DE2124864B2 - Galvanisierverfahren und Einrichtung zur Durchführung des Verfahrens - Google Patents
Galvanisierverfahren und Einrichtung zur Durchführung des VerfahrensInfo
- Publication number
- DE2124864B2 DE2124864B2 DE2124864A DE2124864A DE2124864B2 DE 2124864 B2 DE2124864 B2 DE 2124864B2 DE 2124864 A DE2124864 A DE 2124864A DE 2124864 A DE2124864 A DE 2124864A DE 2124864 B2 DE2124864 B2 DE 2124864B2
- Authority
- DE
- Germany
- Prior art keywords
- liquid
- bath
- water
- solution
- amount
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Ceased
Links
- 238000009713 electroplating Methods 0.000 title claims description 35
- 238000000034 method Methods 0.000 title claims description 31
- 230000008569 process Effects 0.000 title claims description 16
- 239000007788 liquid Substances 0.000 claims description 55
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 43
- 239000007789 gas Substances 0.000 claims description 24
- 238000003860 storage Methods 0.000 claims description 23
- 238000012856 packing Methods 0.000 claims description 21
- 239000000126 substance Substances 0.000 claims description 18
- 238000005406 washing Methods 0.000 claims description 13
- 239000003595 mist Substances 0.000 claims description 9
- VYZAMTAEIAYCRO-UHFFFAOYSA-N Chromium Chemical compound [Cr] VYZAMTAEIAYCRO-UHFFFAOYSA-N 0.000 claims description 8
- 150000001768 cations Chemical class 0.000 claims description 8
- 238000001704 evaporation Methods 0.000 claims description 6
- 239000000203 mixture Substances 0.000 claims description 6
- NWUYHJFMYQTDRP-UHFFFAOYSA-N 1,2-bis(ethenyl)benzene;1-ethenyl-2-ethylbenzene;styrene Chemical compound C=CC1=CC=CC=C1.CCC1=CC=CC=C1C=C.C=CC1=CC=CC=C1C=C NWUYHJFMYQTDRP-UHFFFAOYSA-N 0.000 claims description 4
- 229910052804 chromium Inorganic materials 0.000 claims description 4
- 239000011651 chromium Substances 0.000 claims description 4
- 239000003729 cation exchange resin Substances 0.000 claims description 3
- 239000011347 resin Substances 0.000 claims description 3
- 229920005989 resin Polymers 0.000 claims description 3
- 238000005341 cation exchange Methods 0.000 claims 1
- 239000003795 chemical substances by application Substances 0.000 claims 1
- 238000010438 heat treatment Methods 0.000 claims 1
- 239000003960 organic solvent Substances 0.000 claims 1
- 238000005507 spraying Methods 0.000 claims 1
- 239000003643 water by type Substances 0.000 claims 1
- 239000000243 solution Substances 0.000 description 55
- 239000008237 rinsing water Substances 0.000 description 13
- 239000007921 spray Substances 0.000 description 13
- 229910000831 Steel Inorganic materials 0.000 description 10
- 238000004140 cleaning Methods 0.000 description 10
- 239000010959 steel Substances 0.000 description 10
- 239000000463 material Substances 0.000 description 9
- 239000013505 freshwater Substances 0.000 description 6
- 238000012544 monitoring process Methods 0.000 description 5
- 239000003792 electrolyte Substances 0.000 description 4
- 238000000605 extraction Methods 0.000 description 4
- 238000007747 plating Methods 0.000 description 4
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 description 3
- 230000009471 action Effects 0.000 description 3
- 230000008901 benefit Effects 0.000 description 3
- 229910052799 carbon Inorganic materials 0.000 description 3
- 238000001816 cooling Methods 0.000 description 3
- 230000008020 evaporation Effects 0.000 description 3
- 238000011010 flushing procedure Methods 0.000 description 3
- 238000005246 galvanizing Methods 0.000 description 3
- 150000002500 ions Chemical class 0.000 description 3
- 238000011084 recovery Methods 0.000 description 3
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 2
- 229910000975 Carbon steel Inorganic materials 0.000 description 2
- IMNFDUFMRHMDMM-UHFFFAOYSA-N N-Heptane Chemical compound CCCCCCC IMNFDUFMRHMDMM-UHFFFAOYSA-N 0.000 description 2
- 239000010962 carbon steel Substances 0.000 description 2
