DE2347803A1 - Verfahren zur gewinnung chlorierter kohlenwasserstoffe - Google Patents
Verfahren zur gewinnung chlorierter kohlenwasserstoffeInfo
- Publication number
- DE2347803A1 DE2347803A1 DE19732347803 DE2347803A DE2347803A1 DE 2347803 A1 DE2347803 A1 DE 2347803A1 DE 19732347803 DE19732347803 DE 19732347803 DE 2347803 A DE2347803 A DE 2347803A DE 2347803 A1 DE2347803 A1 DE 2347803A1
- Authority
- DE
- Germany
- Prior art keywords
- hydrogen chloride
- water
- reaction product
- temperature
- chlorinated hydrocarbon
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- 150000008280 chlorinated hydrocarbons Chemical class 0.000 title claims description 49
- 238000000034 method Methods 0.000 title claims description 18
- 238000004519 manufacturing process Methods 0.000 title description 5
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 claims description 91
- 229910000041 hydrogen chloride Inorganic materials 0.000 claims description 71
- IXCSERBJSXMMFS-UHFFFAOYSA-N hydrogen chloride Substances Cl.Cl IXCSERBJSXMMFS-UHFFFAOYSA-N 0.000 claims description 71
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 46
- 238000001816 cooling Methods 0.000 claims description 32
- 239000007789 gas Substances 0.000 claims description 29
- WSLDOOZREJYCGB-UHFFFAOYSA-N 1,2-Dichloroethane Chemical compound ClCCCl WSLDOOZREJYCGB-UHFFFAOYSA-N 0.000 claims description 28
- 238000007710 freezing Methods 0.000 claims description 24
- 230000008014 freezing Effects 0.000 claims description 24
- 239000007864 aqueous solution Substances 0.000 claims description 6
- 239000007795 chemical reaction product Substances 0.000 description 53
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 10
- VGGSQFUCUMXWEO-UHFFFAOYSA-N Ethene Chemical compound C=C VGGSQFUCUMXWEO-UHFFFAOYSA-N 0.000 description 10
- 239000005977 Ethylene Substances 0.000 description 10
- 229930195733 hydrocarbon Natural products 0.000 description 9
- 150000002430 hydrocarbons Chemical class 0.000 description 9
- 239000000047 product Substances 0.000 description 8
- 238000006243 chemical reaction Methods 0.000 description 7
- 239000004215 Carbon black (E152) Substances 0.000 description 6
- UGFAIRIUMAVXCW-UHFFFAOYSA-N Carbon monoxide Chemical class [O+]#[C-] UGFAIRIUMAVXCW-UHFFFAOYSA-N 0.000 description 6
- 239000008346 aqueous phase Substances 0.000 description 6
- 238000011084 recovery Methods 0.000 description 6
- SCYULBFZEHDVBN-UHFFFAOYSA-N 1,1-Dichloroethane Chemical compound CC(Cl)Cl SCYULBFZEHDVBN-UHFFFAOYSA-N 0.000 description 5
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 5
- 238000009833 condensation Methods 0.000 description 5
- 230000005494 condensation Effects 0.000 description 5
- 229910052757 nitrogen Inorganic materials 0.000 description 5
- 239000012074 organic phase Substances 0.000 description 5
- 239000001301 oxygen Substances 0.000 description 5
- 229910052760 oxygen Inorganic materials 0.000 description 5
- 239000000243 solution Substances 0.000 description 5
- CURLTUGMZLYLDI-UHFFFAOYSA-N Carbon dioxide Chemical compound O=C=O CURLTUGMZLYLDI-UHFFFAOYSA-N 0.000 description 4
- 229910002090 carbon oxide Inorganic materials 0.000 description 4
- 230000006735 deficit Effects 0.000 description 3
- 239000012071 phase Substances 0.000 description 3
- HFFLGKNGCAIQMO-UHFFFAOYSA-N trichloroacetaldehyde Chemical compound ClC(Cl)(Cl)C=O HFFLGKNGCAIQMO-UHFFFAOYSA-N 0.000 description 3
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 description 2
- 229910002092 carbon dioxide Inorganic materials 0.000 description 2
- 239000001569 carbon dioxide Substances 0.000 description 2
- 229910002091 carbon monoxide Inorganic materials 0.000 description 2
- HRYZWHHZPQKTII-UHFFFAOYSA-N chloroethane Chemical compound CCCl HRYZWHHZPQKTII-UHFFFAOYSA-N 0.000 description 2
- 239000002826 coolant Substances 0.000 description 2
- 229960003750 ethyl chloride Drugs 0.000 description 2
- 239000000203 mixture Substances 0.000 description 2
- 230000004048 modification Effects 0.000 description 2
- 238000012986 modification Methods 0.000 description 2
- 238000000926 separation method Methods 0.000 description 2
- VEXZGXHMUGYJMC-UHFFFAOYSA-M Chloride anion Chemical compound [Cl-] VEXZGXHMUGYJMC-UHFFFAOYSA-M 0.000 description 1
- RYGMFSIKBFXOCR-UHFFFAOYSA-N Copper Chemical compound [Cu] RYGMFSIKBFXOCR-UHFFFAOYSA-N 0.000 description 1
