DE2403427 A1 DE 2403427A1
- Authority
- DE
- Germany
- Prior art keywords
- water
- mixture
- granules
- pesticide
- preparations
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Withdrawn
Links
- 239000000575 pesticide Substances 0.000 title claims description 31
- 238000002360 preparation method Methods 0.000 title claims description 27
- 238000000034 method Methods 0.000 title claims description 24
- 238000004519 manufacturing process Methods 0.000 title claims description 14
- 239000000203 mixture Substances 0.000 claims description 40
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 33
- 239000002245 particle Substances 0.000 claims description 17
- 239000008187 granular material Substances 0.000 claims description 16
- 150000003839 salts Chemical class 0.000 claims description 13
- 239000002270 dispersing agent Substances 0.000 claims description 10
- 239000007787 solid Substances 0.000 claims description 8
- 239000007884 disintegrant Substances 0.000 claims description 7
- 230000007812 deficiency Effects 0.000 claims description 2
- 238000007873 sieving Methods 0.000 claims description 2
- 239000004562 water dispersible granule Substances 0.000 claims 1
- 239000000047 product Substances 0.000 description 20
- 239000000126 substance Substances 0.000 description 11
- 238000001125 extrusion Methods 0.000 description 10
- VMHLLURERBWHNL-UHFFFAOYSA-M Sodium acetate Chemical compound [Na+].CC([O-])=O VMHLLURERBWHNL-UHFFFAOYSA-M 0.000 description 9
- 239000004615 ingredient Substances 0.000 description 9
- 235000017281 sodium acetate Nutrition 0.000 description 8
- 239000001632 sodium acetate Substances 0.000 description 8
- -1 Polyfon H Chemical class 0.000 description 7
- WSFSSNUMVMOOMR-UHFFFAOYSA-N Formaldehyde Chemical compound O=C WSFSSNUMVMOOMR-UHFFFAOYSA-N 0.000 description 6
- CSNNHWWHGAXBCP-UHFFFAOYSA-L Magnesium sulfate Chemical compound [Mg+2].[O-][S+2]([O-])([O-])[O-] CSNNHWWHGAXBCP-UHFFFAOYSA-L 0.000 description 6
- 238000001035 drying Methods 0.000 description 6
- 230000002363 herbicidal effect Effects 0.000 description 6
- 239000004094 surface-active agent Substances 0.000 description 6
- 239000000463 material Substances 0.000 description 5
- 239000000843 powder Substances 0.000 description 5
- 239000013049 sediment Substances 0.000 description 5
- 239000000080 wetting agent Substances 0.000 description 5
- UIIMBOGNXHQVGW-UHFFFAOYSA-M Sodium bicarbonate Chemical compound [Na+].OC([O-])=O UIIMBOGNXHQVGW-UHFFFAOYSA-M 0.000 description 4
- 239000004480 active ingredient Substances 0.000 description 4
- 239000004009 herbicide Substances 0.000 description 4
- 230000000717 retained effect Effects 0.000 description 4
- ODCWYMIRDDJXKW-UHFFFAOYSA-N simazine Chemical compound CCNC1=NC(Cl)=NC(NCC)=N1 ODCWYMIRDDJXKW-UHFFFAOYSA-N 0.000 description 4
- LDVVMCZRFWMZSG-OLQVQODUSA-N (3ar,7as)-2-(trichloromethylsulfanyl)-3a,4,7,7a-tetrahydroisoindole-1,3-dione Chemical compound C1C=CC[C@H]2C(=O)N(SC(Cl)(Cl)Cl)C(=O)[C@H]21 LDVVMCZRFWMZSG-OLQVQODUSA-N 0.000 description 3
- ZRGHYHHYHYAJBT-UHFFFAOYSA-N 4-[(2-chlorophenyl)diazenyl]-3-methyl-2H-1,2-oxazol-5-one Chemical compound ClC1=C(C=CC=C1)N=NC1=C(NOC1=O)C ZRGHYHHYHYAJBT-UHFFFAOYSA-N 0.000 description 3
- 239000005745 Captan Substances 0.000 description 3
- 239000005923 Pirimicarb Substances 0.000 description 3
