DE1768566B2 - Verfahren zur Herstellung von flüssigen Kohlenwasserstoffen aus gebundenen Sauerstoff enthaltender Kohle - Google Patents
Verfahren zur Herstellung von flüssigen Kohlenwasserstoffen aus gebundenen Sauerstoff enthaltender KohleInfo
- Publication number
- DE1768566B2 DE1768566B2 DE1768566A DE1768566A DE1768566B2 DE 1768566 B2 DE1768566 B2 DE 1768566B2 DE 1768566 A DE1768566 A DE 1768566A DE 1768566 A DE1768566 A DE 1768566A DE 1768566 B2 DE1768566 B2 DE 1768566B2
- Authority
- DE
- Germany
- Prior art keywords
- coal
- range
- hydrogen
- zone
- solvent
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Withdrawn
Links
- 239000003245 coal Substances 0.000 title claims description 52
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 title claims description 17
- 229910052760 oxygen Inorganic materials 0.000 title claims description 17
- 239000001301 oxygen Substances 0.000 title claims description 17
- 238000000034 method Methods 0.000 title claims description 11
- 239000007788 liquid Substances 0.000 title claims description 9
- 229930195733 hydrocarbon Natural products 0.000 title claims description 6
- 150000002430 hydrocarbons Chemical class 0.000 title claims description 6
- 238000004519 manufacturing process Methods 0.000 title claims description 4
- 239000001257 hydrogen Substances 0.000 claims description 28
- 229910052739 hydrogen Inorganic materials 0.000 claims description 28
- 238000000605 extraction Methods 0.000 claims description 27
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 claims description 26
- 239000002904 solvent Substances 0.000 claims description 23
- 238000009903 catalytic hydrogenation reaction Methods 0.000 claims description 16
- CXWXQJXEFPUFDZ-UHFFFAOYSA-N tetralin Chemical compound C1=CC=C2CCCCC2=C1 CXWXQJXEFPUFDZ-UHFFFAOYSA-N 0.000 claims description 15
- 239000012263 liquid product Substances 0.000 claims description 14
- 238000005984 hydrogenation reaction Methods 0.000 claims description 10
- 239000003054 catalyst Substances 0.000 claims description 9
- 238000009835 boiling Methods 0.000 claims description 4
- KYYSIVCCYWZZLR-UHFFFAOYSA-N cobalt(2+);dioxido(dioxo)molybdenum Chemical compound [Co+2].[O-][Mo]([O-])(=O)=O KYYSIVCCYWZZLR-UHFFFAOYSA-N 0.000 claims description 3
- 150000001454 anthracenes Chemical class 0.000 claims description 2
- 125000003118 aryl group Chemical group 0.000 claims description 2
- 230000004048 modification Effects 0.000 claims description 2
- 238000012986 modification Methods 0.000 claims description 2
- TWNQGVIAIRXVLR-UHFFFAOYSA-N oxo(oxoalumanyloxy)alumane Chemical compound O=[Al]O[Al]=O TWNQGVIAIRXVLR-UHFFFAOYSA-N 0.000 claims 1
- 238000006243 chemical reaction Methods 0.000 description 18
- 239000007789 gas Substances 0.000 description 10
- 239000000047 product Substances 0.000 description 9
- 239000003921 oil Substances 0.000 description 8
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 6
- 229910052799 carbon Inorganic materials 0.000 description 6
- 238000004517 catalytic hydrocracking Methods 0.000 description 5
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 4
- 239000003502 gasoline Substances 0.000 description 3
- 239000010802 sludge Substances 0.000 description 3
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 2
- 230000015572 biosynthetic process Effects 0.000 description 2
- 230000003197 catalytic effect Effects 0.000 description 2
- 238000001914 filtration Methods 0.000 description 2
- 150000002431 hydrogen Chemical class 0.000 description 2
- 239000003077 lignite Substances 0.000 description 2
- 239000007791 liquid phase Substances 0.000 description 2
- 239000000203 mixture Substances 0.000 description 2
- 239000002245 particle Substances 0.000 description 2
- 239000004215 Carbon black (E152) Substances 0.000 description 1
- OFBQJSOFQDEBGM-UHFFFAOYSA-N Pentane Chemical class CCCCC OFBQJSOFQDEBGM-UHFFFAOYSA-N 0.000 description 1
- NINIDFKCEFEMDL-UHFFFAOYSA-N Sulfur Chemical compound [S] NINIDFKCEFEMDL-UHFFFAOYSA-N 0.000 description 1
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 description 1
- 229910052782 aluminium Inorganic materials 0.000 description 1
- PNEYBMLMFCGWSK-UHFFFAOYSA-N aluminium oxide Inorganic materials [O-2].[O-2].[O-2].[Al+3].[Al+3] PNEYBMLMFCGWSK-UHFFFAOYSA-N 0.000 description 1
