DE1793832A1 - Organophosphatchromat-verbindungen und verfahren zu deren herstellung - Google Patents
Organophosphatchromat-verbindungen und verfahren zu deren herstellungInfo
- Publication number
- DE1793832A1 DE1793832A1 DE19671793832 DE1793832A DE1793832A1 DE 1793832 A1 DE1793832 A1 DE 1793832A1 DE 19671793832 DE19671793832 DE 19671793832 DE 1793832 A DE1793832 A DE 1793832A DE 1793832 A1 DE1793832 A1 DE 1793832A1
- Authority
- DE
- Germany
- Prior art keywords
- phosphate
- production
- chromium trioxide
- reacted
- chromyl
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- 238000000034 method Methods 0.000 title claims description 9
- 238000004519 manufacturing process Methods 0.000 title claims description 4
- ZCDOYSPFYFSLEW-UHFFFAOYSA-N chromate(2-) Chemical class [O-][Cr]([O-])(=O)=O ZCDOYSPFYFSLEW-UHFFFAOYSA-N 0.000 title description 2
- WGLPBDUCMAPZCE-UHFFFAOYSA-N Trioxochromium Chemical compound O=[Cr](=O)=O WGLPBDUCMAPZCE-UHFFFAOYSA-N 0.000 claims description 12
- 229940117975 chromium trioxide Drugs 0.000 claims description 10
- GAMDZJFZMJECOS-UHFFFAOYSA-N chromium(6+);oxygen(2-) Chemical compound [O-2].[O-2].[O-2].[Cr+6] GAMDZJFZMJECOS-UHFFFAOYSA-N 0.000 claims description 10
- 239000002904 solvent Substances 0.000 claims description 10
- 229910019142 PO4 Inorganic materials 0.000 claims description 9
- 150000001875 compounds Chemical class 0.000 claims description 9
- NBIIXXVUZAFLBC-UHFFFAOYSA-K phosphate Chemical compound [O-]P([O-])([O-])=O NBIIXXVUZAFLBC-UHFFFAOYSA-K 0.000 claims description 9
- 239000010452 phosphate Substances 0.000 claims description 9
- 238000006243 chemical reaction Methods 0.000 claims description 8
- XZZNDPSIHUTMOC-UHFFFAOYSA-N triphenyl phosphate Chemical compound C=1C=CC=CC=1OP(OC=1C=CC=CC=1)(=O)OC1=CC=CC=C1 XZZNDPSIHUTMOC-UHFFFAOYSA-N 0.000 claims description 4
- 239000004215 Carbon black (E152) Substances 0.000 claims description 3
- 125000000217 alkyl group Chemical group 0.000 claims description 3
- 125000003710 aryl alkyl group Chemical group 0.000 claims description 3
- ASMQGLCHMVWBQR-UHFFFAOYSA-M diphenyl phosphate Chemical compound C=1C=CC=CC=1OP(=O)([O-])OC1=CC=CC=C1 ASMQGLCHMVWBQR-UHFFFAOYSA-M 0.000 claims description 3
- 229930195733 hydrocarbon Natural products 0.000 claims description 3
- 238000010992 reflux Methods 0.000 claims description 3
- 125000003118 aryl group Chemical group 0.000 claims description 2
- 229910052799 carbon Inorganic materials 0.000 claims description 2
- 229910000423 chromium oxide Inorganic materials 0.000 claims description 2
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 claims 1
- 239000003348 petrochemical agent Substances 0.000 claims 1
- 125000001997 phenyl group Chemical group [H]C1=C([H])C([H])=C(*)C([H])=C1[H] 0.000 claims 1
- 238000002360 preparation method Methods 0.000 claims 1
- YMWUJEATGCHHMB-UHFFFAOYSA-N Dichloromethane Chemical compound ClCCl YMWUJEATGCHHMB-UHFFFAOYSA-N 0.000 description 9
- VGGSQFUCUMXWEO-UHFFFAOYSA-N Ethene Chemical compound C=C VGGSQFUCUMXWEO-UHFFFAOYSA-N 0.000 description 6
- 239000005977 Ethylene Substances 0.000 description 6
- 238000006116 polymerization reaction Methods 0.000 description 5
- YSMRWXYRXBRSND-UHFFFAOYSA-N TOTP Chemical compound CC1=CC=CC=C1OP(=O)(OC=1C(=CC=CC=1)C)OC1=CC=CC=C1C YSMRWXYRXBRSND-UHFFFAOYSA-N 0.000 description 4
- 239000003054 catalyst Substances 0.000 description 4
- 239000000376 reactant Substances 0.000 description 4
- 239000004698 Polyethylene Substances 0.000 description 3
- VLKZOEOYAKHREP-UHFFFAOYSA-N n-Hexane Chemical compound CCCCCC VLKZOEOYAKHREP-UHFFFAOYSA-N 0.000 description 3
- -1 polyethylene Polymers 0.000 description 3
- 229920000573 polyethylene Polymers 0.000 description 3
- 230000035484 reaction time Effects 0.000 description 3
