DE2263498C3 - Verfahren zur kontinuierlichen Herstellung sauerstoffhaltiger Verbindungen - Google Patents
Verfahren zur kontinuierlichen Herstellung sauerstoffhaltiger VerbindungenInfo
- Publication number
- DE2263498C3 DE2263498C3 DE2263498A DE2263498A DE2263498C3 DE 2263498 C3 DE2263498 C3 DE 2263498C3 DE 2263498 A DE2263498 A DE 2263498A DE 2263498 A DE2263498 A DE 2263498A DE 2263498 C3 DE2263498 C3 DE 2263498C3
- Authority
- DE
- Germany
- Prior art keywords
- chamber
- reaction
- liquid
- reactor
- gaseous phase
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- 238000000034 method Methods 0.000 title claims description 25
- 150000001875 compounds Chemical class 0.000 title claims description 8
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 title claims description 6
- 238000010924 continuous production Methods 0.000 title claims description 6
- 239000001301 oxygen Substances 0.000 title claims description 6
- 229910052760 oxygen Inorganic materials 0.000 title claims description 6
- 238000006243 chemical reaction Methods 0.000 claims description 60
- 239000007789 gas Substances 0.000 claims description 20
- 238000001816 cooling Methods 0.000 claims description 18
- 239000007791 liquid phase Substances 0.000 claims description 17
- 239000007792 gaseous phase Substances 0.000 claims description 13
- 239000001257 hydrogen Substances 0.000 claims description 8
- 229910052739 hydrogen Inorganic materials 0.000 claims description 8
- 239000003054 catalyst Substances 0.000 claims description 7
- UGFAIRIUMAVXCW-UHFFFAOYSA-N Carbon monoxide Chemical compound [O+]#[C-] UGFAIRIUMAVXCW-UHFFFAOYSA-N 0.000 claims description 6
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 claims description 6
- 229910002091 carbon monoxide Inorganic materials 0.000 claims description 6
- 229910052751 metal Inorganic materials 0.000 claims description 4
- 239000002184 metal Substances 0.000 claims description 4
- 229930195733 hydrocarbon Natural products 0.000 claims description 3
- 150000002430 hydrocarbons Chemical class 0.000 claims description 3
- 150000002739 metals Chemical class 0.000 claims description 3
- 230000007704 transition Effects 0.000 claims description 2
- 230000000414 obstructive effect Effects 0.000 claims 1
- 230000015572 biosynthetic process Effects 0.000 description 21
- 238000003786 synthesis reaction Methods 0.000 description 15
- 150000001336 alkenes Chemical class 0.000 description 14
- 239000007795 chemical reaction product Substances 0.000 description 14
- 239000007788 liquid Substances 0.000 description 12
- JRZJOMJEPLMPRA-UHFFFAOYSA-N olefin Natural products CCCCCCCC=C JRZJOMJEPLMPRA-UHFFFAOYSA-N 0.000 description 11
- 239000000376 reactant Substances 0.000 description 8
- 239000000047 product Substances 0.000 description 6
- 238000002474 experimental method Methods 0.000 description 4
- 238000002156 mixing Methods 0.000 description 4
- 150000001299 aldehydes Chemical class 0.000 description 3
- QQONPFPTGQHPMA-UHFFFAOYSA-N propylene Natural products CC=C QQONPFPTGQHPMA-UHFFFAOYSA-N 0.000 description 3
- 125000004805 propylene group Chemical group [H]C([H])([H])C([H])([*:1])C([H])([H])[*:2] 0.000 description 3
- 239000007858 starting material Substances 0.000 description 3
- LRHPLDYGYMQRHN-UHFFFAOYSA-N N-Butanol Chemical compound CCCCO LRHPLDYGYMQRHN-UHFFFAOYSA-N 0.000 description 2
- ATUOYWHBWRKTHZ-UHFFFAOYSA-N Propane Chemical compound CCC ATUOYWHBWRKTHZ-UHFFFAOYSA-N 0.000 description 2
- 239000006227 byproduct Substances 0.000 description 2
- 239000003814 drug Substances 0.000 description 2
- 230000017525 heat dissipation Effects 0.000 description 2
- 239000000203 mixture Substances 0.000 description 2
- 238000002360 preparation method Methods 0.000 description 2
- 239000001294 propane Substances 0.000 description 2
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 1
- CURLTUGMZLYLDI-UHFFFAOYSA-N Carbon dioxide Chemical compound O=C=O CURLTUGMZLYLDI-UHFFFAOYSA-N 0.000 description 1
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 1
- AMIMRNSIRUDHCM-UHFFFAOYSA-N Isopropylaldehyde Chemical compound CC(C)C=O AMIMRNSIRUDHCM-UHFFFAOYSA-N 0.000 description 1
- 230000001133 acceleration Effects 0.000 description 1