- 239000002802 bituminous coal Substances 0.000 description 1
- 235000013844 butane Nutrition 0.000 description 1
- 239000003795 chemical substances by application Substances 0.000 description 1
- 229910000428 cobalt oxide Inorganic materials 0.000 description 1
- IVMYJDGYRUAWML-UHFFFAOYSA-N cobalt(ii) oxide Chemical compound [Co]=O IVMYJDGYRUAWML-UHFFFAOYSA-N 0.000 description 1
- 238000005336 cracking Methods 0.000 description 1
- 239000003085 diluting agent Substances 0.000 description 1
- 238000004821 distillation Methods 0.000 description 1
- 238000009826 distribution Methods 0.000 description 1
- 239000000446 fuel Substances 0.000 description 1
- 239000000295 fuel oil Substances 0.000 description 1
- 238000010438 heat treatment Methods 0.000 description 1
- 238000002156 mixing Methods 0.000 description 1
- 229910000476 molybdenum oxide Inorganic materials 0.000 description 1
- IJDNQMDRQITEOD-UHFFFAOYSA-N n-butane Chemical class CCCC IJDNQMDRQITEOD-UHFFFAOYSA-N 0.000 description 1
- 229910052757 nitrogen Inorganic materials 0.000 description 1
- PQQKPALAQIIWST-UHFFFAOYSA-N oxomolybdenum Chemical compound [Mo]=O PQQKPALAQIIWST-UHFFFAOYSA-N 0.000 description 1
- 239000012071 phase Substances 0.000 description 1
- 238000000926 separation method Methods 0.000 description 1
- 239000002002 slurry Substances 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 229910052717 sulfur Inorganic materials 0.000 description 1
- 239000011593 sulfur Substances 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
- C10G1/00—Production of liquid hydrocarbon mixtures from oil-shale, oil-sand, or non-melting solid carbonaceous or similar materials, e.g. wood, coal
- C10G1/006—Combinations of processes provided in groups C10G1/02 - C10G1/08
Landscapes
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Life Sciences & Earth Sciences (AREA)
- Wood Science & Technology (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Production Of Liquid Hydrocarbon Mixture For Refining Petroleum (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US64200967A | 1967-05-29 | 1967-05-29 |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| DE1768566A1 DE1768566A1 (de) | 1971-11-18 |
| DE1768566B2 true DE1768566B2 (de) | 1979-02-15 |
Family
ID=24574786
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DE1768566A Withdrawn DE1768566B2 (de) | 1967-05-29 | 1968-05-29 | Verfahren zur Herstellung von flüssigen Kohlenwasserstoffen aus gebundenen Sauerstoff enthaltender Kohle |
Country Status (5)
Families Citing this family (34)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3617513A (en) * | 1969-01-03 | 1971-11-02 | Exxon Research Engineering Co | Coking of heavy feedstocks |
| US3652446A (en) * | 1969-11-17 | 1972-03-28 | Exxon Research Engineering Co | Combination process for liquefaction of coal and catalytic cracking of selected fractions thereof |
| US3642608A (en) * | 1970-01-09 | 1972-02-15 | Kerr Mc Gee Chem Corp | Solvation of coal in byproduct streams |
| US3930984A (en) * | 1970-10-01 | 1976-01-06 | Phillips Petroleum Company | Coal-anthracene oil slurry liquefied with carbon monoxide and barium-promoted catalysts |
| US3671418A (en) * | 1970-12-18 | 1972-06-20 | Universal Oil Prod Co | Coal liquefaction process using ash as a catalyst |
| US4111788A (en) * | 1976-09-23 | 1978-09-05 | Hydrocarbon Research, Inc. | Staged hydrogenation of low rank coal |
| US4391699A (en) * | 1976-12-27 | 1983-07-05 | Chevron Research Company | Coal liquefaction process |
| US4330389A (en) * | 1976-12-27 | 1982-05-18 | Chevron Research Company | Coal liquefaction process |
| US4330391A (en) * | 1976-12-27 | 1982-05-18 | Chevron Research Company | Coal liquefaction process |
| US4105535A (en) * | 1977-03-07 | 1978-08-08 | Mobil Oil Corporation | Conversion of coal-derived liquids with a crystalline aluminosilicate zeolite catalyst |
| US4108758A (en) * | 1977-03-14 | 1978-08-22 | Mobil Oil Corporation | Conversion of coal into liquid fuels |
| GB1604230A (en) * | 1978-05-31 | 1981-12-02 | Mobil Oil Corp | Hydroprocessing coal liquids |
| US4331530A (en) * | 1978-02-27 | 1982-05-25 | Occidental Research Corporation | Process for the conversion of coal |
| US4283267A (en) * | 1978-05-11 | 1981-08-11 | Exxon Research & Engineering Co. | Staged temperature hydrogen-donor coal liquefaction process |