- MYMOFIZGZYHOMD-UHFFFAOYSA-N Dioxygen Chemical compound O=O MYMOFIZGZYHOMD-UHFFFAOYSA-N 0.000 description 1
- OTMSDBZUPAUEDD-UHFFFAOYSA-N Ethane Chemical compound CC OTMSDBZUPAUEDD-UHFFFAOYSA-N 0.000 description 1
- XSTXAVWGXDQKEL-UHFFFAOYSA-N Trichloroethylene Chemical group ClC=C(Cl)Cl XSTXAVWGXDQKEL-UHFFFAOYSA-N 0.000 description 1
- 239000002253 acid Substances 0.000 description 1
- 239000003054 catalyst Substances 0.000 description 1
- 150000001805 chlorine compounds Chemical class 0.000 description 1
- 238000002485 combustion reaction Methods 0.000 description 1
- 229910052802 copper Inorganic materials 0.000 description 1
- 239000010949 copper Substances 0.000 description 1
- 238000010586 diagram Methods 0.000 description 1
- 229910001882 dioxygen Inorganic materials 0.000 description 1
- 239000002360 explosive Substances 0.000 description 1
- 238000000605 extraction Methods 0.000 description 1
- 239000004744 fabric Substances 0.000 description 1
- 238000005194 fractionation Methods 0.000 description 1
- 229910052742 iron Inorganic materials 0.000 description 1
- 229910052751 metal Inorganic materials 0.000 description 1
- 239000002184 metal Substances 0.000 description 1
- 238000006386 neutralization reaction Methods 0.000 description 1
- 229920006395 saturated elastomer Polymers 0.000 description 1
- 229930195734 saturated hydrocarbon Natural products 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
- 229930195735 unsaturated hydrocarbon Natural products 0.000 description 1
- 238000005406 washing Methods 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C17/00—Preparation of halogenated hydrocarbons
- C07C17/38—Separation; Purification; Stabilisation; Use of additives
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D53/00—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols
- B01D53/34—Chemical or biological purification of waste gases
- B01D53/46—Removing components of defined structure
- B01D53/68—Halogens or halogen compounds
- B01D53/70—Organic halogen compounds
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C17/00—Preparation of halogenated hydrocarbons
- C07C17/093—Preparation of halogenated hydrocarbons by replacement by halogens
- C07C17/15—Preparation of halogenated hydrocarbons by replacement by halogens with oxygen as auxiliary reagent, e.g. oxychlorination
- C07C17/152—Preparation of halogenated hydrocarbons by replacement by halogens with oxygen as auxiliary reagent, e.g. oxychlorination of hydrocarbons
- C07C17/156—Preparation of halogenated hydrocarbons by replacement by halogens with oxygen as auxiliary reagent, e.g. oxychlorination of hydrocarbons of unsaturated hydrocarbons
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P20/00—Technologies relating to chemical industry
- Y02P20/151—Reduction of greenhouse gas [GHG] emissions, e.g. CO2
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Health & Medical Sciences (AREA)
- Biomedical Technology (AREA)
- Environmental & Geological Engineering (AREA)
- Analytical Chemistry (AREA)
- General Chemical & Material Sciences (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US29291572A | 1972-09-28 | 1972-09-28 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| DE2347803A1 true DE2347803A1 (de) | 1974-04-11 |
Family
ID=23126796
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DE19732347803 Pending DE2347803A1 (de) | 1972-09-28 | 1973-09-22 | Verfahren zur gewinnung chlorierter kohlenwasserstoffe |
Country Status (7)
| Country | Link |
|---|---|
| US (1) | US3793801A (cg-RX-API-DMAC10.html) |
| JP (1) | JPS4970906A (cg-RX-API-DMAC10.html) |
| CA (1) | CA1014575A (cg-RX-API-DMAC10.html) |
| DE (1) | DE2347803A1 (cg-RX-API-DMAC10.html) |
| FR (1) | FR2201278B3 (cg-RX-API-DMAC10.html) |
| GB (1) | GB1405046A (cg-RX-API-DMAC10.html) |
| NL (1) | NL7313335A (cg-RX-API-DMAC10.html) |
Families Citing this family (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE2337055C2 (de) * | 1973-07-20 | 1982-12-09 | Linde Ag, 6200 Wiesbaden | Verfahren und Vorrichtung zur Rückgewinnung der in einem Benzin-Luft-Gemisch enthaltenen Kohlenwasserstoffe |
| US3948622A (en) * | 1974-07-12 | 1976-04-06 | The Lummus Company | Separation of aqueous hydrogen chloride from gaseous chlorinated hydrocarbons |
