DE2061111C2 - Kontinuierliches Verfahren zum Kristallisieren von Lösungsmittel aus einer Lösung - Google Patents
Kontinuierliches Verfahren zum Kristallisieren von Lösungsmittel aus einer LösungInfo
- Publication number
- DE2061111C2 DE2061111C2 DE2061111A DE2061111A DE2061111C2 DE 2061111 C2 DE2061111 C2 DE 2061111C2 DE 2061111 A DE2061111 A DE 2061111A DE 2061111 A DE2061111 A DE 2061111A DE 2061111 C2 DE2061111 C2 DE 2061111C2
- Authority
- DE
- Germany
- Prior art keywords
- zone
- crystal
- recrystallization
- crystals
- solution
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- 239000002904 solvent Substances 0.000 title claims description 13
- 238000010924 continuous production Methods 0.000 title claims description 4
- 239000013078 crystal Substances 0.000 claims description 102
- 238000001953 recrystallisation Methods 0.000 claims description 49
- 238000002425 crystallisation Methods 0.000 claims description 26
- 238000000034 method Methods 0.000 claims description 26
- 230000008025 crystallization Effects 0.000 claims description 25
- 239000012452 mother liquor Substances 0.000 claims description 14
- 239000002002 slurry Substances 0.000 claims description 12
- 230000015572 biosynthetic process Effects 0.000 claims description 8
- 239000000243 solution Substances 0.000 description 24
- 230000006911 nucleation Effects 0.000 description 22
- 238000010899 nucleation Methods 0.000 description 22
- 238000001816 cooling Methods 0.000 description 7
- 230000007423 decrease Effects 0.000 description 7
- 244000052616 bacterial pathogen Species 0.000 description 5
- 239000012141 concentrate Substances 0.000 description 5
- 239000007788 liquid Substances 0.000 description 5
- 239000000725 suspension Substances 0.000 description 5
- 238000001704 evaporation Methods 0.000 description 4
- 230000008020 evaporation Effects 0.000 description 4
- 239000000126 substance Substances 0.000 description 4
- CZMRCDWAGMRECN-UGDNZRGBSA-N Sucrose Chemical compound O[C@H]1[C@H](O)[C@@H](CO)O[C@@]1(CO)O[C@@H]1[C@H](O)[C@@H](O)[C@H](O)[C@@H](CO)O1 CZMRCDWAGMRECN-UGDNZRGBSA-N 0.000 description 2
- 229930006000 Sucrose Natural products 0.000 description 2
- 230000001627 detrimental effect Effects 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- 238000000605 extraction Methods 0.000 description 2
- 230000008014 freezing Effects 0.000 description 2
- 238000007710 freezing Methods 0.000 description 2
- 230000002631 hypothermal effect Effects 0.000 description 2
- 239000007791 liquid phase Substances 0.000 description 2
- 238000004519 manufacturing process Methods 0.000 description 2
- 239000000203 mixture Substances 0.000 description 2
- 239000012266 salt solution Substances 0.000 description 2
- 238000000926 separation method Methods 0.000 description 2
- 239000007787 solid Substances 0.000 description 2
- 239000005720 sucrose Substances 0.000 description 2
- 238000005406 washing Methods 0.000 description 2
- 240000007594 Oryza sativa Species 0.000 description 1
- 235000007164 Oryza sativa Nutrition 0.000 description 1
- 238000005299 abrasion Methods 0.000 description 1
- 239000007864 aqueous solution Substances 0.000 description 1
- 239000011362 coarse particle Substances 0.000 description 1
- 239000002826 coolant Substances 0.000 description 1
- 238000009826 distribution Methods 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 238000010309 melting process Methods 0.000 description 1
- 238000002156 mixing Methods 0.000 description 1
- 235000021395 porridge Nutrition 0.000 description 1
- 235000009566 rice Nutrition 0.000 description 1
- 230000005070 ripening Effects 0.000 description 1
- 150000003839 salts Chemical class 0.000 description 1
- 238000006748 scratching Methods 0.000 description 1
- 230000002393 scratching effect Effects 0.000 description 1
- 230000002269 spontaneous effect Effects 0.000 description 1
- 238000003756 stirring Methods 0.000 description 1
- 238000003860 storage Methods 0.000 description 1
- 238000004781 supercooling Methods 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C13—SUGAR INDUSTRY
- C13B—PRODUCTION OF SUCROSE; APPARATUS SPECIALLY ADAPTED THEREFOR
- C13B30/00—Crystallisation; Crystallising apparatus; Separating crystals from mother liquors ; Evaporating or boiling sugar juice
- C13B30/02—Crystallisation; Crystallising apparatus
- C13B30/022—Continuous processes, apparatus therefor
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D9/00—Crystallisation
- B01D9/0004—Crystallisation cooling by heat exchange
- B01D9/0013—Crystallisation cooling by heat exchange by indirect heat exchange
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D9/00—Crystallisation
- B01D9/0018—Evaporation of components of the mixture to be separated
- B01D9/0031—Evaporation of components of the mixture to be separated by heating
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D9/00—Crystallisation
- B01D9/0036—Crystallisation on to a bed of product crystals; Seeding
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D9/00—Crystallisation