- PMZURENOXWZQFD-UHFFFAOYSA-L Sodium Sulfate Chemical compound [Na+].[Na+].[O-]S([O-])(=O)=O PMZURENOXWZQFD-UHFFFAOYSA-L 0.000 description 3
- 229940117949 captan Drugs 0.000 description 3
- KRKNYBCHXYNGOX-UHFFFAOYSA-N citric acid Chemical compound OC(=O)CC(O)(C(O)=O)CC(O)=O KRKNYBCHXYNGOX-UHFFFAOYSA-N 0.000 description 3
- 239000006185 dispersion Substances 0.000 description 3
- 239000012530 fluid Substances 0.000 description 3
- 229910052943 magnesium sulfate Inorganic materials 0.000 description 3
- 235000019341 magnesium sulphate Nutrition 0.000 description 3
- 238000002156 mixing Methods 0.000 description 3
- FIKAKWIAUPDISJ-UHFFFAOYSA-L paraquat dichloride Chemical compound [Cl-].[Cl-].C1=C[N+](C)=CC=C1C1=CC=[N+](C)C=C1 FIKAKWIAUPDISJ-UHFFFAOYSA-L 0.000 description 3
- YFGYUFNIOHWBOB-UHFFFAOYSA-N pirimicarb Chemical compound CN(C)C(=O)OC1=NC(N(C)C)=NC(C)=C1C YFGYUFNIOHWBOB-UHFFFAOYSA-N 0.000 description 3
- 229910052938 sodium sulfate Inorganic materials 0.000 description 3
- 235000011152 sodium sulphate Nutrition 0.000 description 3
- 239000000454 talc Substances 0.000 description 3
- 229910052623 talc Inorganic materials 0.000 description 3
- BMPXDMCZKAPJDC-UHFFFAOYSA-N 3-methyl-2h-1,2-oxazol-5-one Chemical compound CC1=CC(=O)ON1 BMPXDMCZKAPJDC-UHFFFAOYSA-N 0.000 description 2
- PAYRUJLWNCNPSJ-UHFFFAOYSA-N Aniline Chemical class NC1=CC=CC=C1 PAYRUJLWNCNPSJ-UHFFFAOYSA-N 0.000 description 2
- CDBYLPFSWZWCQE-UHFFFAOYSA-L Sodium Carbonate Chemical compound [Na+].[Na+].[O-]C([O-])=O CDBYLPFSWZWCQE-UHFFFAOYSA-L 0.000 description 2
- XSQUKJJJFZCRTK-UHFFFAOYSA-N Urea Chemical compound NC(N)=O XSQUKJJJFZCRTK-UHFFFAOYSA-N 0.000 description 2
- 239000004202 carbamide Substances 0.000 description 2
- 238000006243 chemical reaction Methods 0.000 description 2
- 239000004927 clay Substances 0.000 description 2
- 239000007859 condensation product Substances 0.000 description 2
- 230000006735 deficit Effects 0.000 description 2
- 239000000428 dust Substances 0.000 description 2
- 239000012065 filter cake Substances 0.000 description 2
- 239000007788 liquid Substances 0.000 description 2
- INFDPOAKFNIJBF-UHFFFAOYSA-N paraquat Chemical compound C1=C[N+](C)=CC=C1C1=CC=[N+](C)C=C1 INFDPOAKFNIJBF-UHFFFAOYSA-N 0.000 description 2
- 230000000361 pesticidal effect Effects 0.000 description 2
- 229910000030 sodium bicarbonate Inorganic materials 0.000 description 2
- 235000017557 sodium bicarbonate Nutrition 0.000 description 2
- HLHUAEFBYPEEJL-UHFFFAOYSA-N (2-chlorophenyl)azaniumylideneazanide Chemical compound [N]Nc1ccccc1Cl HLHUAEFBYPEEJL-UHFFFAOYSA-N 0.000 description 1
- FIDRAVVQGKNYQK-UHFFFAOYSA-N 1,2,3,4-tetrahydrotriazine Chemical compound C1NNNC=C1 FIDRAVVQGKNYQK-UHFFFAOYSA-N 0.000 description 1
- DNCYBUMDUBHIJZ-UHFFFAOYSA-N 1h-pyrimidin-6-one Chemical compound O=C1C=CN=CN1 DNCYBUMDUBHIJZ-UHFFFAOYSA-N 0.000 description 1
- WBIQQQGBSDOWNP-UHFFFAOYSA-N 2-dodecylbenzenesulfonic acid Chemical class CCCCCCCCCCCCC1=CC=CC=C1S(O)(=O)=O WBIQQQGBSDOWNP-UHFFFAOYSA-N 0.000 description 1
- XMTQQYYKAHVGBJ-UHFFFAOYSA-N 3-(3,4-DICHLOROPHENYL)-1,1-DIMETHYLUREA Chemical compound CN(C)C(=O)NC1=CC=C(Cl)C(Cl)=C1 XMTQQYYKAHVGBJ-UHFFFAOYSA-N 0.000 description 1
- CIFFBTOJCKSRJY-UHFFFAOYSA-N 3α,4,7,7α-tetrahydro-1h-isoindole-1,3(2h)-dione Chemical compound C1C=CCC2C(=O)NC(=O)C21 CIFFBTOJCKSRJY-UHFFFAOYSA-N 0.000 description 1