- 238000006243 chemical reaction Methods 0.000 description 2
- 239000003153 chemical reaction reagent Substances 0.000 description 2
- KRVSOGSZCMJSLX-UHFFFAOYSA-L chromic acid Substances O[Cr](O)(=O)=O KRVSOGSZCMJSLX-UHFFFAOYSA-L 0.000 description 2
- 238000005260 corrosion Methods 0.000 description 2
- 230000007797 corrosion Effects 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- 238000005868 electrolysis reaction Methods 0.000 description 2
- 238000003912 environmental pollution Methods 0.000 description 2
- 239000000945 filler Substances 0.000 description 2
- AWJWCTOOIBYHON-UHFFFAOYSA-N furo[3,4-b]pyrazine-5,7-dione Chemical compound C1=CN=C2C(=O)OC(=O)C2=N1 AWJWCTOOIBYHON-UHFFFAOYSA-N 0.000 description 2
- 238000005342 ion exchange Methods 0.000 description 2
- 238000000926 separation method Methods 0.000 description 2
- 101150096316 5 gene Proteins 0.000 description 1
- KRHYYFGTRYWZRS-UHFFFAOYSA-M Fluoride anion Chemical compound [F-] KRHYYFGTRYWZRS-UHFFFAOYSA-M 0.000 description 1
- 229910001335 Galvanized steel Inorganic materials 0.000 description 1
- QAOWNCQODCNURD-UHFFFAOYSA-L Sulfate Chemical compound [O-]S([O-])(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-L 0.000 description 1
- ATJFFYVFTNAWJD-UHFFFAOYSA-N Tin Chemical compound [Sn] ATJFFYVFTNAWJD-UHFFFAOYSA-N 0.000 description 1
- RTAQQCXQSZGOHL-UHFFFAOYSA-N Titanium Chemical compound [Ti] RTAQQCXQSZGOHL-UHFFFAOYSA-N 0.000 description 1
- 229910045601 alloy Inorganic materials 0.000 description 1
- 239000000956 alloy Substances 0.000 description 1
- 229910052787 antimony Inorganic materials 0.000 description 1
- WATWJIUSRGPENY-UHFFFAOYSA-N antimony atom Chemical compound [Sb] WATWJIUSRGPENY-UHFFFAOYSA-N 0.000 description 1
- 230000033228 biological regulation Effects 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 235000015895 biscuits Nutrition 0.000 description 1
- 239000003054 catalyst Substances 0.000 description 1
- JOPOVCBBYLSVDA-UHFFFAOYSA-N chromium(6+) Chemical compound [Cr+6] JOPOVCBBYLSVDA-UHFFFAOYSA-N 0.000 description 1
- 238000009833 condensation Methods 0.000 description 1
- 230000005494 condensation Effects 0.000 description 1
- 239000000356 contaminant Substances 0.000 description 1
- 238000010924 continuous production Methods 0.000 description 1
- 230000007423 decrease Effects 0.000 description 1
- 238000007599 discharging Methods 0.000 description 1
- 238000009826 distribution Methods 0.000 description 1
- 238000001035 drying Methods 0.000 description 1
- 239000008151 electrolyte solution Substances 0.000 description 1
- CJMZLCRLBNZJQR-UHFFFAOYSA-N ethyl 2-amino-4-(4-fluorophenyl)thiophene-3-carboxylate Chemical compound CCOC(=O)C1=C(N)SC=C1C1=CC=C(F)C=C1 CJMZLCRLBNZJQR-UHFFFAOYSA-N 0.000 description 1
- 239000004744 fabric Substances 0.000 description 1
- 239000000446 fuel Substances 0.000 description 1
- 239000008397 galvanized steel Substances 0.000 description 1
- 239000011521 glass Substances 0.000 description 1
- 229910002804 graphite Inorganic materials 0.000 description 1
- 239000010439 graphite Substances 0.000 description 1
- 230000005484 gravity Effects 0.000 description 1
- 238000007654 immersion Methods 0.000 description 1
- 239000003456 ion exchange resin Substances 0.000 description 1
- 229920003303 ion-exchange polymer Polymers 0.000 description 1
- 229910052742 iron Inorganic materials 0.000 description 1
- 230000007935 neutral effect Effects 0.000 description 1
- 231100000252 nontoxic Toxicity 0.000 description 1
- 230000003000 nontoxic effect Effects 0.000 description 1
- 238000005192 partition Methods 0.000 description 1
- 230000000737 periodic effect Effects 0.000 description 1
- 231100000614 poison Toxicity 0.000 description 1
- 230000007096 poisonous effect Effects 0.000 description 1
- 229920001467 poly(styrenesulfonates) Polymers 0.000 description 1
- 229920000915 polyvinyl chloride Polymers 0.000 description 1
- 239000004800 polyvinyl chloride Substances 0.000 description 1
