DE2329045A1 - Verfahren zur reinigung von titantetrachlorid - Google Patents
Verfahren zur reinigung von titantetrachloridInfo
- Publication number
- DE2329045A1 DE2329045A1 DE2329045A DE2329045A DE2329045A1 DE 2329045 A1 DE2329045 A1 DE 2329045A1 DE 2329045 A DE2329045 A DE 2329045A DE 2329045 A DE2329045 A DE 2329045A DE 2329045 A1 DE2329045 A1 DE 2329045A1
- Authority
- DE
- Germany
- Prior art keywords
- ticl
- vanadium
- titanium tetrachloride
- distillation
- crude
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- 238000000034 method Methods 0.000 title claims description 18
- 238000004140 cleaning Methods 0.000 title description 8
- RTAQQCXQSZGOHL-UHFFFAOYSA-N Titanium Chemical compound [Ti] RTAQQCXQSZGOHL-UHFFFAOYSA-N 0.000 title description 3
- 239000010936 titanium Substances 0.000 title description 3
- 229910052719 titanium Inorganic materials 0.000 title description 3
- MWPLVEDNUUSJAV-UHFFFAOYSA-N anthracene Chemical compound C1=CC=CC2=CC3=CC=CC=C3C=C21 MWPLVEDNUUSJAV-UHFFFAOYSA-N 0.000 claims description 22
- 229910052720 vanadium Inorganic materials 0.000 claims description 18
- LEONUFNNVUYDNQ-UHFFFAOYSA-N vanadium atom Chemical compound [V] LEONUFNNVUYDNQ-UHFFFAOYSA-N 0.000 claims description 18
- XJDNKRIXUMDJCW-UHFFFAOYSA-J titanium tetrachloride Chemical compound Cl[Ti](Cl)(Cl)Cl XJDNKRIXUMDJCW-UHFFFAOYSA-J 0.000 claims description 17
- HYBBIBNJHNGZAN-UHFFFAOYSA-N furfural Chemical compound O=CC1=CC=CO1 HYBBIBNJHNGZAN-UHFFFAOYSA-N 0.000 claims description 8
- 150000001491 aromatic compounds Chemical class 0.000 claims description 7
- -1 cyclic aliphatic Chemical class 0.000 claims description 7
- CTQNGGLPUBDAKN-UHFFFAOYSA-N O-Xylene Chemical compound CC1=CC=CC=C1C CTQNGGLPUBDAKN-UHFFFAOYSA-N 0.000 claims description 4
- HPXRVTGHNJAIIH-UHFFFAOYSA-N cyclohexanol Chemical compound OC1CCCCC1 HPXRVTGHNJAIIH-UHFFFAOYSA-N 0.000 claims description 4
- 238000000746 purification Methods 0.000 claims description 4
- 239000008096 xylene Substances 0.000 claims description 4
- 150000002894 organic compounds Chemical class 0.000 claims description 3
- 238000004821 distillation Methods 0.000 description 18
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 description 6
- 238000009835 boiling Methods 0.000 description 6
- 239000007787 solid Substances 0.000 description 6
- GWEVSGVZZGPLCZ-UHFFFAOYSA-N Titan oxide Chemical compound O=[Ti]=O GWEVSGVZZGPLCZ-UHFFFAOYSA-N 0.000 description 5
- 150000001875 compounds Chemical class 0.000 description 5
- 238000010438 heat treatment Methods 0.000 description 5
- 239000000049 pigment Substances 0.000 description 5
- 150000001805 chlorine compounds Chemical class 0.000 description 4
- 239000012535 impurity Substances 0.000 description 4
- 150000003682 vanadium compounds Chemical class 0.000 description 4
- 229910052742 iron Inorganic materials 0.000 description 3
- 238000004519 manufacturing process Methods 0.000 description 3
- 239000000047 product Substances 0.000 description 3
- XUIMIQQOPSSXEZ-UHFFFAOYSA-N Silicon Chemical compound [Si] XUIMIQQOPSSXEZ-UHFFFAOYSA-N 0.000 description 2
- 229910052782 aluminium Inorganic materials 0.000 description 2
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 description 2
- 238000006243 chemical reaction Methods 0.000 description 2
