DE1667406A1 - Anlage und Verfahren zur Herstellung von Phosphorsaeure - Google Patents
Anlage und Verfahren zur Herstellung von PhosphorsaeureInfo
- Publication number
- DE1667406A1 DE1667406A1 DE19671667406 DE1667406A DE1667406A1 DE 1667406 A1 DE1667406 A1 DE 1667406A1 DE 19671667406 DE19671667406 DE 19671667406 DE 1667406 A DE1667406 A DE 1667406A DE 1667406 A1 DE1667406 A1 DE 1667406A1
- Authority
- DE
- Germany
- Prior art keywords
- container
- rock
- reaction
- retaining wall
- partial
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- NBIIXXVUZAFLBC-UHFFFAOYSA-N Phosphoric acid Chemical compound OP(O)(O)=O NBIIXXVUZAFLBC-UHFFFAOYSA-N 0.000 title claims description 38
- 229910000147 aluminium phosphate Inorganic materials 0.000 title claims description 19
- 238000004519 manufacturing process Methods 0.000 title claims description 8
- 238000000034 method Methods 0.000 title claims description 5
- 230000008569 process Effects 0.000 title claims description 4
- 238000006243 chemical reaction Methods 0.000 claims description 68
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 claims description 56
- 239000011435 rock Substances 0.000 claims description 34
- 239000007795 chemical reaction product Substances 0.000 claims description 22
- 239000012066 reaction slurry Substances 0.000 claims description 11
- 239000002367 phosphate rock Substances 0.000 claims description 10
- NBIIXXVUZAFLBC-UHFFFAOYSA-K phosphate Chemical compound [O-]P([O-])([O-])=O NBIIXXVUZAFLBC-UHFFFAOYSA-K 0.000 claims description 8
- 229910019142 PO4 Inorganic materials 0.000 claims description 6
- 239000007788 liquid Substances 0.000 claims description 6
- 239000010452 phosphate Substances 0.000 claims description 6
- 239000000047 product Substances 0.000 claims description 5
- 230000002706 hydrostatic effect Effects 0.000 claims description 4
- 238000003756 stirring Methods 0.000 claims description 4
- 238000007599 discharging Methods 0.000 claims description 2
- 239000002002 slurry Substances 0.000 claims description 2
- 238000010924 continuous production Methods 0.000 claims 2
- 238000003860 storage Methods 0.000 claims 2
- 230000008676 import Effects 0.000 claims 1
- 230000002093 peripheral effect Effects 0.000 claims 1
- 238000004321 preservation Methods 0.000 claims 1
- 239000000344 soap Substances 0.000 claims 1
- 239000000725 suspension Substances 0.000 claims 1
- 238000010276 construction Methods 0.000 description 11
- OSGAYBCDTDRGGQ-UHFFFAOYSA-L calcium sulfate Chemical compound [Ca+2].[O-]S([O-])(=O)=O OSGAYBCDTDRGGQ-UHFFFAOYSA-L 0.000 description 10
- 239000010440 gypsum Substances 0.000 description 8
- 229910052602 gypsum Inorganic materials 0.000 description 8
- 239000001506 calcium phosphate Substances 0.000 description 7
- 230000015572 biosynthetic process Effects 0.000 description 6
- 239000003245 coal Substances 0.000 description 6
- 239000013078 crystal Substances 0.000 description 6
- 235000011132 calcium sulphate Nutrition 0.000 description 5
- 238000000605 extraction Methods 0.000 description 5
- 235000019739 Dicalciumphosphate Nutrition 0.000 description 4
- QAOWNCQODCNURD-UHFFFAOYSA-L Sulfate Chemical compound [O-]S([O-])(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-L 0.000 description 4
- 230000008859 change Effects 0.000 description 4
- 238000005260 corrosion Methods 0.000 description 4
- 230000007797 corrosion Effects 0.000 description 4
- NEFBYIFKOOEVPA-UHFFFAOYSA-K dicalcium phosphate Chemical compound [Ca+2].[Ca+2].[O-]P([O-])([O-])=O NEFBYIFKOOEVPA-UHFFFAOYSA-K 0.000 description 4
- 229910000390 dicalcium phosphate Inorganic materials 0.000 description 4
- 229940038472 dicalcium phosphate Drugs 0.000 description 4
- 239000000463 material Substances 0.000 description 4
- 229910052751 metal Inorganic materials 0.000 description 4
- 239000002184 metal Substances 0.000 description 4
- 230000001105 regulatory effect Effects 0.000 description 4
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 3
- 239000002253 acid Substances 0.000 description 3
- 230000008901 benefit Effects 0.000 description 3
- 239000001175 calcium sulphate Substances 0.000 description 3
- 229910052799 carbon Inorganic materials 0.000 description 3
- 238000001914 filtration Methods 0.000 description 3
- 239000002198 insoluble material Substances 0.000 description 3
- 239000002245 particle Substances 0.000 description 3
- 239000002244 precipitate Substances 0.000 description 3
- QORWJWZARLRLPR-UHFFFAOYSA-H tricalcium bis(phosphate) Chemical compound [Ca+2].[Ca+2].[Ca+2].[O-]P([O-])([O-])=O.[O-]P([O-])([O-])=O QORWJWZARLRLPR-UHFFFAOYSA-H 0.000 description 3
- 229910000391 tricalcium phosphate Inorganic materials 0.000 description 3
- 229940078499 tricalcium phosphate Drugs 0.000 description 3
- 235000019731 tricalcium phosphate Nutrition 0.000 description 3
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical group [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 description 2
- 150000007513 acids Chemical class 0.000 description 2
- 230000009471 action Effects 0.000 description 2
- 229910003460 diamond Inorganic materials 0.000 description 2
