DE1496830B1 - Verfahren zum galvanischen Abscheiden von duktilen halbglaenzenden Nickelschichten aus Cumarin und Cumarinderivate enthaltenden Nic - Google Patents
Verfahren zum galvanischen Abscheiden von duktilen halbglaenzenden Nickelschichten aus Cumarin und Cumarinderivate enthaltenden NicInfo
- Publication number
- DE1496830B1 DE1496830B1 DE19661496830 DE1496830A DE1496830B1 DE 1496830 B1 DE1496830 B1 DE 1496830B1 DE 19661496830 DE19661496830 DE 19661496830 DE 1496830 A DE1496830 A DE 1496830A DE 1496830 B1 DE1496830 B1 DE 1496830B1
- Authority
- DE
- Germany
- Prior art keywords
- coumarin
- glossy
- semi
- nickel
- bath
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- ZYGHJZDHTFUPRJ-UHFFFAOYSA-N coumarin Chemical compound C1=CC=C2OC(=O)C=CC2=C1 ZYGHJZDHTFUPRJ-UHFFFAOYSA-N 0.000 title claims description 65
- PXHVJJICTQNCMI-UHFFFAOYSA-N Nickel Chemical compound [Ni] PXHVJJICTQNCMI-UHFFFAOYSA-N 0.000 title claims description 53
- 235000001671 coumarin Nutrition 0.000 title claims description 37
- 229960000956 coumarin Drugs 0.000 title claims description 29
- 229910052759 nickel Inorganic materials 0.000 title claims description 27
- 150000004775 coumarins Chemical class 0.000 title claims description 17
- 238000000034 method Methods 0.000 title claims description 8
- 230000008569 process Effects 0.000 title claims description 3
- 238000004070 electrodeposition Methods 0.000 title 1
- 150000001875 compounds Chemical class 0.000 claims description 15
- 238000000354 decomposition reaction Methods 0.000 claims description 14
- HUSDTFBXUYBZJD-UHFFFAOYSA-N 2-(2-prop-2-ynoxyethoxy)ethanol Chemical compound OCCOCCOCC#C HUSDTFBXUYBZJD-UHFFFAOYSA-N 0.000 claims description 12
- 238000000151 deposition Methods 0.000 claims description 6
- 230000008030 elimination Effects 0.000 claims 1
- 238000003379 elimination reaction Methods 0.000 claims 1
- CJBDUOMQLFKVQC-UHFFFAOYSA-N 3-(2-hydroxyphenyl)propanoic acid Chemical group OC(=O)CCC1=CC=CC=C1O CJBDUOMQLFKVQC-UHFFFAOYSA-N 0.000 description 30
- WSFSSNUMVMOOMR-UHFFFAOYSA-N Formaldehyde Chemical compound O=C WSFSSNUMVMOOMR-UHFFFAOYSA-N 0.000 description 21
- 239000000047 product Substances 0.000 description 21
- 239000002244 precipitate Substances 0.000 description 19
- 238000001556 precipitation Methods 0.000 description 16
- 238000007747 plating Methods 0.000 description 6
- HFFLGKNGCAIQMO-UHFFFAOYSA-N trichloroacetaldehyde Chemical compound ClC(Cl)(Cl)C=O HFFLGKNGCAIQMO-UHFFFAOYSA-N 0.000 description 6
- GOLORTLGFDVFDW-UHFFFAOYSA-N 3-(1h-benzimidazol-2-yl)-7-(diethylamino)chromen-2-one Chemical compound C1=CC=C2NC(C3=CC4=CC=C(C=C4OC3=O)N(CC)CC)=NC2=C1 GOLORTLGFDVFDW-UHFFFAOYSA-N 0.000 description 4
- 229910021586 Nickel(II) chloride Inorganic materials 0.000 description 4
- 239000000654 additive Substances 0.000 description 4
- 230000008021 deposition Effects 0.000 description 4
- QMMRZOWCJAIUJA-UHFFFAOYSA-L nickel dichloride Chemical compound Cl[Ni]Cl QMMRZOWCJAIUJA-UHFFFAOYSA-L 0.000 description 4
- 238000011282 treatment Methods 0.000 description 4
- YTGSYRVSBPFKMQ-UHFFFAOYSA-N 2,2,2-tribromoacetaldehyde Chemical compound BrC(Br)(Br)C=O YTGSYRVSBPFKMQ-UHFFFAOYSA-N 0.000 description 3
- CKCOPMSBJBNBCQ-UHFFFAOYSA-N 3-chlorochromen-2-one Chemical compound C1=CC=C2OC(=O)C(Cl)=CC2=C1 CKCOPMSBJBNBCQ-UHFFFAOYSA-N 0.000 description 3
- VEXZGXHMUGYJMC-UHFFFAOYSA-M Chloride anion Chemical compound [Cl-] VEXZGXHMUGYJMC-UHFFFAOYSA-M 0.000 description 3
- 239000004327 boric acid Substances 0.000 description 3
- -1 diethylene glycol nickel Chemical compound 0.000 description 3
- 238000000926 separation method Methods 0.000 description 3
- LIFAQMGORKPVDH-UHFFFAOYSA-N 7-ethoxycoumarin Chemical compound C1=CC(=O)OC2=CC(OCC)=CC=C21 LIFAQMGORKPVDH-UHFFFAOYSA-N 0.000 description 2
