DE1443853A1 - Verfahren zur Herstellung von Persaeuren - Google Patents
Verfahren zur Herstellung von PersaeurenInfo
- Publication number
- DE1443853A1 DE1443853A1 DE19631443853 DE1443853A DE1443853A1 DE 1443853 A1 DE1443853 A1 DE 1443853A1 DE 19631443853 DE19631443853 DE 19631443853 DE 1443853 A DE1443853 A DE 1443853A DE 1443853 A1 DE1443853 A1 DE 1443853A1
- Authority
- DE
- Germany
- Prior art keywords
- acid
- aliphatic
- water
- strong
- τοη
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- 238000000034 method Methods 0.000 title claims description 32
- 238000002360 preparation method Methods 0.000 title description 3
- 239000002253 acid Substances 0.000 claims description 74
- MHAJPDPJQMAIIY-UHFFFAOYSA-N Hydrogen peroxide Chemical compound OO MHAJPDPJQMAIIY-UHFFFAOYSA-N 0.000 claims description 42
- 125000001931 aliphatic group Chemical group 0.000 claims description 32
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 claims description 31
- QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 claims description 30
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 28
- 230000002378 acidificating effect Effects 0.000 claims description 8
- 238000004519 manufacturing process Methods 0.000 claims description 8
- 239000000126 substance Substances 0.000 claims description 8
- 239000007795 chemical reaction product Substances 0.000 claims description 6
- 229920006395 saturated elastomer Polymers 0.000 claims description 5
- 229910052739 hydrogen Inorganic materials 0.000 claims description 3
- 239000001257 hydrogen Substances 0.000 claims description 3
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 claims description 2
- 241000287182 Sturnidae Species 0.000 claims description 2
- NBIIXXVUZAFLBC-UHFFFAOYSA-N Phosphoric acid Chemical compound OP(O)(O)=O NBIIXXVUZAFLBC-UHFFFAOYSA-N 0.000 claims 4
- 229910000147 aluminium phosphate Inorganic materials 0.000 claims 2
- 239000011049 pearl Substances 0.000 claims 1
- 238000006243 chemical reaction Methods 0.000 description 28
- 239000000047 product Substances 0.000 description 18
- 150000004965 peroxy acids Chemical class 0.000 description 16
- 229960000583 acetic acid Drugs 0.000 description 10
- 229910052760 oxygen Inorganic materials 0.000 description 10
- 150000002978 peroxides Chemical class 0.000 description 10
- 238000004821 distillation Methods 0.000 description 9
- 239000001301 oxygen Substances 0.000 description 9
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 7
- 239000000203 mixture Substances 0.000 description 7
- 239000000243 solution Substances 0.000 description 7
- 150000007513 acids Chemical class 0.000 description 6
- 238000001704 evaporation Methods 0.000 description 6
- 239000002360 explosive Substances 0.000 description 6
- -1 pereseigeüure Chemical compound 0.000 description 6
- 239000003054 catalyst Substances 0.000 description 5
- 230000008020 evaporation Effects 0.000 description 5
- 239000007864 aqueous solution Substances 0.000 description 4
- 239000007788 liquid Substances 0.000 description 4
- 239000011541 reaction mixture Substances 0.000 description 4
- LEHOTFFKMJEONL-UHFFFAOYSA-N Uric Acid Chemical compound N1C(=O)NC(=O)C2=C1NC(=O)N2 LEHOTFFKMJEONL-UHFFFAOYSA-N 0.000 description 3
- TVWHNULVHGKJHS-UHFFFAOYSA-N Uric acid Natural products N1C(=O)NC(=O)C2NC(=O)NC21 TVWHNULVHGKJHS-UHFFFAOYSA-N 0.000 description 3
- 238000010924 continuous production Methods 0.000 description 3
- 239000012362 glacial acetic acid Substances 0.000 description 3
- 229910000462 iron(III) oxide hydroxide Inorganic materials 0.000 description 3
- 229940116269 uric acid Drugs 0.000 description 3
- KAKZBPTYRLMSJV-UHFFFAOYSA-N Butadiene Chemical compound C=CC=C KAKZBPTYRLMSJV-UHFFFAOYSA-N 0.000 description 2
- 230000015572 biosynthetic process Effects 0.000 description 2
- 239000004927 clay Substances 0.000 description 2
- 150000001875 compounds Chemical class 0.000 description 2