- UJVMVEZTSSMXAC-UHFFFAOYSA-N 4-[(3-chlorophenyl)diazenyl]-3-methyl-2H-1,2-oxazol-5-one Chemical compound ClC=1C=C(C=CC=1)N=NC1=C(NOC1=O)C UJVMVEZTSSMXAC-UHFFFAOYSA-N 0.000 description 1
- LZZYPRNAOMGNLH-UHFFFAOYSA-M Cetrimonium bromide Chemical compound [Br-].CCCCCCCCCCCCCCCC[N+](C)(C)C LZZYPRNAOMGNLH-UHFFFAOYSA-M 0.000 description 1
- 239000005630 Diquat Substances 0.000 description 1
- 239000005510 Diuron Substances 0.000 description 1
- IAYPIBMASNFSPL-UHFFFAOYSA-N Ethylene oxide Chemical compound C1CO1 IAYPIBMASNFSPL-UHFFFAOYSA-N 0.000 description 1
- 229920001732 Lignosulfonate Polymers 0.000 description 1
- 230000000895 acaricidal effect Effects 0.000 description 1
- 239000000642 acaricide Substances 0.000 description 1
- 239000002253 acid Substances 0.000 description 1
- HZVVJJIYJKGMFL-UHFFFAOYSA-N almasilate Chemical compound O.[Mg+2].[Al+3].[Al+3].O[Si](O)=O.O[Si](O)=O HZVVJJIYJKGMFL-UHFFFAOYSA-N 0.000 description 1
- 150000001413 amino acids Chemical class 0.000 description 1
- 238000004458 analytical method Methods 0.000 description 1
- 230000000844 anti-bacterial effect Effects 0.000 description 1
- 239000003443 antiviral agent Substances 0.000 description 1
- 239000007864 aqueous solution Substances 0.000 description 1
- 239000007900 aqueous suspension Substances 0.000 description 1
- MXWJVTOOROXGIU-UHFFFAOYSA-N atrazine Chemical compound CCNC1=NC(Cl)=NC(NC(C)C)=N1 MXWJVTOOROXGIU-UHFFFAOYSA-N 0.000 description 1
- 239000003899 bactericide agent Substances 0.000 description 1
- SRSXLGNVWSONIS-UHFFFAOYSA-N benzenesulfonic acid Chemical class OS(=O)(=O)C1=CC=CC=C1 SRSXLGNVWSONIS-UHFFFAOYSA-N 0.000 description 1
- 150000001768 cations Chemical class 0.000 description 1
- 235000015165 citric acid Nutrition 0.000 description 1
- 239000012141 concentrate Substances 0.000 description 1
- 238000002425 crystallisation Methods 0.000 description 1
- 230000008025 crystallization Effects 0.000 description 1
- 238000010790 dilution Methods 0.000 description 1
- 239000012895 dilution Substances 0.000 description 1
- SYJFEGQWDCRVNX-UHFFFAOYSA-N diquat Chemical class C1=CC=[N+]2CC[N+]3=CC=CC=C3C2=C1 SYJFEGQWDCRVNX-UHFFFAOYSA-N 0.000 description 1
- YDEXUEFDPVHGHE-GGMCWBHBSA-L disodium;(2r)-3-(2-hydroxy-3-methoxyphenyl)-2-[2-methoxy-4-(3-sulfonatopropyl)phenoxy]propane-1-sulfonate Chemical compound [Na+].[Na+].COC1=CC=CC(C[C@H](CS([O-])(=O)=O)OC=2C(=CC(CCCS([O-])(=O)=O)=CC=2)OC)=C1O YDEXUEFDPVHGHE-GGMCWBHBSA-L 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- BBXXLROWFHWFQY-UHFFFAOYSA-N ethirimol Chemical compound CCCCC1=C(C)NC(NCC)=NC1=O BBXXLROWFHWFQY-UHFFFAOYSA-N 0.000 description 1
- 125000000031 ethylamino group Chemical group [H]C([H])([H])C([H])([H])N([H])[*] 0.000 description 1
- 239000000945 filler Substances 0.000 description 1
- 230000000855 fungicidal effect Effects 0.000 description 1
- 239000000417 fungicide Substances 0.000 description 1
- 150000004820 halides Chemical class 0.000 description 1
- 239000008233 hard water Substances 0.000 description 1
- 238000002347 injection Methods 0.000 description 1
- 239000007924 injection Substances 0.000 description 1
- 239000002917 insecticide Substances 0.000 description 1
- 239000003607 modifier Substances 0.000 description 1
- 239000003750 molluscacide Substances 0.000 description 1
- 230000002013 molluscicidal effect Effects 0.000 description 1