- 238000005660 chlorination reaction Methods 0.000 description 2
- 239000000460 chlorine Substances 0.000 description 2
- 239000012459 cleaning agent Substances 0.000 description 2
- 239000003925 fat Substances 0.000 description 2
- 229910052751 metal Inorganic materials 0.000 description 2
- 239000002184 metal Substances 0.000 description 2
- 238000000926 separation method Methods 0.000 description 2
- 229910052710 silicon Inorganic materials 0.000 description 2
- 239000010703 silicon Substances 0.000 description 2
- 239000000725 suspension Substances 0.000 description 2
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 1
- ZAMOUSCENKQFHK-UHFFFAOYSA-N Chlorine atom Chemical compound [Cl] ZAMOUSCENKQFHK-UHFFFAOYSA-N 0.000 description 1
- RYGMFSIKBFXOCR-UHFFFAOYSA-N Copper Chemical compound [Cu] RYGMFSIKBFXOCR-UHFFFAOYSA-N 0.000 description 1
- 229910021552 Vanadium(IV) chloride Inorganic materials 0.000 description 1
- 229910007926 ZrCl Inorganic materials 0.000 description 1
- 239000000654 additive Substances 0.000 description 1
- 150000001298 alcohols Chemical class 0.000 description 1
- VSCWAEJMTAWNJL-UHFFFAOYSA-K aluminium trichloride Chemical class Cl[Al](Cl)Cl VSCWAEJMTAWNJL-UHFFFAOYSA-K 0.000 description 1
- 150000001412 amines Chemical class 0.000 description 1
- 239000010775 animal oil Substances 0.000 description 1
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 229910052799 carbon Inorganic materials 0.000 description 1
- 229910052801 chlorine Inorganic materials 0.000 description 1
- ZHXZNKNQUHUIGN-UHFFFAOYSA-N chloro hypochlorite;vanadium Chemical compound [V].ClOCl ZHXZNKNQUHUIGN-UHFFFAOYSA-N 0.000 description 1
- 238000002485 combustion reaction Methods 0.000 description 1
- 239000000356 contaminant Substances 0.000 description 1
- 238000010924 continuous production Methods 0.000 description 1
- 229910052802 copper Inorganic materials 0.000 description 1
- 239000010949 copper Substances 0.000 description 1
- 239000012043 crude product Substances 0.000 description 1
- 238000006298 dechlorination reaction Methods 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 229930195733 hydrocarbon Natural products 0.000 description 1
- 150000002430 hydrocarbons Chemical class 0.000 description 1
- YDZQQRWRVYGNER-UHFFFAOYSA-N iron;titanium;trihydrate Chemical compound O.O.O.[Ti].[Fe] YDZQQRWRVYGNER-UHFFFAOYSA-N 0.000 description 1
- 150000002576 ketones Chemical class 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 150000002739 metals Chemical class 0.000 description 1
- 239000003921 oil Substances 0.000 description 1
- 235000019198 oils Nutrition 0.000 description 1
- 230000003287 optical effect Effects 0.000 description 1
- 150000007524 organic acids Chemical class 0.000 description 1
- 235000005985 organic acids Nutrition 0.000 description 1
- 230000003647 oxidation Effects 0.000 description 1
- 238000007254 oxidation reaction Methods 0.000 description 1
- 229910052760 oxygen Inorganic materials 0.000 description 1
- 239000001301 oxygen Substances 0.000 description 1
- RPESBQCJGHJMTK-UHFFFAOYSA-I pentachlorovanadium Chemical class [Cl-].[Cl-].[Cl-].[Cl-].[Cl-].[V+5] RPESBQCJGHJMTK-UHFFFAOYSA-I 0.000 description 1
- 239000002244 precipitate Substances 0.000 description 1
- 238000010992 reflux Methods 0.000 description 1