- ODRDTKMYQDXVGG-UHFFFAOYSA-N 8-methoxychromen-2-one Chemical compound C1=CC(=O)OC2=C1C=CC=C2OC ODRDTKMYQDXVGG-UHFFFAOYSA-N 0.000 description 2
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 2
- KGBXLFKZBHKPEV-UHFFFAOYSA-N boric acid Chemical compound OB(O)O KGBXLFKZBHKPEV-UHFFFAOYSA-N 0.000 description 2
- 230000008859 change Effects 0.000 description 2
- 239000011248 coating agent Substances 0.000 description 2
- 238000000576 coating method Methods 0.000 description 2
- 230000000052 comparative effect Effects 0.000 description 2
- 238000002474 experimental method Methods 0.000 description 2
- 230000006872 improvement Effects 0.000 description 2
- LGQLOGILCSXPEA-UHFFFAOYSA-L nickel sulfate Chemical compound [Ni+2].[O-]S([O-])(=O)=O LGQLOGILCSXPEA-UHFFFAOYSA-L 0.000 description 2
- 229910000363 nickel(II) sulfate Inorganic materials 0.000 description 2
- 239000010454 slate Substances 0.000 description 2
- 238000003756 stirring Methods 0.000 description 2
- QIVUCLWGARAQIO-OLIXTKCUSA-N (3s)-n-[(3s,5s,6r)-6-methyl-2-oxo-1-(2,2,2-trifluoroethyl)-5-(2,3,6-trifluorophenyl)piperidin-3-yl]-2-oxospiro[1h-pyrrolo[2,3-b]pyridine-3,6'-5,7-dihydrocyclopenta[b]pyridine]-3'-carboxamide Chemical compound C1([C@H]2[C@H](N(C(=O)[C@@H](NC(=O)C=3C=C4C[C@]5(CC4=NC=3)C3=CC=CN=C3NC5=O)C2)CC(F)(F)F)C)=C(F)C=CC(F)=C1F QIVUCLWGARAQIO-OLIXTKCUSA-N 0.000 description 1
- CSPIFKKOBWYOEX-UHFFFAOYSA-N 3-acetylcoumarin Chemical compound C1=CC=C2OC(=O)C(C(=O)C)=CC2=C1 CSPIFKKOBWYOEX-UHFFFAOYSA-N 0.000 description 1
- DZCTYFCCOGXULA-UHFFFAOYSA-N 3-bromochromen-2-one Chemical compound C1=CC=C2OC(=O)C(Br)=CC2=C1 DZCTYFCCOGXULA-UHFFFAOYSA-N 0.000 description 1
- HRDCVMSNCBAMAM-UHFFFAOYSA-N 3-prop-2-ynoxyprop-1-yne Chemical compound C#CCOCC#C HRDCVMSNCBAMAM-UHFFFAOYSA-N 0.000 description 1
- QECFPFZIFALPKP-UHFFFAOYSA-N 4,8-dimethylchromen-2-one Chemical compound CC1=CC=CC2=C1OC(=O)C=C2C QECFPFZIFALPKP-UHFFFAOYSA-N 0.000 description 1
- ZAMOUSCENKQFHK-UHFFFAOYSA-N Chlorine atom Chemical compound [Cl] ZAMOUSCENKQFHK-UHFFFAOYSA-N 0.000 description 1
- VYZAMTAEIAYCRO-UHFFFAOYSA-N Chromium Chemical compound [Cr] VYZAMTAEIAYCRO-UHFFFAOYSA-N 0.000 description 1
- QAOWNCQODCNURD-UHFFFAOYSA-L Sulfate Chemical compound [O-]S([O-])(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-L 0.000 description 1
- 238000010521 absorption reaction Methods 0.000 description 1
- 230000035508 accumulation Effects 0.000 description 1
- 238000009825 accumulation Methods 0.000 description 1
- 238000013019 agitation Methods 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 125000005619 boric acid group Chemical group 0.000 description 1
- 229910052801 chlorine Inorganic materials 0.000 description 1
- 239000000460 chlorine Substances 0.000 description 1
- 229910052804 chromium Inorganic materials 0.000 description 1
- 239000011651 chromium Substances 0.000 description 1
- 238000004140 cleaning Methods 0.000 description 1
- 239000000356 contaminant Substances 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 238000005868 electrolysis reaction Methods 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 230000009467 reduction Effects 0.000 description 1
- 229910021653 sulphate ion Inorganic materials 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C25—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES; APPARATUS THEREFOR
- C25D—PROCESSES FOR THE ELECTROLYTIC OR ELECTROPHORETIC PRODUCTION OF COATINGS; ELECTROFORMING; APPARATUS THEREFOR
- C25D3/00—Electroplating: Baths therefor
- C25D3/02—Electroplating: Baths therefor from solutions
- C25D3/12—Electroplating: Baths therefor from solutions of nickel or cobalt
- C25D3/14—Electroplating: Baths therefor from solutions of nickel or cobalt from baths containing acetylenic or heterocyclic compounds
Landscapes