- HEDRZPFGACZZDS-UHFFFAOYSA-N Chloroform Chemical compound ClC(Cl)Cl HEDRZPFGACZZDS-UHFFFAOYSA-N 0.000 description 2
- OFBQJSOFQDEBGM-UHFFFAOYSA-N Pentane Chemical compound CCCCC OFBQJSOFQDEBGM-UHFFFAOYSA-N 0.000 description 2
- 125000000753 cycloalkyl group Chemical group 0.000 description 2
- NNBZCPXTIHJBJL-UHFFFAOYSA-N decalin Chemical compound C1CCCC2CCCCC21 NNBZCPXTIHJBJL-UHFFFAOYSA-N 0.000 description 2
- 150000002430 hydrocarbons Chemical class 0.000 description 2
- VZGDMQKNWNREIO-UHFFFAOYSA-N tetrachloromethane Chemical compound ClC(Cl)(Cl)Cl VZGDMQKNWNREIO-UHFFFAOYSA-N 0.000 description 2
- IELLVVGAXDLVSW-UHFFFAOYSA-N tricyclohexyl phosphate Chemical compound C1CCCCC1OP(OC1CCCCC1)(=O)OC1CCCCC1 IELLVVGAXDLVSW-UHFFFAOYSA-N 0.000 description 2
- VOITXYVAKOUIBA-UHFFFAOYSA-N triethylaluminium Chemical compound CC[Al](CC)CC VOITXYVAKOUIBA-UHFFFAOYSA-N 0.000 description 2
- XDTMQSROBMDMFD-UHFFFAOYSA-N Cyclohexane Chemical compound C1CCCCC1 XDTMQSROBMDMFD-UHFFFAOYSA-N 0.000 description 1
- JYFHYPJRHGVZDY-UHFFFAOYSA-N Dibutyl phosphate Chemical compound CCCCOP(O)(=O)OCCCC JYFHYPJRHGVZDY-UHFFFAOYSA-N 0.000 description 1
- 239000003638 chemical reducing agent Substances 0.000 description 1
- YQHVEGTZGGQQMV-UHFFFAOYSA-N dicyclohexyl hydrogen phosphate Chemical compound C1CCCCC1OP(=O)(O)OC1CCCCC1 YQHVEGTZGGQQMV-UHFFFAOYSA-N 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- TVMXDCGIABBOFY-UHFFFAOYSA-N octane Chemical compound CCCCCCCC TVMXDCGIABBOFY-UHFFFAOYSA-N 0.000 description 1
- 230000001590 oxidative effect Effects 0.000 description 1
- 239000012429 reaction media Substances 0.000 description 1
- 229920006395 saturated elastomer Polymers 0.000 description 1
- 229930195734 saturated hydrocarbon Natural products 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
- 238000003756 stirring Methods 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- STCOOQWBFONSKY-UHFFFAOYSA-N tributyl phosphate Chemical compound CCCCOP(=O)(OCCCC)OCCCC STCOOQWBFONSKY-UHFFFAOYSA-N 0.000 description 1
- 229930195735 unsaturated hydrocarbon Natural products 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
- C07F9/00—Compounds containing elements of Groups 5 or 15 of the Periodic Table
- C07F9/02—Phosphorus compounds
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
- C08F10/00—Homopolymers and copolymers of unsaturated aliphatic hydrocarbons having only one carbon-to-carbon double bond
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Biochemistry (AREA)
- General Health & Medical Sciences (AREA)
- Molecular Biology (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Transition And Organic Metals Composition Catalysts For Addition Polymerization (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US56080266A | 1966-06-27 | 1966-06-27 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| DE1793832A1 true DE1793832A1 (de) | 1976-10-21 |
Family
ID=24239444
Family Applications (2)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DE19671793832 Pending DE1793832A1 (de) | 1966-06-27 | 1967-06-27 | Organophosphatchromat-verbindungen und verfahren zu deren herstellung |
| DE19671745185 Pending DE1745185A1 (de) | 1966-06-27 | 1967-06-27 | Katalytisches Verfahren zur Olefinpolymerisation |
Family Applications After (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DE19671745185 Pending DE1745185A1 (de) | 1966-06-27 | 1967-06-27 | Katalytisches Verfahren zur Olefinpolymerisation |
Country Status (6)
| Country | Link |
|---|---|
| US (1) | US3474080A (enExample) |
| BE (1) | BE700573A (enExample) |
| DE (2) | DE1793832A1 (enExample) |
| FR (1) | FR1530111A (enExample) |
| GB (1) | GB1167951A (enExample) |
| NL (1) | NL151998B (enExample) |
