DE1949278C3 - Verfahren zur Vorbehandlung von Kunststoffteilen für das chemische und galvanische Metallisieren auf Gestellen - Google Patents
Verfahren zur Vorbehandlung von Kunststoffteilen für das chemische und galvanische Metallisieren auf GestellenInfo
- Publication number
- DE1949278C3 DE1949278C3 DE1949278A DE1949278A DE1949278C3 DE 1949278 C3 DE1949278 C3 DE 1949278C3 DE 1949278 A DE1949278 A DE 1949278A DE 1949278 A DE1949278 A DE 1949278A DE 1949278 C3 DE1949278 C3 DE 1949278C3
- Authority
- DE
- Germany
- Prior art keywords
- racks
- percent
- chemical
- pretreatment
- plastic parts
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- 239000004033 plastic Substances 0.000 title claims description 22
- 229920003023 plastic Polymers 0.000 title claims description 22
- 238000000034 method Methods 0.000 title claims description 16
- 239000000126 substance Substances 0.000 title claims description 10
- 238000001465 metallisation Methods 0.000 title description 3
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 claims description 20
- KDLHZDBZIXYQEI-UHFFFAOYSA-N Palladium Chemical compound [Pd] KDLHZDBZIXYQEI-UHFFFAOYSA-N 0.000 claims description 19
- KRVSOGSZCMJSLX-UHFFFAOYSA-L chromic acid Substances O[Cr](O)(=O)=O KRVSOGSZCMJSLX-UHFFFAOYSA-L 0.000 claims description 12
- AWJWCTOOIBYHON-UHFFFAOYSA-N furo[3,4-b]pyrazine-5,7-dione Chemical compound C1=CN=C2C(=O)OC(=O)C2=N1 AWJWCTOOIBYHON-UHFFFAOYSA-N 0.000 claims description 12
- 229910052763 palladium Inorganic materials 0.000 claims description 10
- BASFCYQUMIYNBI-UHFFFAOYSA-N platinum Chemical compound [Pt] BASFCYQUMIYNBI-UHFFFAOYSA-N 0.000 claims description 6
- 229920000642 polymer Polymers 0.000 claims description 6
- 229910000510 noble metal Inorganic materials 0.000 claims description 5
- 229910052697 platinum Inorganic materials 0.000 claims description 3
- 150000001805 chlorine compounds Chemical class 0.000 claims description 2
- 238000009713 electroplating Methods 0.000 claims description 2
- PCHJSUWPFVWCPO-UHFFFAOYSA-N gold Chemical compound [Au] PCHJSUWPFVWCPO-UHFFFAOYSA-N 0.000 claims description 2
- 229910052737 gold Inorganic materials 0.000 claims description 2
- 239000010931 gold Substances 0.000 claims description 2
- 229940100890 silver compound Drugs 0.000 claims 1
- 150000003379 silver compounds Chemical class 0.000 claims 1
- 239000000243 solution Substances 0.000 claims 1
- 230000004913 activation Effects 0.000 description 9
- 238000005554 pickling Methods 0.000 description 9
- -1 polypropylenes Polymers 0.000 description 9
- PXHVJJICTQNCMI-UHFFFAOYSA-N Nickel Chemical compound [Ni] PXHVJJICTQNCMI-UHFFFAOYSA-N 0.000 description 8
- 239000004743 Polypropylene Substances 0.000 description 8
- 239000004676 acrylonitrile butadiene styrene Substances 0.000 description 8
- 229920001155 polypropylene Polymers 0.000 description 8
- XECAHXYUAAWDEL-UHFFFAOYSA-N acrylonitrile butadiene styrene Chemical compound C=CC=C.C=CC#N.C=CC1=CC=CC=C1 XECAHXYUAAWDEL-UHFFFAOYSA-N 0.000 description 7
- 229920000122 acrylonitrile butadiene styrene Polymers 0.000 description 7
- 229910052751 metal Inorganic materials 0.000 description 7
- 239000002184 metal Substances 0.000 description 7
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 7
- KRKNYBCHXYNGOX-UHFFFAOYSA-N citric acid Chemical compound OC(=O)CC(O)(C(O)=O)CC(O)=O KRKNYBCHXYNGOX-UHFFFAOYSA-N 0.000 description 6