- 239000010432 diamond Substances 0.000 description 2
- 238000005516 engineering process Methods 0.000 description 2
- 238000011068 loading method Methods 0.000 description 2
- 238000012423 maintenance Methods 0.000 description 2
- 238000011084 recovery Methods 0.000 description 2
- 239000004575 stone Substances 0.000 description 2
- -1 sulphate ions Chemical class 0.000 description 2
- 229910052782 aluminium Chemical group 0.000 description 1
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical group [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 description 1
- 230000004888 barrier function Effects 0.000 description 1
- 239000006227 byproduct Substances 0.000 description 1
- 239000011575 calcium Substances 0.000 description 1
- 230000015556 catabolic process Effects 0.000 description 1
- 238000004140 cleaning Methods 0.000 description 1
- 238000002425 crystallisation Methods 0.000 description 1
- 230000008025 crystallization Effects 0.000 description 1
- 238000000354 decomposition reaction Methods 0.000 description 1
- 230000003247 decreasing effect Effects 0.000 description 1
- 238000006731 degradation reaction Methods 0.000 description 1
- 230000029087 digestion Effects 0.000 description 1
- 150000004683 dihydrates Chemical group 0.000 description 1
- 238000007865 diluting Methods 0.000 description 1
- 239000012895 dilution Substances 0.000 description 1
- 238000010790 dilution Methods 0.000 description 1
- 238000004090 dissolution Methods 0.000 description 1
- 238000009826 distribution Methods 0.000 description 1
- 239000000428 dust Substances 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 239000007789 gas Substances 0.000 description 1
- 230000005484 gravity Effects 0.000 description 1
- 238000009434 installation Methods 0.000 description 1
- 150000002500 ions Chemical class 0.000 description 1
- 229910052742 iron Inorganic materials 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- 229910052585 phosphate mineral Inorganic materials 0.000 description 1
- OTYBMLCTZGSZBG-UHFFFAOYSA-L potassium sulfate Chemical compound [K+].[K+].[O-]S([O-])(=O)=O OTYBMLCTZGSZBG-UHFFFAOYSA-L 0.000 description 1
- 229910052939 potassium sulfate Inorganic materials 0.000 description 1
- 235000011151 potassium sulphates Nutrition 0.000 description 1
- 230000002265 prevention Effects 0.000 description 1
- 239000000376 reactant Substances 0.000 description 1
- 230000035484 reaction time Effects 0.000 description 1
- 230000009257 reactivity Effects 0.000 description 1
- 238000004064 recycling Methods 0.000 description 1
- 230000000717 retained effect Effects 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
- 239000002195 soluble material Substances 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 229910021653 sulphate ion Inorganic materials 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B25/00—Phosphorus; Compounds thereof
- C01B25/16—Oxyacids of phosphorus; Salts thereof
- C01B25/18—Phosphoric acid
- C01B25/22—Preparation by reacting phosphate-containing material with an acid, e.g. wet process
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Physical Or Chemical Processes And Apparatus (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US522249A US3415629A (en) | 1966-01-21 | 1966-01-21 | Apparatus for the production of phosphoric acid |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| DE1667406A1 true DE1667406A1 (de) | 1971-06-09 |
Family
ID=24080091
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DE19671667406 Pending DE1667406A1 (de) | 1966-01-21 | 1967-01-18 | Anlage und Verfahren zur Herstellung von Phosphorsaeure |
Country Status (4)
| Country | Link |
|---|---|
| US (1) | US3415629A (forum.php) |
| BE (1) | BE692958A (forum.php) |
| DE (1) | DE1667406A1 (forum.php) |
| NL (1) | NL6700727A (forum.php) |
Families Citing this family (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| RO67651A2 (ro) * | 1978-01-18 | 1982-10-11 | Institutul De Inginerie Tehnologica Si Proiectare Pentru Industria Chimica,Ro | Reactor pentru fabricarea acidului fosforic |
| US4242308A (en) * | 1978-11-06 | 1980-12-30 | Mihail Dochia | Controllable reaction medium single reactor for phosphoric acid production |
Family Cites Families (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2306962A (en) * | 1940-10-28 | 1942-12-29 | Standard Oil Co | Mixing apparatus |
| US2845936A (en) * | 1955-05-09 | 1958-08-05 | Hercules Powder Co Ltd | Countercurrent contacting apparatus |
| BE629736A (forum.php) * | 1960-11-18 | |||
| NL274891A (forum.php) * | 1961-02-17 |
-
1966
- 1966-01-21 US US522249A patent/US3415629A/en not_active Expired - Lifetime
-
1967
- 1967-01-17 NL NL6700727A patent/NL6700727A/xx unknown
- 1967-01-18 DE DE19671667406 patent/DE1667406A1/de active Pending
- 1967-01-20 BE BE692958D patent/BE692958A/xx unknown
Also Published As
| Publication number | Publication date |
|---|---|
| US3415629A (en) | 1968-12-10 |
| BE692958A (forum.php) | 1967-07-20 |
| NL6700727A (forum.php) | 1967-07-24 |
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