| US4028427A (en) * | 1975-08-27 | 1977-06-07 | The Lummus Company | Aqueous stream treatment in chlorinated hydrocarbon production |
| US4976862A (en) * | 1989-04-10 | 1990-12-11 | Dupont Canada Inc. | Process for extraction and recovery of blowing agents from polymeric foams |
| US4932984A (en) * | 1989-07-27 | 1990-06-12 | The Dow Chemical Company | Process for reduction of chlorinated solvent emissions |
| JP5747684B2 (ja) * | 2010-09-14 | 2015-07-15 | セントラル硝子株式会社 | ヒドロフルオロカーボンまたはヒドロクロロフルオロカーボンの脱水方法、および該脱水方法を用いた１，３，３，３−テトラフルオロプロペンの製造方法 |
Family Cites Families (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| GB675038A (en) * | 1949-01-25 | 1952-07-02 | Schweizerhall Saeurefab | Process for treating the gaseous products of the chlorination of oxidic ores |
| US2528028A (en) * | 1950-03-20 | 1950-10-31 | Arthur F Barry | Method and means for separating hydrocarbon liquids and water from high-pressure gasstreams |
| US2852517A (en) * | 1955-11-07 | 1958-09-16 | Dow Chemical Co | Separating method |
-
1972
- 1972-09-28 US US00292915A patent/US3793801A/en not_active Expired - Lifetime
-
1973
- 1973-08-24 CA CA179,553A patent/CA1014575A/en not_active Expired
- 1973-09-22 DE DE19732347803 patent/DE2347803A1/de active Pending
- 1973-09-26 JP JP48107668A patent/JPS4970906A/ja active Pending
- 1973-09-27 GB GB4532073A patent/GB1405046A/en not_active Expired
- 1973-09-27 NL NL7313335A patent/NL7313335A/xx not_active Application Discontinuation
- 1973-09-28 FR FR7334924A patent/FR2201278B3/fr not_active Expired
Also Published As
| Publication number | Publication date |
|---|---|
| CA1014575A (en) | 1977-07-26 |
| NL7313335A (cg-RX-API-DMAC10.html) | 1974-04-01 |
| AU6071073A (en) | 1975-03-27 |
| FR2201278A1 (cg-RX-API-DMAC10.html) | 1974-04-26 |
| JPS4970906A (cg-RX-API-DMAC10.html) | 1974-07-09 |
| FR2201278B3 (cg-RX-API-DMAC10.html) | 1976-08-27 |
| US3793801A (en) | 1974-02-26 |
| GB1405046A (en) | 1975-09-03 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| AT236928B (de) | Verfahren zur Herstellung von Äthylenoxyd | |
| DE2255895C2 (de) | Verfahren zur Wiedergewinnung von Chlorwasserstoff aus einem wäßrigen Chlorwasserstoffstrom | |
| DE19654516C1 (de) | Verfahren zur Auftrennung des Produktgasgemisches der katalytischen Synthese von Methylmercaptan | |
| DE2314786A1 (de) | Verfahren zur gewinnung von chlorwasserstoff | |
| DE2426640A1 (de) | Herstellung von allylchlorid | |
| DE2364149A1 (de) | Verfahren zur gleichzeitigen abtrennung von aethylenoxid und kohlendioxid aus bei der direktoxidation von aethylen mit sauerstoff anfallenden gasgemischen | |
| EP0307673B1 (de) | Verfahren zur Gewinnung von reinem Tetrafluorethylen | |
| DD146588A5 (de) | Verfahren zur rueckgewinnung von acrylsaeure | |
| DE2536286A1 (de) | Verfahren zur gewinnung von 1,2- dichloraethan | |
| DE2626133A1 (de) | Zyklisches verfahren zur herstellung von aethylendichlorid | |
| EP0053335B1 (de) | Verfahren zur Herstellung von 1,2-Dichlorethan | |
| DE2530306A1 (de) | Verfahren zur behandlung eines chlorierten kohlenwasserstoff enthaltenden gasfoermigen ausgangsprodukts | |
| EP0006526B1 (de) | Verfahren zur Gewinnung eines wasserfreien Chlorwasserstoff enthaltenden Gasgemisches aus Chlor enthaltenden organischen Rückständen | |
| DE3002660A1 (de) | Verfahren zur gewinnung von methacrolein | |
| DE1109151B (de) | Verfahren zur Wiedergewinnung von trockenem Chlor aus chlorhaltigem Chlorwasserstoff | |
| DE1693042A1 (de) | Verfahren zur Herstellung von Vinylchlorid | |
| DE910536C (de) | Verfahren zur Gewinnung von reinem Schwefeltrioxyd | |
| DE2714027A1 (de) | Verfahren zur wiedergewinnung von chlorwasserstoff | |
| DE2509966A1 (de) | Verfahren zur oxidation von salzschmelzen und rueckgewinnung von chlor | |
| DE2602749A1 (de) | Verfahren zur abtrennung eines niedrig siedenden, chlorierten kohlenwasserstoffs aus einem gasstrom | |
| DE2431531A1 (de) | Verfahren zur abtrennung von von sauren gasen im wesentlichen freiem ammoniak | |
| CH631135A5 (de) | Verfahren zur herstellung von hochreinem brom. | |
| DE3226042A1 (de) | Verfahren zur herstellung von 1,2-dichlorethan | |
| DE2705427A1 (de) | Verfahren zur oxidation einer geschmolzenen salzmischung | |
| DE2247343A1 (de) | Verfahren zur erzeugung von acetaldehyd |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| OHA | Expiration of time for request for examination |