- 238000009413 insulation Methods 0.000 description 5
- 230000000694 effects Effects 0.000 description 4
- 229910052759 nickel Inorganic materials 0.000 description 4
- WSFSSNUMVMOOMR-UHFFFAOYSA-N Formaldehyde Chemical compound O=C WSFSSNUMVMOOMR-UHFFFAOYSA-N 0.000 description 3
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 3
- QAOWNCQODCNURD-UHFFFAOYSA-L Sulfate Chemical compound [O-]S([O-])(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-L 0.000 description 3
- 238000006243 chemical reaction Methods 0.000 description 3
- 239000003638 chemical reducing agent Substances 0.000 description 3
- 229910052802 copper Inorganic materials 0.000 description 3
- NWZSZGALRFJKBT-KNIFDHDWSA-N (2s)-2,6-diaminohexanoic acid;(2s)-2-hydroxybutanedioic acid Chemical compound OC(=O)[C@@H](O)CC(O)=O.NCCCC[C@H](N)C(O)=O NWZSZGALRFJKBT-KNIFDHDWSA-N 0.000 description 2
- KWSLGOVYXMQPPX-UHFFFAOYSA-N 5-[3-(trifluoromethyl)phenyl]-2h-tetrazole Chemical compound FC(F)(F)C1=CC=CC(C2=NNN=N2)=C1 KWSLGOVYXMQPPX-UHFFFAOYSA-N 0.000 description 2
- VEXZGXHMUGYJMC-UHFFFAOYSA-M Chloride anion Chemical compound [Cl-] VEXZGXHMUGYJMC-UHFFFAOYSA-M 0.000 description 2
- ZAMOUSCENKQFHK-UHFFFAOYSA-N Chlorine atom Chemical compound [Cl] ZAMOUSCENKQFHK-UHFFFAOYSA-N 0.000 description 2
- RYGMFSIKBFXOCR-UHFFFAOYSA-N Copper Chemical compound [Cu] RYGMFSIKBFXOCR-UHFFFAOYSA-N 0.000 description 2
- BQCADISMDOOEFD-UHFFFAOYSA-N Silver Chemical compound [Ag] BQCADISMDOOEFD-UHFFFAOYSA-N 0.000 description 2
- 239000000460 chlorine Substances 0.000 description 2
- 229910052801 chlorine Inorganic materials 0.000 description 2
- GRWVQDDAKZFPFI-UHFFFAOYSA-H chromium(III) sulfate Chemical compound [Cr+3].[Cr+3].[O-]S([O-])(=O)=O.[O-]S([O-])(=O)=O.[O-]S([O-])(=O)=O GRWVQDDAKZFPFI-UHFFFAOYSA-H 0.000 description 2
- 230000000052 comparative effect Effects 0.000 description 2
- 239000010949 copper Substances 0.000 description 2
- 238000002474 experimental method Methods 0.000 description 2
- IKDUDTNKRLTJSI-UHFFFAOYSA-N hydrazine monohydrate Substances O.NN IKDUDTNKRLTJSI-UHFFFAOYSA-N 0.000 description 2
- LGQLOGILCSXPEA-UHFFFAOYSA-L nickel sulfate Chemical compound [Ni+2].[O-]S([O-])(=O)=O LGQLOGILCSXPEA-UHFFFAOYSA-L 0.000 description 2
- 229910000363 nickel(II) sulfate Inorganic materials 0.000 description 2
- 238000006722 reduction reaction Methods 0.000 description 2
- KIWUVOGUEXMXSV-UHFFFAOYSA-N rhodanine Chemical compound O=C1CSC(=S)N1 KIWUVOGUEXMXSV-UHFFFAOYSA-N 0.000 description 2
- 229910001379 sodium hypophosphite Inorganic materials 0.000 description 2
- 229910003803 Gold(III) chloride Inorganic materials 0.000 description 1
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 description 1
- 241000530268 Lycaena heteronea Species 0.000 description 1
- 241001465754 Metazoa Species 0.000 description 1
- 102100035031 Palladin Human genes 0.000 description 1
- 101710128215 Palladin Proteins 0.000 description 1
- 229930040373 Paraformaldehyde Natural products 0.000 description 1
- 239000004952 Polyamide Substances 0.000 description 1
- 150000001242 acetic acid derivatives Chemical class 0.000 description 1
- 230000003213 activating effect Effects 0.000 description 1
- 239000000853 adhesive Substances 0.000 description 1
- 230000001070 adhesive effect Effects 0.000 description 1