- 150000001298 alcohols Chemical class 0.000 description 1
- 238000009835 boiling Methods 0.000 description 1
- QJEBFGJWFJQTAO-UHFFFAOYSA-N butanal;prop-1-ene Chemical compound CC=C.CCCC=O QJEBFGJWFJQTAO-UHFFFAOYSA-N 0.000 description 1
- 229910052799 carbon Inorganic materials 0.000 description 1
- 229910002090 carbon oxide Inorganic materials 0.000 description 1
- 150000001728 carbonyl compounds Chemical class 0.000 description 1
- 125000002915 carbonyl group Chemical group [*:2]C([*:1])=O 0.000 description 1
- 230000003197 catalytic effect Effects 0.000 description 1
- 239000012295 chemical reaction liquid Substances 0.000 description 1
- 239000007805 chemical reaction reactant Substances 0.000 description 1
- 229910017052 cobalt Inorganic materials 0.000 description 1
- 239000010941 cobalt Substances 0.000 description 1
- -1 cobalt carbonyl compounds Chemical class 0.000 description 1
- 239000012043 crude product Substances 0.000 description 1
- 238000013461 design Methods 0.000 description 1
- 238000001704 evaporation Methods 0.000 description 1
- 150000002431 hydrogen Chemical class 0.000 description 1
- ZXEKIIBDNHEJCQ-UHFFFAOYSA-N isobutanol Chemical compound CC(C)CO ZXEKIIBDNHEJCQ-UHFFFAOYSA-N 0.000 description 1
- 239000012263 liquid product Substances 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 210000000056 organ Anatomy 0.000 description 1
- 238000013021 overheating Methods 0.000 description 1
- 150000002927 oxygen compounds Chemical class 0.000 description 1
- 238000010517 secondary reaction Methods 0.000 description 1
- 238000000926 separation method Methods 0.000 description 1
- 239000002904 solvent Substances 0.000 description 1
- 125000006850 spacer group Chemical group 0.000 description 1
- 238000012546 transfer Methods 0.000 description 1
- 230000007306 turnover Effects 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/24—Stationary reactors without moving elements inside
- B01J19/2415—Tubular reactors
- B01J19/2425—Tubular reactors in parallel
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C45/00—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds
- C07C45/49—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by reaction with carbon monoxide
- C07C45/50—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by reaction with carbon monoxide by oxo-reactions
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J2219/00049—Controlling or regulating processes
- B01J2219/00051—Controlling the temperature
- B01J2219/00074—Controlling the temperature by indirect heating or cooling employing heat exchange fluids
- B01J2219/00076—Controlling the temperature by indirect heating or cooling employing heat exchange fluids with heat exchange elements inside the reactor
- B01J2219/00083—Coils
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J2219/00049—Controlling or regulating processes
- B01J2219/00051—Controlling the temperature
- B01J2219/00159—Controlling the temperature controlling multiple zones along the direction of flow, e.g. pre-heating and after-cooling
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
Priority Applications (10)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE2263498A DE2263498C3 (de) | 1972-12-27 | 1972-12-27 | Verfahren zur kontinuierlichen Herstellung sauerstoffhaltiger Verbindungen |
| NL7301403.A NL162050C (nl) | 1972-12-27 | 1973-01-31 | Werkwijze voor de continue bereiding van zuurstofhoudende verbindingen. |
| US424988A US3929900A (en) | 1972-12-27 | 1973-12-14 | Continuous process for the production of oxygen containing compounds |
| PL1973167452A PL104156B1 (pl) | 1972-12-27 | 1973-12-19 | Urzadzenie do ciaglego wytwarzania zwiazkow zawierajacych tlen |
| GB5919873A GB1447370A (en) | 1972-12-27 | 1973-12-20 | Process for the production of oxygen-containing compounds by the oxo reaction |
| JP48142910A JPS5115007B2 (cg-RX-API-DMAC7.html) | 1972-12-27 | 1973-12-20 | |
| FR7345769A FR2212314B1 (cg-RX-API-DMAC7.html) | 1972-12-27 | 1973-12-20 | |
| CA188,796A CA1018996A (en) | 1972-12-27 | 1973-12-21 | Continuous process for the production of oxygen containing compounds |
| IT54637/73A IT1002560B (it) | 1972-12-27 | 1973-12-27 | Procedimento per la produzione in continuo di composti contenenti ossigeno |
