DE2219402A1 - Verfahren zur Herstellung von Vinylchloridpolymerisaten - Google Patents
Verfahren zur Herstellung von VinylchloridpolymerisatenInfo
- Publication number
- DE2219402A1 DE2219402A1 DE19722219402 DE2219402A DE2219402A1 DE 2219402 A1 DE2219402 A1 DE 2219402A1 DE 19722219402 DE19722219402 DE 19722219402 DE 2219402 A DE2219402 A DE 2219402A DE 2219402 A1 DE2219402 A1 DE 2219402A1
- Authority
- DE
- Germany
- Prior art keywords
- vinyl chloride
- primary polymer
- polymerization
- polymer
- primary
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- 229920000642 polymer Polymers 0.000 title claims description 111
- BZHJMEDXRYGGRV-UHFFFAOYSA-N Vinyl chloride Chemical compound ClC=C BZHJMEDXRYGGRV-UHFFFAOYSA-N 0.000 title claims description 74
- 238000000034 method Methods 0.000 title claims description 44
- 238000004519 manufacturing process Methods 0.000 title claims description 11
- 229920000915 polyvinyl chloride Polymers 0.000 claims description 23
- 239000004800 polyvinyl chloride Substances 0.000 claims description 23
- 238000006116 polymerization reaction Methods 0.000 claims description 22
- 239000000178 monomer Substances 0.000 claims description 19
- 239000000725 suspension Substances 0.000 claims description 19
- 239000000203 mixture Substances 0.000 claims description 13
- 238000010557 suspension polymerization reaction Methods 0.000 claims description 11
- 239000000126 substance Substances 0.000 claims description 9
- 229920001577 copolymer Polymers 0.000 claims description 8
- 238000012662 bulk polymerization Methods 0.000 claims description 7
- 238000010526 radical polymerization reaction Methods 0.000 claims description 7
- 238000007720 emulsion polymerization reaction Methods 0.000 claims description 4
- 239000003999 initiator Substances 0.000 claims description 3
- 238000010528 free radical solution polymerization reaction Methods 0.000 claims description 2
- 230000000379 polymerizing effect Effects 0.000 claims description 2
- 150000003254 radicals Chemical class 0.000 claims description 2
- YIVJZNGAASQVEM-UHFFFAOYSA-N Lauroyl peroxide Chemical compound CCCCCCCCCCCC(=O)OOC(=O)CCCCCCCCCCC YIVJZNGAASQVEM-UHFFFAOYSA-N 0.000 description 28
- 239000011347 resin Substances 0.000 description 26
- 229920005989 resin Polymers 0.000 description 26
- 239000004816 latex Substances 0.000 description 23
- 229920000126 latex Polymers 0.000 description 23
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 23
- QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 description 21
- 239000012153 distilled water Substances 0.000 description 16
- 239000000047 product Substances 0.000 description 14
- 229920003091 Methocel™ Polymers 0.000 description 12
- 238000002441 X-ray diffraction Methods 0.000 description 12
- 239000000843 powder Substances 0.000 description 7
- QZFAGHFGBLEISM-DBQHITQZSA-N 3-[(1r)-1-hydroxy-2-(methylamino)ethyl]phenol;4-[1-hydroxy-2-(propan-2-ylamino)butyl]benzene-1,2-diol;dihydrochloride Chemical compound Cl.Cl.CNC[C@H](O)C1=CC=CC(O)=C1.CC(C)NC(CC)C(O)C1=CC=C(O)C(O)=C1 QZFAGHFGBLEISM-DBQHITQZSA-N 0.000 description 6
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 description 6
- 239000004372 Polyvinyl alcohol Substances 0.000 description 6
- 229920002451 polyvinyl alcohol Polymers 0.000 description 6
- 229910001220 stainless steel Inorganic materials 0.000 description 6