- B01D9/0059—General arrangements of crystallisation plant, e.g. flow sheets
Landscapes
- Chemical & Material Sciences (AREA)
- Crystallography & Structural Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Physics & Mathematics (AREA)
- Thermal Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Biochemistry (AREA)
- Organic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Paper (AREA)
- Saccharide Compounds (AREA)
- Enzymes And Modification Thereof (AREA)
- Peptides Or Proteins (AREA)
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| NL696918686A NL148242B (nl) | 1969-12-12 | 1969-12-12 | Werkwijze voor het uitvriezen van een oplosmiddel uit een oplossing. |
| NL7002961A NL7002961A (en) | 1970-03-02 | 1970-03-02 | Continuous crystalliser unit |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| DE2061111A1 DE2061111A1 (de) | 1971-06-24 |
| DE2061111C2 true DE2061111C2 (de) | 1982-07-15 |
Family
ID=26644500
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DE2061111A Expired DE2061111C2 (de) | 1969-12-12 | 1970-12-11 | Kontinuierliches Verfahren zum Kristallisieren von Lösungsmittel aus einer Lösung |
Country Status (15)
| Country | Link |
|---|---|
| JP (1) | JPS5651803B1 (enExample) |
| AT (1) | AT317850B (enExample) |
| BE (1) | BE760140A (enExample) |
| CA (1) | CA919578A (enExample) |
| CH (1) | CH524382A (enExample) |
| DE (1) | DE2061111C2 (enExample) |
| DK (1) | DK130047B (enExample) |
| ES (1) | ES386356A1 (enExample) |
| FR (1) | FR2073064A5 (enExample) |
| GB (1) | GB1322197A (enExample) |
| IL (1) | IL35793A (enExample) |
| LU (1) | LU62210A1 (enExample) |
| NO (1) | NO128252B (enExample) |
| OA (1) | OA03541A (enExample) |
| SE (1) | SE388362B (enExample) |
Families Citing this family (10)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE3270132D1 (en) * | 1982-09-23 | 1986-04-30 | Csm Suiker | Preparation of seeding crystals for massecuite |
| GB2180253B (en) * | 1985-09-10 | 1989-09-06 | Alfa Laval Food & Dairy Eng | Method and plant for cooling of fatty oils |
| IT1208310B (it) * | 1987-06-22 | 1989-06-12 | Eridania | Produzione di zucchero commerciale mediante cristallizzazione nontradizionale per raffreddamento da soluzioni zuccherine |
| US5695795A (en) | 1993-03-23 | 1997-12-09 | Labatt Brewing Company Limited | Methods for chill-treating non-distilled malted barley beverages |
| USRE36897E (en) | 1993-03-23 | 2000-10-03 | Labatt Brewing Company Limited | Methods for chill treating non-distilled malted barley beverages |
| US5304384A (en) | 1993-03-23 | 1994-04-19 | Labatt Brewing Company Limited | Improvements in production of fermented malt beverages |
| US5869114A (en) | 1994-03-18 | 1999-02-09 | Labatt Brewing Company Limited | Production of fermented malt beverages |
| DE10026619A1 (de) * | 2000-05-29 | 2001-12-06 | Basf Ag | Vorrichtung zur Herstellung von Kristallen |
| DE102005048881A1 (de) * | 2005-10-12 | 2007-04-19 | Forschungszentrum Karlsruhe Gmbh | Verfahren zur Lösungskristallisation von Stoffgemischen |
| CN114452673A (zh) * | 2022-01-29 | 2022-05-10 | 常州中源工程技术有限公司 | 连续冷冻结晶釜及其冷冻结晶装置 |
Family Cites Families (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE1286507B (de) * | 1962-05-14 | 1969-01-09 | Phillips Petroleum Co | Verfahren zum Konzentrieren eines aus mehreren Bestandteilen bestehenden fluessigen Materials |
-
1970
- 1970-12-04 IL IL35793A patent/IL35793A/en unknown
- 1970-12-08 FR FR7044093A patent/FR2073064A5/fr not_active Expired
- 1970-12-09 CH CH1819370A patent/CH524382A/de not_active IP Right Cessation
- 1970-12-10 LU LU62210D patent/LU62210A1/xx unknown
- 1970-12-10 BE BE760140A patent/BE760140A/xx not_active IP Right Cessation
- 1970-12-11 AT AT1119370A patent/AT317850B/de not_active IP Right Cessation
- 1970-12-11 SE SE7016829A patent/SE388362B/xx unknown
- 1970-12-11 GB GB5909270A patent/GB1322197A/en not_active Expired
- 1970-12-11 DE DE2061111A patent/DE2061111C2/de not_active Expired
- 1970-12-11 CA CA100396A patent/CA919578A/en not_active Expired
- 1970-12-11 JP JP11036570A patent/JPS5651803B1/ja active Pending
- 1970-12-11 DK DK631470AA patent/DK130047B/da not_active IP Right Cessation
- 1970-12-11 NO NO04785/70A patent/NO128252B/no unknown
- 1970-12-12 OA OA54114A patent/OA03541A/xx unknown
- 1970-12-29 ES ES386356A patent/ES386356A1/es not_active Expired
Also Published As
| Publication number | Publication date |
|---|---|
| CA919578A (en) | 1973-01-23 |
| NO128252B (enExample) | 1973-10-22 |
| FR2073064A5 (enExample) | 1971-09-24 |
| ES386356A1 (es) | 1973-03-16 |
| DK130047B (da) | 1974-12-16 |
| SE388362B (sv) | 1976-10-04 |
| IL35793A (en) | 1973-10-25 |
| GB1322197A (en) | 1973-07-04 |
| DE2061111A1 (de) | 1971-06-24 |
| IL35793A0 (en) | 1971-02-25 |
| LU62210A1 (enExample) | 1971-05-14 |
| BE760140A (fr) | 1971-06-10 |
| CH524382A (de) | 1972-06-30 |
| JPS5651803B1 (enExample) | 1981-12-08 |
| DK130047C (enExample) | 1975-05-26 |
| OA03541A (fr) | 1971-03-30 |
| AT317850B (de) | 1974-09-10 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| OGA | New person/name/address of the applicant | ||
| D2 | Grant after examination |