DE270663C - - Google Patents

Info

Publication number

DE270663C

DE270663C DENDAT270663D DE270663DA DE270663C DE 270663 C DE270663 C DE 270663C DE NDAT270663 D DENDAT270663 D DE NDAT270663D DE 270663D A DE270663D A DE 270663DA DE 270663 C DE270663 C DE 270663C

Authority

DE

Germany

Prior art keywords

xylidine

diaminodi

xylylmethane

water

formaldehyde

Prior art date

Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)

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• WSFSSNUMVMOOMR-UHFFFAOYSA-N Formaldehyde Chemical compound O=C WSFSSNUMVMOOMR-UHFFFAOYSA-N 0.000 claims description 12
• CDULGHZNHURECF-UHFFFAOYSA-N 2,3-dimethylaniline 2,4-dimethylaniline 2,5-dimethylaniline 2,6-dimethylaniline 3,4-dimethylaniline 3,5-dimethylaniline Chemical group CC1=CC=C(N)C(C)=C1.CC1=CC=C(C)C(N)=C1.CC1=CC(C)=CC(N)=C1.CC1=CC=C(N)C=C1C.CC1=CC=CC(N)=C1C.CC1=CC=CC(C)=C1N CDULGHZNHURECF-UHFFFAOYSA-N 0.000 claims description 8
• VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical class Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 claims description 6
• 238000000034 method Methods 0.000 claims description 6
• QAOWNCQODCNURD-UHFFFAOYSA-L Sulfate Chemical compound [O-]S([O-])(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-L 0.000 claims description 4
• UACOVYUOWMWQPJ-UHFFFAOYSA-N bis(2,3-dimethylphenyl)methanediamine Chemical compound NC(C1=C(C(=CC=C1)C)C)(C1=C(C(=CC=C1)C)C)N UACOVYUOWMWQPJ-UHFFFAOYSA-N 0.000 claims description 4
• 238000000926 separation method Methods 0.000 claims description 3
• 239000007864 aqueous solution Substances 0.000 claims description 2
• 150000003467 sulfuric acid derivatives Chemical class 0.000 claims description 2
• 239000000203 mixture Substances 0.000 description 5
• 239000000243 solution Substances 0.000 description 5
• VOWZNBNDMFLQGM-UHFFFAOYSA-N 2,5-dimethylaniline Chemical group CC1=CC=C(C)C(N)=C1 VOWZNBNDMFLQGM-UHFFFAOYSA-N 0.000 description 4
• 239000002585 base Substances 0.000 description 4
• XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 4
• 239000010446 mirabilite Substances 0.000 description 3
• RSIJVJUOQBWMIM-UHFFFAOYSA-L sodium sulfate decahydrate Chemical class O.O.O.O.O.O.O.O.O.O.[Na+].[Na+].[O-]S([O-])(=O)=O RSIJVJUOQBWMIM-UHFFFAOYSA-L 0.000 description 3
• PAYRUJLWNCNPSJ-UHFFFAOYSA-N Aniline Chemical compound NC1=CC=CC=C1 PAYRUJLWNCNPSJ-UHFFFAOYSA-N 0.000 description 2
• 125000003118 aryl group Chemical group 0.000 description 2
• 238000004519 manufacturing process Methods 0.000 description 2
• UHOVQNZJYSORNB-UHFFFAOYSA-N monobenzene Natural products C1=CC=CC=C1 UHOVQNZJYSORNB-UHFFFAOYSA-N 0.000 description 2
• 150000004992 toluidines Chemical class 0.000 description 2
• -1 Glauber's salt Sulphates Chemical class 0.000 description 1
• 230000001476 alcoholic effect Effects 0.000 description 1
• 239000003513 alkali Substances 0.000 description 1
• 125000003277 amino group Chemical group 0.000 description 1
• 239000000987 azo dye Substances 0.000 description 1
• 238000009835 boiling Methods 0.000 description 1
• 239000007795 chemical reaction product Substances 0.000 description 1
• 238000001816 cooling Methods 0.000 description 1
• FBAFATDZDUQKNH-UHFFFAOYSA-M iron chloride Chemical compound [Cl-].[Fe] FBAFATDZDUQKNH-UHFFFAOYSA-M 0.000 description 1
• 238000002844 melting Methods 0.000 description 1
• 230000008018 melting Effects 0.000 description 1
• VNWKTOKETHGBQD-UHFFFAOYSA-N methane Natural products C VNWKTOKETHGBQD-UHFFFAOYSA-N 0.000 description 1
• WSFSSNUMVMOOMR-NJFSPNSNSA-N methanone Chemical compound O=[14CH2] WSFSSNUMVMOOMR-NJFSPNSNSA-N 0.000 description 1
• 239000003960 organic solvent Substances 0.000 description 1
• 239000002244 precipitate Substances 0.000 description 1
• 229920006395 saturated elastomer Polymers 0.000 description 1
• 238000003756 stirring Methods 0.000 description 1
• 229910021653 sulphate ion Inorganic materials 0.000 description 1

Cited By (2)