- 244000052616 bacterial pathogen Species 0.000 description 1
- 238000009835 boiling Methods 0.000 description 1
- 238000000576 coating method Methods 0.000 description 1
- 229920001577 copolymer Polymers 0.000 description 1
- RJHLTVSLYWWTEF-UHFFFAOYSA-K gold trichloride Chemical compound Cl[Au](Cl)Cl RJHLTVSLYWWTEF-UHFFFAOYSA-K 0.000 description 1
- 239000011256 inorganic filler Substances 0.000 description 1
- 229910003475 inorganic filler Inorganic materials 0.000 description 1
- 150000002500 ions Chemical class 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 229910001510 metal chloride Inorganic materials 0.000 description 1
- 150000002736 metal compounds Chemical class 0.000 description 1
- 150000002823 nitrates Chemical class 0.000 description 1
- 239000003960 organic solvent Substances 0.000 description 1
- 239000007800 oxidant agent Substances 0.000 description 1
- 230000003647 oxidation Effects 0.000 description 1
- 238000007254 oxidation reaction Methods 0.000 description 1
- GPNDARIEYHPYAY-UHFFFAOYSA-N palladium(ii) nitrate Chemical compound [Pd+2].[O-][N+]([O-])=O.[O-][N+]([O-])=O GPNDARIEYHPYAY-UHFFFAOYSA-N 0.000 description 1
- 229920002866 paraformaldehyde Polymers 0.000 description 1
- 238000007747 plating Methods 0.000 description 1
- 229920002647 polyamide Polymers 0.000 description 1
- 239000000256 polyoxyethylene sorbitan monolaurate Substances 0.000 description 1
- LJCNRYVRMXRIQR-OLXYHTOASA-L potassium sodium L-tartrate Chemical compound [Na+].[K+].[O-]C(=O)[C@H](O)[C@@H](O)C([O-])=O LJCNRYVRMXRIQR-OLXYHTOASA-L 0.000 description 1
- 229940074439 potassium sodium tartrate Drugs 0.000 description 1
- 150000003839 salts Chemical class 0.000 description 1
- 229910052709 silver Inorganic materials 0.000 description 1
- 239000004332 silver Substances 0.000 description 1
- 229910052708 sodium Inorganic materials 0.000 description 1
- 239000011734 sodium Substances 0.000 description 1
- HELHAJAZNSDZJO-OLXYHTOASA-L sodium L-tartrate Chemical compound [Na+].[Na+].[O-]C(=O)[C@H](O)[C@@H](O)C([O-])=O HELHAJAZNSDZJO-OLXYHTOASA-L 0.000 description 1
- 235000011006 sodium potassium tartrate Nutrition 0.000 description 1
- 239000001433 sodium tartrate Substances 0.000 description 1
- 229960002167 sodium tartrate Drugs 0.000 description 1
- 235000011004 sodium tartrates Nutrition 0.000 description 1
- 150000003467 sulfuric acid derivatives Chemical class 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
- C23C—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
- C23C18/00—Chemical coating by decomposition of either liquid compounds or solutions of the coating forming compounds, without leaving reaction products of surface material in the coating; Contact plating
- C23C18/16—Chemical coating by decomposition of either liquid compounds or solutions of the coating forming compounds, without leaving reaction products of surface material in the coating; Contact plating by reduction or substitution, e.g. electroless plating
- C23C18/18—Pretreatment of the material to be coated
- C23C18/20—Pretreatment of the material to be coated of organic surfaces, e.g. resins
- C23C18/28—Sensitising or activating
Landscapes
- Chemical & Material Sciences (AREA)
- General Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Mechanical Engineering (AREA)