- 239000011347 resin Substances 0.000 description 1
- 229920005989 resin Polymers 0.000 description 1
- 150000003839 salts Chemical class 0.000 description 1
- 239000000344 soap Substances 0.000 description 1
- 238000001228 spectrum Methods 0.000 description 1
- GBECUEIQVRDUKB-UHFFFAOYSA-M thallium monochloride Chemical compound [Tl]Cl GBECUEIQVRDUKB-UHFFFAOYSA-M 0.000 description 1
- 239000004408 titanium dioxide Substances 0.000 description 1
- OGIDPMRJRNCKJF-UHFFFAOYSA-N titanium oxide Inorganic materials [Ti]=O OGIDPMRJRNCKJF-UHFFFAOYSA-N 0.000 description 1
- JTJFQBNJBPPZRI-UHFFFAOYSA-J vanadium tetrachloride Chemical compound Cl[V](Cl)(Cl)Cl JTJFQBNJBPPZRI-UHFFFAOYSA-J 0.000 description 1
- 235000015112 vegetable and seed oil Nutrition 0.000 description 1
- 239000008158 vegetable oil Substances 0.000 description 1
- 239000001993 wax Substances 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
- C01G23/00—Compounds of titanium
- C01G23/02—Halides of titanium
- C01G23/022—Titanium tetrachloride
- C01G23/024—Purification of tetrachloride
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Life Sciences & Earth Sciences (AREA)
- Environmental & Geological Engineering (AREA)
- General Life Sciences & Earth Sciences (AREA)
- Geology (AREA)
- Inorganic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Transition And Organic Metals Composition Catalysts For Addition Polymerization (AREA)
Priority Applications (10)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE2329045A DE2329045A1 (de) | 1973-06-07 | 1973-06-07 | Verfahren zur reinigung von titantetrachlorid |
| DD178963A DD114801A5 (cs) | 1973-06-07 | 1974-06-05 | |
| FI1713/74A FI171374A7 (cs) | 1973-06-07 | 1974-06-05 | |
| JP49062979A JPS5021992A (cs) | 1973-06-07 | 1974-06-05 | |
| NL7407560A NL7407560A (cs) | 1973-06-07 | 1974-06-05 | |
| AR254093A AR199159A1 (es) | 1973-06-07 | 1974-06-06 | Procedimiento para la purificacion de tetracloruro de titanio impuro |
| NO742049A NO742049L (cs) | 1973-06-07 | 1974-06-06 | |
| BR4654/74A BR7404654D0 (pt) | 1973-06-07 | 1974-06-06 | Processo para a purificacao de tetracloreto de titanio |
| BE145131A BE815982A (fr) | 1973-06-07 | 1974-06-06 | Purification du tetrachlorure de titane |
| FR7419783A FR2232513A1 (en) | 1973-06-07 | 1974-06-07 | Purification of crude titanium tetrachloride - by distilling off from added anthracene, furfurol, or cyclohexanol |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE2329045A DE2329045A1 (de) | 1973-06-07 | 1973-06-07 | Verfahren zur reinigung von titantetrachlorid |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| DE2329045A1 true DE2329045A1 (de) | 1975-01-02 |
Family
ID=5883332
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DE2329045A Pending DE2329045A1 (de) | 1973-06-07 | 1973-06-07 | Verfahren zur reinigung von titantetrachlorid |
Country Status (10)
| Country | Link |
|---|---|
| JP (1) | JPS5021992A (cs) |
| AR (1) | AR199159A1 (cs) |
| BE (1) | BE815982A (cs) |
| BR (1) | BR7404654D0 (cs) |
| DD (1) | DD114801A5 (cs) |
| DE (1) | DE2329045A1 (cs) |
| FI (1) | FI171374A7 (cs) |
| FR (1) | FR2232513A1 (cs) |
| NL (1) | NL7407560A (cs) |
| NO (1) | NO742049L (cs) |
Families Citing this family (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP5208044B2 (ja) * | 2009-04-21 | 2013-06-12 | Ｊｘ日鉱日石エネルギー株式会社 | 四塩化チタン精製用配合油 |