- 239000010935 stainless steel Substances 0.000 description 6
- 238000012360 testing method Methods 0.000 description 6
- 239000008346 aqueous phase Substances 0.000 description 5
- 239000002245 particle Substances 0.000 description 5
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 4
- 239000007795 chemical reaction product Substances 0.000 description 4
- 230000000052 comparative effect Effects 0.000 description 4
- 239000003995 emulsifying agent Substances 0.000 description 4
- 239000010408 film Substances 0.000 description 4
- 239000007787 solid Substances 0.000 description 4
- 235000021355 Stearic acid Nutrition 0.000 description 3
- 238000013459 approach Methods 0.000 description 3
- 150000001875 compounds Chemical class 0.000 description 3
- QIQXTHQIDYTFRH-UHFFFAOYSA-N octadecanoic acid Chemical compound CCCCCCCCCCCCCCCCCC(O)=O QIQXTHQIDYTFRH-UHFFFAOYSA-N 0.000 description 3
- OQCDKBAXFALNLD-UHFFFAOYSA-N octadecanoic acid Natural products CCCCCCCC(C)CCCCCCCCC(O)=O OQCDKBAXFALNLD-UHFFFAOYSA-N 0.000 description 3
- 239000008117 stearic acid Substances 0.000 description 3
- UXVMQQNJUSDDNG-UHFFFAOYSA-L Calcium chloride Chemical compound [Cl-].[Cl-].[Ca+2] UXVMQQNJUSDDNG-UHFFFAOYSA-L 0.000 description 2
- 239000004908 Emulsion polymer Substances 0.000 description 2
- VZCYOOQTPOCHFL-OWOJBTEDSA-N Fumaric acid Chemical compound OC(=O)\C=C\C(O)=O VZCYOOQTPOCHFL-OWOJBTEDSA-N 0.000 description 2
- WYURNTSHIVDZCO-UHFFFAOYSA-N Tetrahydrofuran Chemical compound C1CCOC1 WYURNTSHIVDZCO-UHFFFAOYSA-N 0.000 description 2
- XTXRWKRVRITETP-UHFFFAOYSA-N Vinyl acetate Chemical compound CC(=O)OC=C XTXRWKRVRITETP-UHFFFAOYSA-N 0.000 description 2
- 239000013556 antirust agent Substances 0.000 description 2
- WDIHJSXYQDMJHN-UHFFFAOYSA-L barium chloride Chemical compound [Cl-].[Cl-].[Ba+2] WDIHJSXYQDMJHN-UHFFFAOYSA-L 0.000 description 2
- 229910001626 barium chloride Inorganic materials 0.000 description 2
- 239000001110 calcium chloride Substances 0.000 description 2
- 229910001628 calcium chloride Inorganic materials 0.000 description 2
- 239000000839 emulsion Substances 0.000 description 2
- 239000000835 fiber Substances 0.000 description 2
- 238000009472 formulation Methods 0.000 description 2
- 238000010438 heat treatment Methods 0.000 description 2
- 229910052757 nitrogen Inorganic materials 0.000 description 2
- 239000002667 nucleating agent Substances 0.000 description 2
- SRSFOMHQIATOFV-UHFFFAOYSA-N octanoyl octaneperoxoate Chemical compound CCCCCCCC(=O)OOC(=O)CCCCCCC SRSFOMHQIATOFV-UHFFFAOYSA-N 0.000 description 2
- 230000005855 radiation Effects 0.000 description 2
- 238000002390 rotary evaporation Methods 0.000 description 2
- OEPOKWHJYJXUGD-UHFFFAOYSA-N 2-(3-phenylmethoxyphenyl)-1,3-thiazole-4-carbaldehyde Chemical compound O=CC1=CSC(C=2C=C(OCC=3C=CC=CC=3)C=CC=2)=N1 OEPOKWHJYJXUGD-UHFFFAOYSA-N 0.000 description 1
- SKIIKRJAQOSWFT-UHFFFAOYSA-N 2-[3-[1-(2,2-difluoroethyl)piperidin-4-yl]oxy-4-[2-(2,3-dihydro-1H-inden-2-ylamino)pyrimidin-5-yl]pyrazol-1-yl]-1-(2,4,6,7-tetrahydrotriazolo[4,5-c]pyridin-5-yl)ethanone Chemical compound FC(CN1CCC(CC1)OC1=NN(C=C1C=1C=NC(=NC=1)NC1CC2=CC=CC=C2C1)CC(=O)N1CC2=C(CC1)NN=N2)F SKIIKRJAQOSWFT-UHFFFAOYSA-N 0.000 description 1
- WSSSPWUEQFSQQG-UHFFFAOYSA-N 4-methyl-1-pentene Chemical compound CC(C)CC=C WSSSPWUEQFSQQG-UHFFFAOYSA-N 0.000 description 1