- XBDQKXXYIPTUBI-UHFFFAOYSA-N dimethylselenoniopropionate Natural products CCC(O)=O XBDQKXXYIPTUBI-UHFFFAOYSA-N 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- 235000013345 egg yolk Nutrition 0.000 description 2
- 210000002969 egg yolk Anatomy 0.000 description 2
- 238000005194 fractionation Methods 0.000 description 2
- 229910052753 mercury Inorganic materials 0.000 description 2
- BDAGIHXWWSANSR-UHFFFAOYSA-N methanoic acid Natural products OC=O BDAGIHXWWSANSR-UHFFFAOYSA-N 0.000 description 2
- OSWFIVFLDKOXQC-UHFFFAOYSA-N 4-(3-methoxyphenyl)aniline Chemical compound COC1=CC=CC(C=2C=CC(N)=CC=2)=C1 OSWFIVFLDKOXQC-UHFFFAOYSA-N 0.000 description 1
- 101100027969 Caenorhabditis elegans old-1 gene Proteins 0.000 description 1
- MQJKPEGWNLWLTK-UHFFFAOYSA-N Dapsone Chemical class C1=CC(N)=CC=C1S(=O)(=O)C1=CC=C(N)C=C1 MQJKPEGWNLWLTK-UHFFFAOYSA-N 0.000 description 1
- 239000004593 Epoxy Substances 0.000 description 1
- 206010065954 Stubbornness Diseases 0.000 description 1
- 241001122767 Theaceae Species 0.000 description 1
- 229910052770 Uranium Inorganic materials 0.000 description 1
- 230000001133 acceleration Effects 0.000 description 1
- 238000009825 accumulation Methods 0.000 description 1
- 235000011054 acetic acid Nutrition 0.000 description 1
- 150000001298 alcohols Chemical class 0.000 description 1
- 125000000217 alkyl group Chemical group 0.000 description 1
- 150000001408 amides Chemical class 0.000 description 1
- 150000008064 anhydrides Chemical class 0.000 description 1
- 239000011260 aqueous acid Substances 0.000 description 1
- 125000003118 aryl group Chemical group 0.000 description 1
- 239000010426 asphalt Substances 0.000 description 1
- 239000011230 binding agent Substances 0.000 description 1
- 229910052799 carbon Inorganic materials 0.000 description 1
- 125000004432 carbon atom Chemical group C* 0.000 description 1
- 230000003197 catalytic effect Effects 0.000 description 1
- 150000001768 cations Chemical class 0.000 description 1
- 238000009833 condensation Methods 0.000 description 1
- 230000005494 condensation Effects 0.000 description 1
- 239000007859 condensation product Substances 0.000 description 1
- 239000000470 constituent Substances 0.000 description 1
- 238000000354 decomposition reaction Methods 0.000 description 1
- 238000009826 distribution Methods 0.000 description 1
- 235000013601 eggs Nutrition 0.000 description 1
- 238000006735 epoxidation reaction Methods 0.000 description 1
- 125000003700 epoxy group Chemical group 0.000 description 1
- 150000002194 fatty esters Chemical class 0.000 description 1
- 239000000835 fiber Substances 0.000 description 1
- 235000019253 formic acid Nutrition 0.000 description 1
- 239000011521 glass Substances 0.000 description 1
- 238000010438 heat treatment Methods 0.000 description 1
- 229910001385 heavy metal Inorganic materials 0.000 description 1
- 150000002431 hydrogen Chemical class 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-M hydroxide Chemical compound [OH-] XLYOFNOQVPJJNP-UHFFFAOYSA-M 0.000 description 1
- 230000033444 hydroxylation Effects 0.000 description 1
- 238000005805 hydroxylation reaction Methods 0.000 description 1
- 239000012535 impurity Substances 0.000 description 1
- 239000004615 ingredient Substances 0.000 description 1
- 239000006193 liquid solution Substances 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- QSHDDOUJBYECFT-UHFFFAOYSA-N mercury Chemical compound [Hg] QSHDDOUJBYECFT-UHFFFAOYSA-N 0.000 description 1
- 239000000178 monomer Substances 0.000 description 1
- 235000021049 nutrient content Nutrition 0.000 description 1
- 239000003921 oil Substances 0.000 description 1
- 238000006053 organic reaction Methods 0.000 description 1
- JTJMJGYZQZDUJJ-UHFFFAOYSA-N phencyclidine Chemical compound C1CCCCN1C1(C=2C=CC=CC=2)CCCCC1 JTJMJGYZQZDUJJ-UHFFFAOYSA-N 0.000 description 1
- 239000006187 pill Substances 0.000 description 1