- Metallurgy (AREA)
- Organic Chemistry (AREA)
- Chemically Coating (AREA)
- Treatments Of Macromolecular Shaped Articles (AREA)
- Manufacturing Of Printed Wiring (AREA)
Priority Applications (20)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| BE756672D BE756672A (fr) | 1969-09-25 | Procede pour le traitement prealable de surfaces en matiere synthetique, en vue de la galvanisation | |
| DE1949278A DE1949278C3 (de) | 1969-09-25 | 1969-09-25 | Verfahren zur Vorbehandlung von Kunststoffteilen für das chemische und galvanische Metallisieren auf Gestellen |
| RO64020A RO57539A (enrdf_load_stackoverflow) | 1969-09-25 | 1970-07-22 | |
| SU1475946A SU368761A3 (enrdf_load_stackoverflow) | 1969-09-25 | 1970-07-31 | |
| CS541470A CS157104B2 (enrdf_load_stackoverflow) | 1969-09-25 | 1970-08-03 | |
| ES382574A ES382574A1 (es) | 1969-09-25 | 1970-08-07 | Procedimiento para el tratamiento previo de superficies de material sintetico. |
| YU2039/70A YU34806B (en) | 1969-09-25 | 1970-08-10 | Process for pre-treating piece goods made of plastics |
| ZA705965*A ZA705965B (en) | 1969-09-25 | 1970-08-31 | Process for activating surfaces of plastic materials |
| GB43156/70A GB1256047A (en) | 1969-09-25 | 1970-09-09 | Process for activating surfaces of plastic materials |
| IE1193/70A IE34641B1 (en) | 1969-09-25 | 1970-09-15 | Process for activating surfaces of plastic materials |
| PL143293A PL74013B2 (enrdf_load_stackoverflow) | 1970-09-18 | ||
| NL7014019.A NL167208C (nl) | 1969-09-25 | 1970-09-22 | Werkwijze voor het voorbehandelen van kunststofopper- vlakken en werkwijze voor het bereiden van een daarvoor geschikte oplossing. |
| CA093,867A CA947153A (en) | 1969-09-25 | 1970-09-23 | Process for activating surfaces of plastic materials |
| HUSCHE295*1A HU167179B (enrdf_load_stackoverflow) | 1969-09-25 | 1970-09-24 | |
| CH1418170A CH562326A5 (enrdf_load_stackoverflow) | 1969-09-25 | 1970-09-24 | |
| AT864370A AT295960B (de) | 1969-09-25 | 1970-09-24 | Verfahren zur Vorbehandlung von Kunststoffoberflächen für das Metallisieren |
| SE13011/70A SE367026B (enrdf_load_stackoverflow) | 1969-09-25 | 1970-09-24 | |
| FR707034599A FR2063003B1 (enrdf_load_stackoverflow) | 1969-09-25 | 1970-09-24 | |
| JP8401970A JPS536186B1 (enrdf_load_stackoverflow) | 1969-09-25 | 1970-09-25 | |
| US05/440,192 US3959564A (en) | 1969-09-25 | 1974-02-06 | Method for the preliminary treatment of plastic surfaces for electroplating |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE1949278A DE1949278C3 (de) | 1969-09-25 | 1969-09-25 | Verfahren zur Vorbehandlung von Kunststoffteilen für das chemische und galvanische Metallisieren auf Gestellen |
Publications (3)
| Publication Number | Publication Date |
|---|---|
| DE1949278A1 DE1949278A1 (de) | 1971-04-08 |
| DE1949278B2 DE1949278B2 (de) | 1978-05-18 |
| DE1949278C3 true DE1949278C3 (de) | 1982-07-15 |
Family
ID=5746907
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DE1949278A Expired DE1949278C3 (de) | 1969-09-25 | 1969-09-25 | Verfahren zur Vorbehandlung von Kunststoffteilen für das chemische und galvanische Metallisieren auf Gestellen |
Country Status (18)
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE10259187B4 (de) * | 2002-12-18 | 2008-06-19 | Enthone Inc., West Haven | Metallisierung von Kunststoffsubstraten und Lösung zum Beizen und Aktivieren |
Families Citing this family (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE3816494A1 (de) * | 1988-05-10 | 1989-11-16 | Schering Ag | Loesung und verfahren zum aetzen und aktivieren von isolierenden oberflaechen |
Family Cites Families (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE1264921B (de) * | 1964-08-07 | 1968-03-28 | Schering Ag | Verfahren zur Vorbehandlung von Kunststoffoberflaechen fuer das Galvanisieren |
| US3561995A (en) * | 1967-04-03 | 1971-02-09 | M & T Chemicals Inc | Method of activating a polymer surface and resultant article |
| US3507681A (en) * | 1967-06-02 | 1970-04-21 | Mine Safety Appliances Co | Metal plating of plastics |
-
0
- BE BE756672D patent/BE756672A/xx not_active IP Right Cessation
-
1969
- 1969-09-25 DE DE1949278A patent/DE1949278C3/de not_active Expired
-
1970
- 1970-07-22 RO RO64020A patent/RO57539A/ro unknown
- 1970-07-31 SU SU1475946A patent/SU368761A3/ru active
- 1970-08-03 CS CS541470A patent/CS157104B2/cs unknown
- 1970-08-07 ES ES382574A patent/ES382574A1/es not_active Expired
- 1970-08-10 YU YU2039/70A patent/YU34806B/xx unknown
- 1970-08-31 ZA ZA705965*A patent/ZA705965B/xx unknown
- 1970-09-09 GB GB43156/70A patent/GB1256047A/en not_active Expired
- 1970-09-15 IE IE1193/70A patent/IE34641B1/xx unknown
- 1970-09-22 NL NL7014019.A patent/NL167208C/xx not_active IP Right Cessation
- 1970-09-23 CA CA093,867A patent/CA947153A/en not_active Expired
- 1970-09-24 SE SE13011/70A patent/SE367026B/xx unknown
- 1970-09-24 FR FR707034599A patent/FR2063003B1/fr not_active Expired
- 1970-09-24 AT AT864370A patent/AT295960B/de not_active IP Right Cessation
- 1970-09-24 CH CH1418170A patent/CH562326A5/xx not_active IP Right Cessation
- 1970-09-24 HU HUSCHE295*1A patent/HU167179B/hu unknown
- 1970-09-25 JP JP8401970A patent/JPS536186B1/ja active Pending
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE10259187B4 (de) * | 2002-12-18 | 2008-06-19 | Enthone Inc., West Haven | Metallisierung von Kunststoffsubstraten und Lösung zum Beizen und Aktivieren |
Also Published As
| Publication number | Publication date |
|---|---|
| PL74013B1 (enrdf_load_stackoverflow) | 1974-10-30 |
| DE1949278B2 (de) | 1978-05-18 |
| FR2063003A1 (enrdf_load_stackoverflow) | 1971-07-02 |
| CH562326A5 (enrdf_load_stackoverflow) | 1975-05-30 |
| NL167208B (nl) | 1981-06-16 |
| DE1949278A1 (de) | 1971-04-08 |
| SU368761A3 (enrdf_load_stackoverflow) | 1973-01-26 |
| IE34641B1 (en) | 1975-07-09 |
| GB1256047A (en) | 1971-12-08 |
| NL7014019A (enrdf_load_stackoverflow) | 1971-03-29 |
| CA947153A (en) | 1974-05-14 |
| NL167208C (nl) | 1981-11-16 |
| HU167179B (enrdf_load_stackoverflow) | 1975-08-28 |
| JPS536186B1 (enrdf_load_stackoverflow) | 1978-03-06 |
| BE756672A (fr) | 1971-03-25 |
| ZA705965B (en) | 1971-04-28 |
| IE34641L (en) | 1971-03-25 |
| CS157104B2 (enrdf_load_stackoverflow) | 1974-08-23 |
| ES382574A1 (es) | 1972-12-01 |
| YU34806B (en) | 1980-03-15 |
| AT295960B (de) | 1972-01-25 |
| SE367026B (enrdf_load_stackoverflow) | 1974-05-13 |
| FR2063003B1 (enrdf_load_stackoverflow) | 1974-07-12 |
| RO57539A (enrdf_load_stackoverflow) | 1974-12-15 |
| YU203970A (en) | 1979-09-10 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C3 | Grant after two publication steps (3rd publication) | ||
| 8339 | Ceased/non-payment of the annual fee |