- DEXFNLNNUZKHNO-UHFFFAOYSA-N 6-[3-[4-[2-(2,3-dihydro-1H-inden-2-ylamino)pyrimidin-5-yl]piperidin-1-yl]-3-oxopropyl]-3H-1,3-benzoxazol-2-one Chemical compound C1C(CC2=CC=CC=C12)NC1=NC=C(C=N1)C1CCN(CC1)C(CCC1=CC2=C(NC(O2)=O)C=C1)=O DEXFNLNNUZKHNO-UHFFFAOYSA-N 0.000 description 1
- NLHHRLWOUZZQLW-UHFFFAOYSA-N Acrylonitrile Chemical compound C=CC#N NLHHRLWOUZZQLW-UHFFFAOYSA-N 0.000 description 1
- VEXZGXHMUGYJMC-UHFFFAOYSA-M Chloride anion Chemical compound [Cl-] VEXZGXHMUGYJMC-UHFFFAOYSA-M 0.000 description 1
- RYGMFSIKBFXOCR-UHFFFAOYSA-N Copper Chemical compound [Cu] RYGMFSIKBFXOCR-UHFFFAOYSA-N 0.000 description 1
- CERQOIWHTDAKMF-UHFFFAOYSA-M Methacrylate Chemical compound CC(=C)C([O-])=O CERQOIWHTDAKMF-UHFFFAOYSA-M 0.000 description 1
- 241000158147 Sator Species 0.000 description 1
- 229920002433 Vinyl chloride-vinyl acetate copolymer Polymers 0.000 description 1
- 241000607479 Yersinia pestis Species 0.000 description 1
- NIXOWILDQLNWCW-UHFFFAOYSA-N acrylic acid group Chemical group C(C=C)(=O)O NIXOWILDQLNWCW-UHFFFAOYSA-N 0.000 description 1
- 238000013019 agitation Methods 0.000 description 1
- 150000001336 alkenes Chemical class 0.000 description 1
- 150000008055 alkyl aryl sulfonates Chemical class 0.000 description 1
- 229940088990 ammonium stearate Drugs 0.000 description 1
- JPNZKPRONVOMLL-UHFFFAOYSA-N azane;octadecanoic acid Chemical compound [NH4+].CCCCCCCCCCCCCCCCCC([O-])=O JPNZKPRONVOMLL-UHFFFAOYSA-N 0.000 description 1
- 244000052616 bacterial pathogen Species 0.000 description 1
- 238000005452 bending Methods 0.000 description 1
- 238000004364 calculation method Methods 0.000 description 1
- 238000005266 casting Methods 0.000 description 1
- 239000003054 catalyst Substances 0.000 description 1
- HGAZMNJKRQFZKS-UHFFFAOYSA-N chloroethene;ethenyl acetate Chemical compound ClC=C.CC(=O)OC=C HGAZMNJKRQFZKS-UHFFFAOYSA-N 0.000 description 1
- 238000007906 compression Methods 0.000 description 1
- 230000006835 compression Effects 0.000 description 1
- 150000004696 coordination complex Chemical class 0.000 description 1
- 229910052802 copper Inorganic materials 0.000 description 1
- 239000010949 copper Substances 0.000 description 1
- 239000002178 crystalline material Substances 0.000 description 1
- 238000002050 diffraction method Methods 0.000 description 1
- 239000002270 dispersing agent Substances 0.000 description 1
- 238000009826 distribution Methods 0.000 description 1
- POULHZVOKOAJMA-UHFFFAOYSA-M dodecanoate Chemical compound CCCCCCCCCCCC([O-])=O POULHZVOKOAJMA-UHFFFAOYSA-M 0.000 description 1
- 238000004945 emulsification Methods 0.000 description 1
- -1 ethylene, propylene, isobutene Chemical class 0.000 description 1
- 238000002474 experimental method Methods 0.000 description 1
- 239000001530 fumaric acid Substances 0.000 description 1
- 239000011521 glass Substances 0.000 description 1
- 239000001866 hydroxypropyl methyl cellulose Substances 0.000 description 1
- 229920003088 hydroxypropyl methyl cellulose Polymers 0.000 description 1
- UFVKGYZPFZQRLF-UHFFFAOYSA-N hydroxypropyl methyl cellulose Chemical compound OC1C(O)C(OC)OC(CO)C1OC1C(O)C(O)C(OC2C(C(O)C(OC3C(C(O)C(O)C(CO)O3)O)C(CO)O2)O)C(CO)O1 UFVKGYZPFZQRLF-UHFFFAOYSA-N 0.000 description 1
- 235000010979 hydroxypropyl methyl cellulose Nutrition 0.000 description 1
- 238000007373 indentation Methods 0.000 description 1
- 229940070765 laurate Drugs 0.000 description 1
- 150000002688 maleic acid derivatives Chemical class 0.000 description 1