- 150000002790 naphthalenes Chemical class 0.000 description 1
- 150000002989 phenols Chemical class 0.000 description 1
- 230000008635 plant growth Effects 0.000 description 1
- 238000007747 plating Methods 0.000 description 1
- 238000005029 sieve analysis Methods 0.000 description 1
- 239000010802 sludge Substances 0.000 description 1
- 229910000029 sodium carbonate Inorganic materials 0.000 description 1
- 239000000243 solution Substances 0.000 description 1
- 238000001694 spray drying Methods 0.000 description 1
- 238000003756 stirring Methods 0.000 description 1
- 150000003871 sulfonates Chemical class 0.000 description 1
- 239000000725 suspension Substances 0.000 description 1
- 238000009489 vacuum treatment Methods 0.000 description 1
- 238000005406 washing Methods 0.000 description 1
- 238000009736 wetting Methods 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N25/00—Biocides, pest repellants or attractants, or plant growth regulators, characterised by their forms, or by their non-active ingredients or by their methods of application, e.g. seed treatment or sequential application; Substances for reducing the noxious effect of the active ingredients to organisms other than pests
- A01N25/12—Powders or granules
- A01N25/14—Powders or granules wettable
Landscapes
- Life Sciences & Earth Sciences (AREA)
- General Health & Medical Sciences (AREA)
- Health & Medical Sciences (AREA)
- Toxicology (AREA)
- Pest Control & Pesticides (AREA)
- Plant Pathology (AREA)
- Agronomy & Crop Science (AREA)
- Engineering & Computer Science (AREA)
- Dentistry (AREA)
- Wood Science & Technology (AREA)
- Zoology (AREA)
- Environmental Sciences (AREA)
- Agricultural Chemicals And Associated Chemicals (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| GB438873*[A GB1433882A (en) | 1973-01-29 | 1973-01-29 | Pesticidal compositions |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| DE2403427A1 true DE2403427A1 (de) | 1974-08-01 |
Family
ID=9776228
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DE2403427A Withdrawn DE2403427A1 (de) | 1973-01-29 | 1974-01-24 | Verfahren zur herstellung von pesticiden praeparaten |
Country Status (14)
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2000042846A1 (en) * | 1999-01-22 | 2000-07-27 | Agform Limited | Process for producing granules |
Families Citing this family (14)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| GB1555489A (en) * | 1975-06-16 | 1979-11-14 | Ici Ltd | Process for preparing a granular herbicidal composition |
| JPS5948401A (ja) * | 1982-09-10 | 1984-03-19 | Kyushu Sankyo Kk | 崩壊分散性の良好な農薬粒剤 |
| JPS59193801A (ja) * | 1983-04-16 | 1984-11-02 | Mikasa Kagaku Kogyo Kk | 湿潤調整性農薬又は防疫用粉粒錠剤 |
| JPH0720842B2 (ja) * | 1986-03-12 | 1995-03-08 | 花王株式会社 | 顆粒状殺生剤組成物 |
| US5443764A (en) * | 1987-07-01 | 1995-08-22 | Ici Australia Operations Propietary Limited | Water-dispersible granules |
| GB8811570D0 (en) * | 1988-05-16 | 1988-06-22 | Allied Colloids Ltd | Pesticide compositions |
| CA2033592A1 (en) * | 1990-01-12 | 1991-07-13 | Richard Martin Jacobson | Bisphosphoryl hydrazines and their use as pesticides |
| CA2054054C (en) * | 1990-10-31 | 2002-11-26 | Richard David Houghton | Propanil dispersible granule formulation |
| US5714439A (en) * | 1990-10-31 | 1998-02-03 | Rohm And Haas Company | Propanil dispersible granule |
