DE163143C - - Google Patents
Info
- Publication number
- DE163143C DE163143C DENDAT163143D DE163143DA DE163143C DE 163143 C DE163143 C DE 163143C DE NDAT163143 D DENDAT163143 D DE NDAT163143D DE 163143D A DE163143D A DE 163143DA DE 163143 C DE163143 C DE 163143C
- Authority
- DE
- Germany
- Prior art keywords
- sulfur
- benzidine
- temperature
- tolylenediamine
- melt
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Active
Links
- NINIDFKCEFEMDL-UHFFFAOYSA-N Sulfur Chemical compound [S] NINIDFKCEFEMDL-UHFFFAOYSA-N 0.000 claims description 5
- HFACYLZERDEVSX-UHFFFAOYSA-N benzidine Chemical compound C1=CC(N)=CC=C1C1=CC=C(N)C=C1 HFACYLZERDEVSX-UHFFFAOYSA-N 0.000 claims description 5
- 229910052717 sulfur Inorganic materials 0.000 claims description 5
- 239000011593 sulfur Substances 0.000 claims description 5
- VOZKAJLKRJDJLL-UHFFFAOYSA-N 2,4-diaminotoluene Chemical compound CC1=CC=C(N)C=C1N VOZKAJLKRJDJLL-UHFFFAOYSA-N 0.000 claims description 4
- 239000000155 melt Substances 0.000 claims description 3
- 229920000742 Cotton Polymers 0.000 claims description 2
- 229910052783 alkali metal Inorganic materials 0.000 claims 1
- 150000001340 alkali metals Chemical class 0.000 claims 1
- 238000002844 melting Methods 0.000 claims 1
- 230000008018 melting Effects 0.000 claims 1
- 238000000034 method Methods 0.000 claims 1
- 238000004383 yellowing Methods 0.000 claims 1
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 3
- 239000002253 acid Substances 0.000 description 3
- 239000000047 product Substances 0.000 description 3
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 2
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 description 2
- 150000007513 acids Chemical class 0.000 description 2
- 239000000975 dye Substances 0.000 description 2
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 2
- QDHHCQZDFGDHMP-UHFFFAOYSA-N Chloramine Chemical compound ClN QDHHCQZDFGDHMP-UHFFFAOYSA-N 0.000 description 1
- RWSOTUBLDIXVET-UHFFFAOYSA-N Dihydrogen sulfide Chemical compound S RWSOTUBLDIXVET-UHFFFAOYSA-N 0.000 description 1
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 description 1
- 239000007795 chemical reaction product Substances 0.000 description 1
- 239000004927 clay Substances 0.000 description 1
- 238000005187 foaming Methods 0.000 description 1
- 235000011187 glycerol Nutrition 0.000 description 1
- 238000010438 heat treatment Methods 0.000 description 1
- 239000000843 powder Substances 0.000 description 1
- 239000011734 sodium Substances 0.000 description 1
- 229910052708 sodium Inorganic materials 0.000 description 1
- 235000011121 sodium hydroxide Nutrition 0.000 description 1
- GRVFOGOEDUUMBP-UHFFFAOYSA-N sodium sulfide (anhydrous) Chemical compound [Na+].[Na+].[S-2] GRVFOGOEDUUMBP-UHFFFAOYSA-N 0.000 description 1
- 238000003756 stirring Methods 0.000 description 1
- QAOWNCQODCNURD-UHFFFAOYSA-N sulfuric acid Substances OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 description 1
- 238000005987 sulfurization reaction Methods 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09B—ORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
- C09B49/00—Sulfur dyes
- C09B49/04—Sulfur dyes from amino compounds of the benzene, naphthalene or anthracene series
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Publications (1)
| Publication Number | Publication Date |
|---|---|
| DE163143C true DE163143C (cs) |
Family
ID=428861
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DENDAT163143D Active DE163143C (cs) |
Country Status (1)
| Country | Link |
|---|---|
| DE (1) | DE163143C (cs) |
-
0
- DE DENDAT163143D patent/DE163143C/de active Active
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| DE163143C (cs) | ||
| DE679985C (de) | Verfahren zur Herstellung von Schwefelfarbstoffen | |
| DE620904C (de) | Verfahren zur Darstellung cyclischer ª‡-Cyanketimide und cyclischer ª‡-Cyanketone | |
| DE845516C (de) | Verfahren zur Darstellung von primaeren aliphatischen, aromatischaliphatischen bzw. cycloaliphatischen Aminen | |
| DE52509C (de) | Verfahren zur Darstellung von geschwefelten Kondensationsprodukten des Parato-Juidins | |
| DE157862C (cs) | ||
| DE76771C (de) | Verfahren zur Darstellung von Amidoguajacol aus Nitroacet-o-Anisidin | |
| DE221465C (cs) | ||
| DE212205C (cs) | ||
| DE160041C (cs) | ||
| DE2454277A1 (de) | Verfahren zur herstellung von mercaptobenzthiazol | |
| DE67478C (de) | Verfahren zur Darstellung eines gelben basischen Farbstoffs der Auramingruppe aus symmetrischem Dimethyldiamidodi-o-tolylmethan | |
| DE138845C (cs) | ||
| DE838139C (de) | Verfahren zur Herstellung von 7-Alkylsulfonylcarbonsäuren | |
| AT88635B (de) | Verfahren zur Darstellung von Arsenoverbindungen der Pyrazolonreihe. | |
| DE145763C (cs) | ||
| DE550571C (de) | Verfahren zur Darstellung von substituierten Guanidinen | |
| DE219830C (cs) | ||
| DE180394C (cs) | ||
| DE1493673A1 (de) | Verfahren zur Herstellung von grenzflaechenaktiven Substanzen mit hoher Elektrolytbestaendigkeit | |
| DE109150C (cs) | ||
| DE144765C (cs) | ||
| DE146917C (cs) | ||
| DE75911C (de) | Verfahren zur Darstellung eines am Stickstoff alkylirten Eurhodins | |
| AT129790B (de) | Verfahren zur Darstellung von Kondensationsprodukten aus Cyanamid und Formaldehyd. |