- 230000009467 reduction Effects 0.000 description 1
- 230000000284 resting effect Effects 0.000 description 1
- 239000012487 rinsing solution Substances 0.000 description 1
- 229910052709 silver Inorganic materials 0.000 description 1
- 239000004332 silver Substances 0.000 description 1
- 239000010935 stainless steel Substances 0.000 description 1
- 229910001220 stainless steel Inorganic materials 0.000 description 1
- 150000003459 sulfonic acid esters Chemical class 0.000 description 1
- 239000000057 synthetic resin Substances 0.000 description 1
- 229920003002 synthetic resin Polymers 0.000 description 1
- 239000010936 titanium Substances 0.000 description 1
- 229910052719 titanium Inorganic materials 0.000 description 1
- 230000007704 transition Effects 0.000 description 1
- 238000011144 upstream manufacturing Methods 0.000 description 1
- 230000008016 vaporization Effects 0.000 description 1
- 239000002699 waste material Substances 0.000 description 1
- 238000010626 work up procedure Methods 0.000 description 1
- 239000012224 working solution Substances 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C25—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES; APPARATUS THEREFOR
- C25D—PROCESSES FOR THE ELECTROLYTIC OR ELECTROPHORETIC PRODUCTION OF COATINGS; ELECTROFORMING; APPARATUS THEREFOR
- C25D21/00—Processes for servicing or operating cells for electrolytic coating
- C25D21/16—Regeneration of process solutions
- C25D21/18—Regeneration of process solutions of electrolytes
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10S—TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10S204/00—Chemistry: electrical and wave energy
- Y10S204/13—Purification and treatment of electroplating baths and plating wastes
Landscapes
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Electrochemistry (AREA)
- Materials Engineering (AREA)
- Metallurgy (AREA)
- Organic Chemistry (AREA)
- Electroplating Methods And Accessories (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US4243570A | 1970-06-01 | 1970-06-01 |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| DE2124864A1 DE2124864A1 (de) | 1971-12-09 |
| DE2124864B2 true DE2124864B2 (de) | 1974-08-08 |
Family
ID=21921927
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DE2124864A Ceased DE2124864B2 (de) | 1970-06-01 | 1971-05-19 | Galvanisierverfahren und Einrichtung zur Durchführung des Verfahrens |
Country Status (7)
| Country | Link |
|---|---|
| US (1) | US3661732A (fr) |
| JP (1) | JPS558599B1 (fr) |
| BE (1) | BE762293A (fr) |
| CA (1) | CA923068A (fr) |
| DE (1) | DE2124864B2 (fr) |
| FR (1) | FR2093929B1 (fr) |
| GB (1) | GB1320645A (fr) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE2914722A1 (de) * | 1979-04-11 | 1980-10-16 | Langbein Pfanhauser Werke Ag | Anlage fuer die galvanotechnische behandlung von gegenstaenden |
Families Citing this family (21)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3903237A (en) * | 1973-06-04 | 1975-09-02 | Nat Steel Corp | Recovering hexavalent chromium for reuse |
| US3950216A (en) * | 1974-01-18 | 1976-04-13 | The United States Of America As Represented By The United States Energy Research And Development Administration | Falling film evaporator |
| US4163705A (en) * | 1975-05-06 | 1979-08-07 | Korpi Teuvo Tapio | Apparatus for chemical and electrochemical treatment |
| US3985628A (en) * | 1975-08-04 | 1976-10-12 | Myers Lyle R | Pollution control in electroplating systems |
| PL111516B1 (en) * | 1976-03-08 | 1980-09-30 | Process for metals recovery with simultaneous neutralization of toxic aqueous wastes,concentrated plating solution and toxic vapours in ventilation systems and apparatus therefor | |
| US4171255A (en) * | 1977-02-18 | 1979-10-16 | Instytut Mechaniki Precyzyjnes | Apparatus for recovery of metals from metal plating baths and neutralizing toxic effluents therefrom |