| US05/588,082 US3988117A (en) | 1972-12-27 | 1975-06-18 | Reactor for the production of oxygen containing compounds |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE2263498A DE2263498C3 (de) | 1972-12-27 | 1972-12-27 | Verfahren zur kontinuierlichen Herstellung sauerstoffhaltiger Verbindungen |
Publications (3)
| Publication Number | Publication Date |
|---|---|
| DE2263498A1 DE2263498A1 (de) | 1974-07-18 |
| DE2263498B2 DE2263498B2 (de) | 1978-03-16 |
| DE2263498C3 true DE2263498C3 (de) | 1978-11-09 |
Family
ID=5865499
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DE2263498A Expired DE2263498C3 (de) | 1972-12-27 | 1972-12-27 | Verfahren zur kontinuierlichen Herstellung sauerstoffhaltiger Verbindungen |
Country Status (9)
| Country | Link |
|---|---|
| US (1) | US3929900A (cg-RX-API-DMAC7.html) |
| JP (1) | JPS5115007B2 (cg-RX-API-DMAC7.html) |
| CA (1) | CA1018996A (cg-RX-API-DMAC7.html) |
| DE (1) | DE2263498C3 (cg-RX-API-DMAC7.html) |
| FR (1) | FR2212314B1 (cg-RX-API-DMAC7.html) |
| GB (1) | GB1447370A (cg-RX-API-DMAC7.html) |
| IT (1) | IT1002560B (cg-RX-API-DMAC7.html) |
| NL (1) | NL162050C (cg-RX-API-DMAC7.html) |
| PL (1) | PL104156B1 (cg-RX-API-DMAC7.html) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE2538037A1 (de) * | 1975-08-27 | 1977-04-07 | Huels Chemische Werke Ag | Verfahren und vorrichtung zur hydroformylierung von olefinen |
Families Citing this family (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE2747302C2 (de) * | 1977-10-21 | 1985-11-21 | Ruhrchemie Ag, 4200 Oberhausen | Verfahren zur kontinuierlichen Herstellung sauerstoffhaltiger Verbindungen |
| US4306084A (en) * | 1978-12-06 | 1981-12-15 | The University Of Texas | Alcohol and aldehyde production using ruthenium carbonyl catalysts |
| US5410091A (en) * | 1994-06-02 | 1995-04-25 | Quimica Oxal C.A. | Rhodium catalyzed oxo process in tubular reactor |
| DE10106482A1 (de) * | 2001-02-13 | 2002-08-14 | Basf Ag | Hydroformylierung |
| DE102007023085A1 (de) * | 2007-05-16 | 2007-10-25 | Alldos Eichler Gmbh | Vorrichtung zur Erzeugung von fluiden Reaktionsprodukten |
| FR3113612B1 (fr) * | 2020-08-27 | 2024-01-12 | Commissariat Energie Atomique | Réacteur- échangeur intégré à deux étages de lits fixes et procédé associé |
Family Cites Families (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2557701A (en) * | 1948-03-19 | 1951-06-19 | Standard Oil Dev Co | Catalytic reaction of olefins with carbon monoxide and hydrogen |
| US2711429A (en) * | 1949-05-02 | 1955-06-21 | Ici Ltd | Method and apparatus for controlling temperature in olefin carbonylation |
-
1972
- 1972-12-27 DE DE2263498A patent/DE2263498C3/de not_active Expired
-
1973
- 1973-01-31 NL NL7301403.A patent/NL162050C/xx not_active IP Right Cessation
- 1973-12-14 US US424988A patent/US3929900A/en not_active Expired - Lifetime
- 1973-12-19 PL PL1973167452A patent/PL104156B1/pl unknown
- 1973-12-20 GB GB5919873A patent/GB1447370A/en not_active Expired
- 1973-12-20 FR FR7345769A patent/FR2212314B1/fr not_active Expired
- 1973-12-20 JP JP48142910A patent/JPS5115007B2/ja not_active Expired
- 1973-12-21 CA CA188,796A patent/CA1018996A/en not_active Expired
- 1973-12-27 IT IT54637/73A patent/IT1002560B/it active
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE2538037A1 (de) * | 1975-08-27 | 1977-04-07 | Huels Chemische Werke Ag | Verfahren und vorrichtung zur hydroformylierung von olefinen |
Also Published As
| Publication number | Publication date |
|---|---|
| NL162050C (nl) | 1980-04-15 |
| NL7301403A (cg-RX-API-DMAC7.html) | 1974-07-01 |
| PL104156B1 (pl) | 1979-08-31 |
| GB1447370A (en) | 1976-08-25 |
| IT1002560B (it) | 1976-05-20 |
| JPS5115007B2 (cg-RX-API-DMAC7.html) | 1976-05-13 |
| NL162050B (nl) | 1979-11-15 |
| JPS4988816A (cg-RX-API-DMAC7.html) | 1974-08-24 |
| US3929900A (en) | 1975-12-30 |
| DE2263498B2 (de) | 1978-03-16 |
| CA1018996A (en) | 1977-10-11 |
| FR2212314A1 (cg-RX-API-DMAC7.html) | 1974-07-26 |
| DE2263498A1 (de) | 1974-07-18 |
| FR2212314B1 (cg-RX-API-DMAC7.html) | 1978-08-11 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C3 | Grant after two publication steps (3rd publication) | ||
| 8339 | Ceased/non-payment of the annual fee |