| CA2062099A1 (en) * | 1991-03-11 | 1992-09-12 | Christine Mary Cayer | Oxyfluorfen dispersible granule formulation |
| EP0623281A1 (en) * | 1993-04-28 | 1994-11-09 | American Cyanamid Company | Herbicidal extruded granular compositions |
| JP2002534514A (ja) | 1999-01-14 | 2002-10-15 | モンサント テクノロジー エルエルシー | 除草活性を有する新規トリアゾールスルホン |
| US6734142B2 (en) | 2001-04-23 | 2004-05-11 | Monsanto Technology Llc | Ammonium glyphosate compositions and process for their preparation |
| GB0413209D0 (en) * | 2004-06-14 | 2004-07-14 | Agform Ltd | Chemical composition |
Family Cites Families (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| FR843357A (fr) * | 1938-03-05 | 1939-07-03 | Cie De Traitements Chimiques E | Produits destinés à la lutte contre les parasites des végétaux et procédé de fabrication de ces produits |
| GB1022164A (en) * | 1962-07-31 | 1966-03-09 | Shell Res Ltd | Manufacture of herbicidally active granules |
| IL31939A0 (en) * | 1968-04-03 | 1969-06-25 | Diamond Shamrock Corp | Granular pesticidal compositions |
| FR1569126A (enrdf_load_stackoverflow) * | 1968-04-19 | 1969-05-30 | ||
| DE1812574A1 (de) * | 1968-12-04 | 1970-06-11 | Riedel De Haen Ag | Verfahren zur Herstellung biozider Granulate |
-
0
- CA CA191,014A patent/CA1022848A/en not_active Expired
-
1973
- 1973-01-29 GB GB438873*[A patent/GB1433882A/en not_active Expired
-
1974
- 1974-01-14 ZA ZA740244A patent/ZA74244B/xx unknown
- 1974-01-20 IL IL44024A patent/IL44024A/en unknown
- 1974-01-22 BE BE140076A patent/BE810041A/xx unknown
- 1974-01-23 IT IT19713/74A patent/IT1014536B/it active
- 1974-01-24 DE DE2403427A patent/DE2403427A1/de not_active Withdrawn
- 1974-01-28 CH CH111474A patent/CH581427A5/xx not_active IP Right Cessation
- 1974-01-28 FR FR7402761A patent/FR2215171B1/fr not_active Expired
- 1974-01-28 NL NL7401110A patent/NL7401110A/xx not_active Application Discontinuation
- 1974-01-28 JP JP49011087A patent/JPS49108251A/ja active Pending
- 1974-01-29 BR BR613/74A patent/BR7400613D0/pt unknown
- 1974-01-29 CS CS74592A patent/CS208694B2/cs unknown
- 1974-01-29 ES ES422710A patent/ES422710A1/es not_active Expired
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2000042846A1 (en) * | 1999-01-22 | 2000-07-27 | Agform Limited | Process for producing granules |
| US6893589B1 (en) | 1999-01-22 | 2005-05-17 | Agform Limited | Process for producing granules |
Also Published As
| Publication number | Publication date |
|---|---|
| IL44024A (en) | 1976-07-30 |
| CH581427A5 (enrdf_load_stackoverflow) | 1976-11-15 |
| CA1022848A (en) | 1977-12-20 |
| ES422710A1 (es) | 1976-04-16 |
| FR2215171B1 (enrdf_load_stackoverflow) | 1977-06-10 |
| ZA74244B (en) | 1974-11-27 |
| BE810041A (fr) | 1974-07-22 |
| BR7400613D0 (pt) | 1974-08-22 |
| AU6464574A (en) | 1975-07-24 |
| FR2215171A1 (enrdf_load_stackoverflow) | 1974-08-23 |
| GB1433882A (en) | 1976-04-28 |
| IL44024A0 (en) | 1974-05-16 |
| IT1014536B (it) | 1977-04-30 |
| JPS49108251A (enrdf_load_stackoverflow) | 1974-10-15 |
| NL7401110A (enrdf_load_stackoverflow) | 1974-07-31 |
| CS208694B2 (en) | 1981-09-15 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| 8139 | Disposal/non-payment of the annual fee | ||
| 8141 | Disposal/no request for examination | ||
| 8180 | Miscellaneous part 1 |
Free format text: IN HEFT 28/82 ABSCHNITT 1H IST ZU STREICHEN: A01N 25-00 2403427 01.08.74 |