- 238000005259 measurement Methods 0.000 description 1
- 229910052751 metal Inorganic materials 0.000 description 1
- 239000002184 metal Substances 0.000 description 1
- 125000005397 methacrylic acid ester group Chemical group 0.000 description 1
- 125000002496 methyl group Chemical group [H]C([H])([H])* 0.000 description 1
- 239000000575 pesticide Substances 0.000 description 1
- 229920003023 plastic Polymers 0.000 description 1
- 239000004033 plastic Substances 0.000 description 1
- 229920000058 polyacrylate Polymers 0.000 description 1
- 239000003505 polymerization initiator Substances 0.000 description 1
- 238000002360 preparation method Methods 0.000 description 1
- 238000003825 pressing Methods 0.000 description 1
- 238000012545 processing Methods 0.000 description 1
- 239000000376 reactant Substances 0.000 description 1
- 230000001105 regulatory effect Effects 0.000 description 1
- 238000009864 tensile test Methods 0.000 description 1
- YLQBMQCUIZJEEH-UHFFFAOYSA-N tetrahydrofuran Natural products C=1C=COC=1 YLQBMQCUIZJEEH-UHFFFAOYSA-N 0.000 description 1
- 239000010409 thin film Substances 0.000 description 1
- VZCYOOQTPOCHFL-UHFFFAOYSA-N trans-butenedioic acid Natural products OC(=O)C=CC(O)=O VZCYOOQTPOCHFL-UHFFFAOYSA-N 0.000 description 1
- 238000001291 vacuum drying Methods 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
- C08F259/00—Macromolecular compounds obtained by polymerising monomers on to polymers of halogen containing monomers as defined in group C08F14/00
- C08F259/02—Macromolecular compounds obtained by polymerising monomers on to polymers of halogen containing monomers as defined in group C08F14/00 on to polymers containing chlorine
- C08F259/04—Macromolecular compounds obtained by polymerising monomers on to polymers of halogen containing monomers as defined in group C08F14/00 on to polymers containing chlorine on to polymers of vinyl chloride
Landscapes
- Chemical & Material Sciences (AREA)
- Health & Medical Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Organic Chemistry (AREA)
- Addition Polymer Or Copolymer, Post-Treatments, Or Chemical Modifications (AREA)
- Polymerisation Methods In General (AREA)
- Compositions Of Macromolecular Compounds (AREA)
- Graft Or Block Polymers (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| GB1039671A GB1378391A (en) | 1971-04-21 | 1971-04-21 | Polymerisation process making same |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| DE2219402A1 true DE2219402A1 (de) | 1972-11-02 |
Family
ID=9967050
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DE19722219402 Pending DE2219402A1 (de) | 1971-04-21 | 1972-04-20 | Verfahren zur Herstellung von Vinylchloridpolymerisaten |
Country Status (13)
| Country | Link |
|---|---|
| US (1) | US3856767A (enExample) |
| BE (1) | BE782523A (enExample) |
| CA (1) | CA984547A (enExample) |
| CH (1) | CH537958A (enExample) |
| DD (1) | DD98291A5 (enExample) |
| DE (1) | DE2219402A1 (enExample) |
| ES (1) | ES401914A1 (enExample) |
| FR (1) | FR2133994B1 (enExample) |
| GB (1) | GB1378391A (enExample) |
| IT (1) | IT953325B (enExample) |
| NL (1) | NL7205408A (enExample) |
| SE (1) | SE400297B (enExample) |
| ZA (1) | ZA722579B (enExample) |
Families Citing this family (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4093794A (en) * | 1972-07-21 | 1978-06-06 | Plastimer | Process for the polymerization of vinyl chloride |