| FR2426098A1 (fr) * | 1978-05-17 | 1979-12-14 | Zindel Laurent | Procede et installation de traitement d'articles dans un bain contenant des produits de traitement polluants, en particulier de traitement de zincage |
| US4409064A (en) * | 1978-10-16 | 1983-10-11 | Air Products And Chemicals, Inc. | Process for concentrating sulfuric acid in an evaporator |
| US4340451A (en) * | 1979-12-17 | 1982-07-20 | Bell Telephone Laboratories, Incorporated | Method of replenishing gold/in plating baths |
| JPS57145999A (en) * | 1981-03-03 | 1982-09-09 | Yamaha Motor Co Ltd | Plating device |
| CA1295283C (fr) * | 1985-10-11 | 1992-02-04 | Dominic Tenace | Systeme de galvaniplastie avec evaporateur et bac de rincage pour effluent contamine |
| US4781806A (en) * | 1985-10-11 | 1988-11-01 | Dominic Tenace | Electroplating system |
| US5269905A (en) * | 1990-04-30 | 1993-12-14 | Elf Atochem North America, Inc. | Apparatus and process to regenerate a trivalent chromium bath |
| US5401379A (en) * | 1993-03-19 | 1995-03-28 | Mazzochi; James L. | Chrome plating process |
| JP2918832B2 (ja) * | 1995-12-15 | 1999-07-12 | 日英ハードクローム工業株式会社 | クロムめっきにおけるクロムめっき液、クロムめっき廃液、クロム酸洗浄水用クローズド・リサイクル・システム |
| US20030064158A1 (en) * | 2001-10-03 | 2003-04-03 | Thirkeldsen C. G. | Method and apparatus for improving corrosion resistance of chrome plated material |
| US6808751B2 (en) * | 2001-10-03 | 2004-10-26 | Industrial Hard Chrome | Method for improving corrosion resistance of chrome plated material |
| FR2847761B1 (fr) * | 2002-11-27 | 2005-02-04 | Framatome Connectors Int | Dispositif de metallisation de formes imprimees munies de pistes conductrices d'electricite et procede de metallisation associe |
| DE102007036651A1 (de) * | 2007-07-25 | 2009-01-29 | A.C.K. Aqua Concept Gmbh Karlsruhe | Prozessrecycling galvanischer Bäder |
| US8366884B2 (en) * | 2008-04-30 | 2013-02-05 | Alcatel Lucent | Plating apparatus with direct electrolyte distribution system |
| CN110965114B (zh) * | 2018-09-29 | 2021-12-14 | 上海梅山钢铁股份有限公司 | 一种甲基磺酸锡系电镀液的回收装置及方法 |
Family Cites Families (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US857927A (en) * | 1906-04-18 | 1907-06-25 | Ontario Nickel Company Ltd | Process of recovering the nickel contained in basic nickel precipitates. |
| US1012809A (en) * | 1911-05-10 | 1911-12-26 | Chloride Process Company | Apparatus for purifying water. |
| BE485185A (fr) * | 1942-02-27 | |||
| US2430750A (en) * | 1944-07-18 | 1947-11-11 | United Chromium Inc | Method of electroplating to produce fissure network chromium plating |
| FR1395008A (fr) * | 1964-02-28 | 1965-04-09 | Cuve de traitement, notamment pour le chromage électrolytique | |
| US3616304A (en) * | 1966-01-26 | 1971-10-26 | M & T Chemicals Inc | Method for treating chromium-containing baths |
| BE683946A (fr) * | 1966-07-11 | 1966-12-16 | ||
| US3485743A (en) * | 1967-07-21 | 1969-12-23 | Girdler Corp | Apparatus for removal of acidic gases from gaseous atmospheres |
-
1970
- 1970-06-01 US US42435A patent/US3661732A/en not_active Expired - Lifetime
- 1970-12-31 CA CA101817A patent/CA923068A/en not_active Expired
-
1971
- 1971-01-29 BE BE762293A patent/BE762293A/fr unknown
- 1971-03-01 JP JP1055471A patent/JPS558599B1/ja active Pending
- 1971-04-19 GB GB2120271A patent/GB1320645A/en not_active Expired
- 1971-04-22 FR FR717114332A patent/FR2093929B1/fr not_active Expired
- 1971-05-19 DE DE2124864A patent/DE2124864B2/de not_active Ceased
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE2914722A1 (de) * | 1979-04-11 | 1980-10-16 | Langbein Pfanhauser Werke Ag | Anlage fuer die galvanotechnische behandlung von gegenstaenden |
Also Published As
| Publication number | Publication date |
|---|---|
| BE762293A (fr) | 1971-07-01 |
| FR2093929B1 (fr) | 1974-02-15 |
| US3661732A (en) | 1972-05-09 |
| FR2093929A1 (fr) | 1972-02-04 |
| CA923068A (en) | 1973-03-20 |
| DE2124864A1 (de) | 1971-12-09 |
| JPS558599B1 (fr) | 1980-03-05 |
| GB1320645A (en) | 1973-06-20 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| BHV | Refusal |