| CN106745215B (zh) * | 2016-01-25 | 2018-09-28 | 攀枝花学院 | 粗四氯化钛的精制过程蒸馏釜残液的回收利用方法 |
-
1973
- 1973-06-07 DE DE2329045A patent/DE2329045A1/de active Pending
-
1974
- 1974-06-05 DD DD178963A patent/DD114801A5/xx unknown
- 1974-06-05 FI FI1713/74A patent/FI171374A7/fi unknown
- 1974-06-05 NL NL7407560A patent/NL7407560A/xx unknown
- 1974-06-05 JP JP49062979A patent/JPS5021992A/ja active Pending
- 1974-06-06 NO NO742049A patent/NO742049L/no unknown
- 1974-06-06 AR AR254093A patent/AR199159A1/es active
- 1974-06-06 BE BE145131A patent/BE815982A/xx unknown
- 1974-06-06 BR BR4654/74A patent/BR7404654D0/pt unknown
- 1974-06-07 FR FR7419783A patent/FR2232513A1/fr not_active Withdrawn
Also Published As
| Publication number | Publication date |
|---|---|
| BE815982A (fr) | 1974-12-06 |
| BR7404654D0 (pt) | 1975-09-30 |
| NO742049L (cs) | 1975-01-06 |
| DD114801A5 (cs) | 1975-08-20 |
| AR199159A1 (es) | 1974-08-08 |
| NL7407560A (cs) | 1974-12-10 |
| FI171374A7 (cs) | 1974-12-08 |
| JPS5021992A (cs) | 1975-03-08 |
| FR2232513A1 (en) | 1975-01-03 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| DE2426640A1 (de) | Herstellung von allylchlorid | |
| DE2343344A1 (de) | Verfahren zur herstellung von titandioxydpigment | |
| DE925775C (de) | Verfahren zur Herstellung von Phenol | |
| DE2439540B1 (de) | Verfahren zur Rückgewinnung von Antimonpentachlorid aus zur Fluorierung von chlorierten Kohlenwasserstoffen eingesetzten Katalysatorlösungen | |
| EP0253183B1 (de) | Verfahren zur Herstellung von TiCl4 | |
| DE1925291C3 (de) | Verfahren zur Gewinnung von Vanadinoxytrichlorid aus festen, trockenen Rückständen der Reinigung von rohem Titantetrachlorid mit Schwefelwasserstoff | |
| DE68904760T2 (de) | Regeneration von erschoepften schwefelsaeuren mittels wasserstoffperoxyd. | |
| DE2329045A1 (de) | Verfahren zur reinigung von titantetrachlorid | |
| DE19649027A1 (de) | Verfahren zur Herstellung von Organocarbonoyloxysilanen | |
| DE2218361A1 (de) | Verfahren zur kontinuierlichen reinigung von titantetrachlorid | |
| DE69020572T2 (de) | Verfahren zur entfernung von chloropren aus 1,2-dichlorethan. | |
| DE2325924C3 (de) | Verfahren zur Reinigung von Titantetrachlorid | |
| DE2325924A1 (de) | Verfahren zur reinigung von titantetrachlorid | |
| DE723223C (de) | Entfaerben von Titan (4) chlorid | |
| DE2729911A1 (de) | Verfahren zur herstellung von alpha-chloralkanoylchloriden | |
| DE1017610B (de) | Verfahren zur Herstellung von Chlorphenylchlorsilanen | |
| DE3837394A1 (de) | Verfahren zur herstellung von telomeren aus chlortriflouraethylen und triflourtrichloraethan | |
| DE1175690B (de) | Verfahren zur Herstellung von 4-Chlor-2-methylphenol | |
| DE1493801A1 (de) | Verfahren zur Trennung und Gewinnung der Reaktionsprodukte im Raschig-Phenolprozess | |
| DE1289836B (de) | Verfahren zur Reinigung von Titantetrachlorid | |
| DE69118595T2 (de) | Verfahren zur Reinigung von 2-Chloropropionsäure | |
| DE2335949A1 (de) | Verfahren zur gewinnung von vinylchlorid | |
| DE69004974T2 (de) | Herstellung von 2-Chlorterephthalsäurechlorid. | |
| DE1237081B (de) | Verfahren zur Reinigung von Vanadylchlorid enthaltendem Titantetrachlorid | |
| DE1443470C (de) | Verfahren zur Entalkylierung von alkylaromatischen Kohlenwasserstoffen |