Families Citing this family (17)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3969272A (en) * | 1972-12-29 | 1976-07-13 | Anderson Development Company | Chromium tris-diorgano-orthophosphate-alkyl aluminum halide catalysts for olefin polymerization and alkylation of aromatic compounds |
| US3907849A (en) * | 1972-12-29 | 1975-09-23 | Anderson Dev Co | Chromium tris-diorgano-orthophosphates and their preparation |
| US3985676A (en) * | 1974-01-24 | 1976-10-12 | National Petro Chemicals Corporation | Catalyst composition and method for the preparation thereof |
| US3901825A (en) * | 1974-03-29 | 1975-08-26 | Anderson Dev Co | Chrome catalyst |
| US4008359A (en) * | 1974-03-29 | 1977-02-15 | Anderson Development Company | Chrome catalyst |
| US4041226A (en) * | 1974-12-12 | 1977-08-09 | Anderson Development Company | Chromium tris-diorgano-orthophosphate-alkyl aluminum halide catalysts for olefin polymerization and alkylation of aromatic compounds |
| US4192775A (en) * | 1975-03-14 | 1980-03-11 | National Petro Chemicals Corporation | Olefin polymerization catalyst |
| US4184028A (en) * | 1975-03-14 | 1980-01-15 | National Petro Chemicals Corporation | Olefin Polymerization catalyst |
| US4234709A (en) * | 1976-05-07 | 1980-11-18 | National Petro Chemicals Corporation | Catalyst composition, method for producing same and method for polymerization of 1-olefins with same |
| US4284527A (en) * | 1978-06-19 | 1981-08-18 | Chemplex Company | Polymerization catalyst |
| US4233253A (en) * | 1978-12-26 | 1980-11-11 | Standard Oil Company (Indiana) | Method for the preparation of metal salts of phosphorus acid esters |
| US4297461A (en) * | 1979-06-08 | 1981-10-27 | National Petro Chemicals Corp. | Olefin polymerization catalyst |
| US4260706A (en) * | 1979-06-21 | 1981-04-07 | National Petro Chemicals Corp. | Olefin polymerization catalyst |
| FR2462441A1 (fr) * | 1979-07-26 | 1981-02-13 | Rhone Poulenc Ind | Procede de stabilisation des solutions de derives organiques du chrome hexavalent dans les solvants hydrocarbones par les esters phosphoriques |
| US4303770A (en) * | 1979-10-24 | 1981-12-01 | Chemplex Company | Method of making polymers and copolymers of 1-olefins |
| US4925928A (en) * | 1988-06-23 | 1990-05-15 | Ciba-Geigy Corporation | Reactive dyes containing vinylsulfonylalkylamino bound to a bis-(triazinylamino)-benzene group |
| US7151073B2 (en) * | 2004-01-16 | 2006-12-19 | Exxonmobil Chemical Patents Inc. | Mesoporous catalyst support, a catalyst system, and method of making and using same for olefin polymerization |
Family Cites Families (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2329707A (en) * | 1941-01-13 | 1943-09-21 | Standard Oil Co California | Metal organophosphates and method of preparing the same |
| US3219676A (en) * | 1960-07-15 | 1965-11-23 | Ethyl Corp | Polymeric molybdenum salts |
| NL125300C (enExample) * | 1961-04-14 | |||
| NL135065C (enExample) * | 1965-05-14 |
-
1966
- 1966-06-27 US US560802A patent/US3474080A/en not_active Expired - Lifetime
-
1967
- 1967-06-21 NL NL676708620A patent/NL151998B/xx not_active IP Right Cessation
- 1967-06-26 FR FR48833A patent/FR1530111A/fr not_active Expired
- 1967-06-27 BE BE700573D patent/BE700573A/xx unknown
- 1967-06-27 DE DE19671793832 patent/DE1793832A1/de active Pending
- 1967-06-27 DE DE19671745185 patent/DE1745185A1/de active Pending
- 1967-06-27 GB GB29516/67A patent/GB1167951A/en not_active Expired
Also Published As
| Publication number | Publication date |
|---|---|
| NL151998B (nl) | 1977-01-17 |
| DE1745185A1 (de) | 1971-08-12 |
| US3474080A (en) | 1969-10-21 |
| FR1530111A (fr) | 1968-06-21 |
| BE700573A (enExample) | 1967-12-01 |
| NL6708620A (enExample) | 1967-12-28 |
| GB1167951A (en) | 1969-10-22 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| OHJ | Non-payment of the annual fee |