| US4358359A (en) * | 1979-09-07 | 1982-11-09 | Chevron Research Company | Two-stage coal liquefaction process with process-derived solvent having a low heptane-insolubles content |
| US4295954A (en) * | 1979-10-18 | 1981-10-20 | Mobil Oil Corporation | Coal conversion catalysts |
| US4350582A (en) * | 1979-10-18 | 1982-09-21 | Chevron Research Company | Two-stage coal liquefaction process with process-derived solvent |
| US4344838A (en) * | 1979-10-18 | 1982-08-17 | Mobil Oil Corporation | Coal conversion catalysts |
| US4264429A (en) * | 1979-10-18 | 1981-04-28 | Chevron Research Company | Two-stage coal liquefaction process with process-derived solvent |
| US4300996A (en) * | 1979-12-26 | 1981-11-17 | Chevron Research Company | Three-stage coal liquefaction process |
| US4298451A (en) * | 1980-02-25 | 1981-11-03 | The United States Of America As Represented By The United States Department Of Energy | Two stage liquefaction of coal |
| US4344837A (en) * | 1980-04-15 | 1982-08-17 | Mitsui Coke Co., Ltd. | Process for the dehydration and liquefaction of water-containing coal |
| US4327058A (en) * | 1980-07-08 | 1982-04-27 | Wheelabrator-Frye, Inc. | Capillary processing unit |
| US4409089A (en) * | 1980-08-14 | 1983-10-11 | Mobil Oil Corporation | Coal liquefaction and resid processing with lignin |
| US4313816A (en) * | 1980-08-25 | 1982-02-02 | Exxon Research & Engineering Co. | Staged temperature coal conversion process |
| US4450066A (en) * | 1980-09-02 | 1984-05-22 | Exxon Research And Engineering Co. | Hydrothermal pretreatment to prevent scale during liquefaction of certain solid carbonaceous materials |
| DE3038842C2 (de) * | 1980-10-15 | 1986-06-19 | Bergwerksverband Gmbh, 4300 Essen | Verfahren zur Steigerung der Kohleölgewinnung bei der Kohlehydrierung |
| JPS58180587A (ja) * | 1982-04-19 | 1983-10-22 | Mitsubishi Chem Ind Ltd | 石炭の転化方法 |
| US4411767A (en) * | 1982-09-30 | 1983-10-25 | Air Products And Chemicals, Inc. | Integrated process for the solvent refining of coal |
| US4879021A (en) * | 1983-03-07 | 1989-11-07 | Hri, Inc. | Hydrogenation of coal and subsequent liquefaction of hydrogenated undissolved coal |
| US4486293A (en) * | 1983-04-25 | 1984-12-04 | Air Products And Chemicals, Inc. | Catalytic coal hydroliquefaction process |
| IT1163480B (it) * | 1983-06-08 | 1987-04-08 | Anic Spa | Procedimento a piu' stadi per la liquefazione diretta del carbone |
| US4816141A (en) * | 1987-10-16 | 1989-03-28 | Hri, Inc. | Catalytic two-stage liquefaction of coal utilizing cascading of used ebullated-bed catalyst |
| US9061953B2 (en) | 2013-11-19 | 2015-06-23 | Uop Llc | Process for converting polycyclic aromatic compounds to monocyclic aromatic compounds |
Family Cites Families (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2215206A (en) * | 1937-07-06 | 1940-09-17 | Carnegie Inst Of Technology | Hydrogenation of coal |
| US2464271A (en) * | 1943-12-24 | 1949-03-15 | Henry H Storch | Coal liquefaction by hydrogenation |
| US3143489A (en) * | 1961-11-24 | 1964-08-04 | Consolidation Coal Co | Process for making liquid fuels from coal |
| US3184401A (en) * | 1962-01-19 | 1965-05-18 | Consolidation Coal Co | Process for producing hydrogenenriched hydrocarbonaceous products from coal |
| US3162594A (en) * | 1962-04-09 | 1964-12-22 | Consolidation Coal Co | Process for producing liquid fuels from coal |
| US3275546A (en) * | 1962-12-28 | 1966-09-27 | Consolidation Coal Co | Method of attriting solids in a hydrocracking process |
-
1967
- 1967-05-29 US US642009A patent/US3488279A/en not_active Expired - Lifetime
-
1968
- 1968-05-23 GB GB24679/68A patent/GB1221696A/en not_active Expired
- 1968-05-29 BE BE715818D patent/BE715818A/xx unknown
- 1968-05-29 DE DE1768566A patent/DE1768566B2/de not_active Withdrawn
- 1968-06-07 FR FR1587888D patent/FR1587888A/fr not_active Expired
Also Published As
| Publication number | Publication date |
|---|---|
| BE715818A (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html) | 1968-11-29 |
| DE1768566A1 (de) | 1971-11-18 |
| US3488279A (en) | 1970-01-06 |
| FR1587888A (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html) | 1970-04-03 |
| GB1221696A (en) | 1971-02-03 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| OF | Willingness to grant licences before publication of examined application | ||
| BHN | Withdrawal |