- 229920000642 polymer Polymers 0.000 description 1
- 230000003449 preventive effect Effects 0.000 description 1
- 235000019260 propionic acid Nutrition 0.000 description 1
- IUVKMZGDUIUOCP-BTNSXGMBSA-N quinbolone Chemical compound O([C@H]1CC[C@H]2[C@H]3[C@@H]([C@]4(C=CC(=O)C=C4CC3)C)CC[C@@]21C)C1=CCCC1 IUVKMZGDUIUOCP-BTNSXGMBSA-N 0.000 description 1
- 239000012429 reaction media Substances 0.000 description 1
- 230000035484 reaction time Effects 0.000 description 1
- 230000029058 respiratory gaseous exchange Effects 0.000 description 1
- 230000028327 secretion Effects 0.000 description 1
- 238000000926 separation method Methods 0.000 description 1
- 238000001577 simple distillation Methods 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
- 238000003860 storage Methods 0.000 description 1
- DNYWZCXLKNTFFI-UHFFFAOYSA-N uranium Chemical compound [U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U] DNYWZCXLKNTFFI-UHFFFAOYSA-N 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C407/00—Preparation of peroxy compounds
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C407/00—Preparation of peroxy compounds
- C07C407/003—Separation; Purification; Stabilisation; Use of additives
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Fertilizers (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US18506362A | 1962-04-04 | 1962-04-04 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| DE1443853A1 true DE1443853A1 (de) | 1968-10-24 |
Family
ID=22679414
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DE19631443853 Pending DE1443853A1 (de) | 1962-04-04 | 1963-03-22 | Verfahren zur Herstellung von Persaeuren |
Country Status (6)
| Country | Link |
|---|---|
| AT (1) | AT238151B (enrdf_load_stackoverflow) |
| BE (1) | BE630363A (enrdf_load_stackoverflow) |
| CH (1) | CH457385A (enrdf_load_stackoverflow) |
| DE (1) | DE1443853A1 (enrdf_load_stackoverflow) |
| ES (1) | ES285966A1 (enrdf_load_stackoverflow) |
| GB (1) | GB1014361A (enrdf_load_stackoverflow) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP0641777A1 (de) * | 1993-09-08 | 1995-03-08 | LAPORTE GmbH | Verfahren und Vorrichtung zur kontinuierlichen Herstellung von Peroxycarbonsäuren |
Families Citing this family (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE2619091C2 (de) * | 1976-05-03 | 1983-10-27 | Degussa Ag, 6000 Frankfurt | Kontinuierliches Verfahren zum Epoxidieren von olefinische Doppelbindungen enthaltenden organischen Verbindungen |
| DE3418450A1 (de) * | 1984-05-18 | 1985-11-28 | Degussa Ag, 6000 Frankfurt | Verfahren zur herstellung wasserunloeslicher peroxycarbonsaeuren |
| SE9600347L (sv) † | 1996-01-31 | 1997-08-01 | Eka Chemicals Ab | Sätt att framställa kemisk produkt |
| EP1004576A1 (en) * | 1998-11-23 | 2000-05-31 | SOLVAY (Société Anonyme) | Process for producing peracetic acid |
| FI111459B (fi) | 2001-04-04 | 2003-07-31 | Kemira Chemicals Oy | Menetelmä stabiilin peretikkahappotuotteen valmistamiseksi |
| FI112363B (fi) | 2001-04-04 | 2003-11-28 | Kemira Chemicals Oy | Menetelmä peretikkahapon valmistamiseksi |
| FI116466B (fi) | 2001-10-30 | 2005-11-30 | Kemira Oyj | Menetelmä perkarboksyylihapon valmistamiseksi |
| KR102740111B1 (ko) * | 2017-11-27 | 2024-12-06 | 미츠비시 가스 가가쿠 가부시키가이샤 | 식품 첨가물로서 사용되는 과아세트산 조성물의 제조 방법 |
-
0
- BE BE630363D patent/BE630363A/xx unknown
-
1963
- 1963-03-12 ES ES285966A patent/ES285966A1/es not_active Expired
- 1963-03-22 DE DE19631443853 patent/DE1443853A1/de active Pending
- 1963-03-25 GB GB1165863A patent/GB1014361A/en not_active Expired
- 1963-03-28 AT AT248963A patent/AT238151B/de active
- 1963-04-02 CH CH418663A patent/CH457385A/de unknown
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP0641777A1 (de) * | 1993-09-08 | 1995-03-08 | LAPORTE GmbH | Verfahren und Vorrichtung zur kontinuierlichen Herstellung von Peroxycarbonsäuren |
Also Published As
| Publication number | