DE194884C - - Google Patents

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Publication number

DE194884C

DE194884C DENDAT194884D DE194884DA DE194884C DE 194884 C DE194884 C DE 194884C DE NDAT194884 D DENDAT194884 D DE NDAT194884D DE 194884D A DE194884D A DE 194884DA DE 194884 C DE194884 C DE 194884C

Authority

DE

Germany

Prior art keywords

ester

aniline

reaction

chloroacetic

phenylglycine

Prior art date

Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)

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• PAYRUJLWNCNPSJ-UHFFFAOYSA-N Aniline Chemical compound NC1=CC=CC=C1 PAYRUJLWNCNPSJ-UHFFFAOYSA-N 0.000 claims description 18
• -1 phenylglycine ester Chemical class 0.000 claims description 13
• 238000006243 chemical reaction Methods 0.000 claims description 7
• XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 7
• 238000000034 method Methods 0.000 claims description 5
• 238000002360 preparation method Methods 0.000 claims description 3
• VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 claims description 2
• 150000001447 alkali salts Chemical class 0.000 claims description 2
• 229910000041 hydrogen chloride Inorganic materials 0.000 claims description 2
• IXCSERBJSXMMFS-UHFFFAOYSA-N hydrogen chloride Substances Cl.Cl IXCSERBJSXMMFS-UHFFFAOYSA-N 0.000 claims description 2
• 150000007529 inorganic bases Chemical class 0.000 claims 1
• VTYYLEPIZMXCLO-UHFFFAOYSA-L Calcium carbonate Chemical compound [Ca+2].[O-]C([O-])=O VTYYLEPIZMXCLO-UHFFFAOYSA-L 0.000 description 4
• 239000002253 acid Substances 0.000 description 2
• 229910000019 calcium carbonate Inorganic materials 0.000 description 2
• 239000003085 diluting agent Substances 0.000 description 2
• 239000000203 mixture Substances 0.000 description 2
• 150000005331 phenylglycines Chemical class 0.000 description 2
• 239000000126 substance Substances 0.000 description 2
• RRTQTOBOLIGMED-UHFFFAOYSA-N 2-(carboxyamino)-2-phenylacetic acid Chemical compound OC(=O)NC(C(O)=O)C1=CC=CC=C1 RRTQTOBOLIGMED-UHFFFAOYSA-N 0.000 description 1
• UXVMQQNJUSDDNG-UHFFFAOYSA-L Calcium chloride Chemical compound [Cl-].[Cl-].[Ca+2] UXVMQQNJUSDDNG-UHFFFAOYSA-L 0.000 description 1
• JBCSOBKDUKAJHR-UHFFFAOYSA-N ClO.NC1=CC=CC=C1 Chemical compound ClO.NC1=CC=CC=C1 JBCSOBKDUKAJHR-UHFFFAOYSA-N 0.000 description 1
• DHMQDGOQFOQNFH-UHFFFAOYSA-N Glycine Natural products NCC(O)=O DHMQDGOQFOQNFH-UHFFFAOYSA-N 0.000 description 1
• 239000004471 Glycine Substances 0.000 description 1
• MMCPOSDMTGQNKG-UHFFFAOYSA-N anilinium chloride Chemical compound Cl.NC1=CC=CC=C1 MMCPOSDMTGQNKG-UHFFFAOYSA-N 0.000 description 1
• 239000007900 aqueous suspension Substances 0.000 description 1
• 239000001110 calcium chloride Substances 0.000 description 1
• 229910001628 calcium chloride Inorganic materials 0.000 description 1
• BVKZGUZCCUSVTD-UHFFFAOYSA-N carbonic acid Chemical compound OC(O)=O BVKZGUZCCUSVTD-UHFFFAOYSA-N 0.000 description 1
• 239000007795 chemical reaction product Substances 0.000 description 1
• FOCAUTSVDIKZOP-UHFFFAOYSA-N chloroacetic acid Chemical class OC(=O)CCl FOCAUTSVDIKZOP-UHFFFAOYSA-N 0.000 description 1
• 230000004087 circulation Effects 0.000 description 1
• 238000009833 condensation Methods 0.000 description 1
• 230000005494 condensation Effects 0.000 description 1
• 230000003111 delayed effect Effects 0.000 description 1
• 150000002148 esters Chemical class 0.000 description 1
• 239000012467 final product Substances 0.000 description 1
• 229910001510 metal chloride Inorganic materials 0.000 description 1
• 239000012266 salt solution Substances 0.000 description 1
• 238000007127 saponification reaction Methods 0.000 description 1
• 238000000926 separation method Methods 0.000 description 1
• 239000000243 solution Substances 0.000 description 1
• 239000000725 suspension Substances 0.000 description 1
• 238000005303 weighing Methods 0.000 description 1