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Electrochemistry (AREA)
- Materials Engineering (AREA)
- Metallurgy (AREA)
- Organic Chemistry (AREA)
- Electroplating And Plating Baths Therefor (AREA)
- Electrolytic Production Of Metals (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US502603A US3414491A (en) | 1965-10-22 | 1965-10-22 | Electrodeposition of nickel |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| DE1496830B1 true DE1496830B1 (de) | 1970-10-15 |
Family
ID=23998561
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DE19661496830 Pending DE1496830B1 (de) | 1965-10-22 | 1966-10-21 | Verfahren zum galvanischen Abscheiden von duktilen halbglaenzenden Nickelschichten aus Cumarin und Cumarinderivate enthaltenden Nic |
Country Status (6)
Families Citing this family (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CA1030484A (en) * | 1973-02-28 | 1978-05-02 | Roy W. Klein | Nickel electroplating composition and process |
| US4203808A (en) * | 1976-07-14 | 1980-05-20 | Monsanto Company | Electroplating cathodes for electrochemical synthesis |
| JP2004508997A (ja) * | 2000-09-11 | 2004-03-25 | ダウ グローバル テクノロジーズ インコーポレイティド | ランフラットタイヤ支持体及びそのための着色剤 |
| US20030178314A1 (en) * | 2002-03-21 | 2003-09-25 | United States Steel Corporation | Stainless steel electrolytic coating |
| CN105506689B (zh) * | 2015-12-22 | 2018-02-16 | 福建金杨科技股份有限公司 | 一种电池钢壳双层镀镍工艺及该工艺制得的电池钢壳 |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE860128C (de) * | 1947-01-29 | 1952-12-18 | Harshaw Chem Corp | Vernicklungsbad |
| DE1003531B (de) * | 1954-04-05 | 1957-02-28 | Udylite Res Corp | Saures galvanisches Glanzvernickelungsbad |
Family Cites Families (10)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| NL269880A (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html) * | ||||
| BE542292A (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html) * | ||||
| CA632773A (en) * | 1961-12-12 | Kardos Otto | Electrodeposition of nickel | |
| NL185994B (nl) * | 1953-03-24 | Wabco Westinghouse | Koppelingskop voor een persluchtleiding. | |
| US2782153A (en) * | 1954-02-16 | 1957-02-19 | Harshaw Chem Corp | Nickel electrodeposition |
| US2900707A (en) * | 1954-08-06 | 1959-08-25 | Udylite Corp | Metallic protective coating |
| US2818376A (en) * | 1956-12-28 | 1957-12-31 | Hanson Van Winkle Munning Co | Nickel plating |
| US2986501A (en) * | 1959-07-27 | 1961-05-30 | Mcgean Chem Co Inc | Electrodeposition of nickel |
| NL257194A (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html) * | 1960-03-21 | |||
| US3305462A (en) * | 1965-09-02 | 1967-02-21 | Barnet D Ostrow | Acid nickel electroplating bath |
-
0
- NL NL133678D patent/NL133678C/xx active
-
1965
- 1965-10-22 US US502603A patent/US3414491A/en not_active Expired - Lifetime
-
1966
- 1966-10-18 GB GB46482/66A patent/GB1093490A/en not_active Expired
- 1966-10-21 NL NL6614936A patent/NL6614936A/xx unknown
- 1966-10-21 FR FR80966A patent/FR1508159A/fr not_active Expired
- 1966-10-21 ES ES0332548A patent/ES332548A1/es not_active Expired
- 1966-10-21 DE DE19661496830 patent/DE1496830B1/de active Pending
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE860128C (de) * | 1947-01-29 | 1952-12-18 | Harshaw Chem Corp | Vernicklungsbad |
| DE1003531B (de) * | 1954-04-05 | 1957-02-28 | Udylite Res Corp | Saures galvanisches Glanzvernickelungsbad |
Also Published As
| Publication number | Publication date |
|---|---|
| GB1093490A (en) | 1967-12-06 |
| FR1508159A (fr) | 1968-01-05 |
| ES332548A1 (es) | 1967-11-16 |
| US3414491A (en) | 1968-12-03 |
| NL6614936A (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html) | 1967-04-24 |
| NL133678C (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html) |
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