| US4031299A (en) * | 1975-04-11 | 1977-06-21 | Stauffer Chemical Company | Process for forming a polyvinyl chloride extender resin by incorporating in the suspension polymerization medium a prehomogenized solution of a polyallyl compound and a low molecular polymer of propylene |
| NO841494L (no) * | 1983-04-21 | 1984-10-22 | Conoco Inc | Fremgangsmaate for fremstilling av pvc-harpiks |
| ATE283291T1 (de) * | 2001-06-15 | 2004-12-15 | Saudi Basic Ind Corp | Verfahren zur herstellung von hautfreiem pvc |
Family Cites Families (11)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| NL99445C (enExample) * | 1957-10-30 | |||
| GB931629A (en) * | 1959-07-11 | 1963-07-17 | Distillers Co Yeast Ltd | Vinyl chloride polymerisation process |
| GB1050625A (enExample) * | 1962-12-21 | |||
| US3380946A (en) * | 1965-10-22 | 1968-04-30 | Pittsburgh Plate Glass Co | Polymerization using peroxycarbonate esters with salts of sulfurous acid |
| FR1483020A (fr) * | 1966-04-22 | 1967-06-02 | Pechiney Saint Gobain | Perfectionnement à la préparation en suspension de polymères et de copolymères à base de chlorure de vinyle, et produits en résultant |
| US3523111A (en) * | 1967-08-18 | 1970-08-04 | Monsanto Co | Emulsion polymerization of vinyl chloride with redox initiator system components and emulsifier prepared before monomer addition |
| US3520867A (en) * | 1967-09-28 | 1970-07-21 | Chatillon Italiana Fibre | Process for the polymerization of vinyl chloride |
| FR1574734A (enExample) * | 1968-03-05 | 1969-07-18 | ||
| US3652525A (en) * | 1968-06-17 | 1972-03-28 | Sumitomo Chemical Co | Method for producing polyvinylchloride particles |
| GB1304517A (enExample) * | 1969-05-19 | 1973-01-24 | ||
| DE1942823B2 (de) * | 1969-08-22 | 1971-06-16 | Badische Anilin & Soda Fabrik AG, 6700 Ludwigshafen | Verfahren zur herstellung von vinylchlorid polymerisaten |
-
1971
- 1971-04-21 GB GB1039671A patent/GB1378391A/en not_active Expired
-
1972
- 1972-04-17 ZA ZA722579A patent/ZA722579B/xx unknown
- 1972-04-18 SE SE7205027A patent/SE400297B/xx unknown
- 1972-04-18 US US00245193A patent/US3856767A/en not_active Expired - Lifetime
- 1972-04-19 ES ES401914A patent/ES401914A1/es not_active Expired
- 1972-04-20 CH CH584772A patent/CH537958A/fr not_active IP Right Cessation
- 1972-04-20 CA CA140,095A patent/CA984547A/en not_active Expired
- 1972-04-20 IT IT7288/72A patent/IT953325B/it active
- 1972-04-20 DE DE19722219402 patent/DE2219402A1/de active Pending
- 1972-04-21 NL NL7205408A patent/NL7205408A/xx not_active Application Discontinuation
- 1972-04-21 DD DD162502A patent/DD98291A5/xx unknown
- 1972-04-21 FR FR7214114A patent/FR2133994B1/fr not_active Expired
- 1972-04-21 BE BE782523A patent/BE782523A/xx unknown
Also Published As
| Publication number | Publication date |
|---|---|
| FR2133994B1 (enExample) | 1976-10-29 |
| NL7205408A (enExample) | 1972-10-24 |
| ES401914A1 (es) | 1975-04-16 |
| US3856767A (en) | 1974-12-24 |
| BE782523A (fr) | 1972-10-23 |
| SE400297B (sv) | 1978-03-20 |
| CA984547A (en) | 1976-02-24 |
| AU4138372A (en) | 1973-10-25 |
| CH537958A (fr) | 1973-06-15 |
| ZA722579B (en) | 1973-11-28 |
| GB1378391A (en) | 1974-12-27 |
| IT953325B (it) | 1973-08-10 |
| FR2133994A1 (enExample) | 1972-12-01 |
| DD98291A5 (enExample) | 1973-06-12 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| OHW | Rejection |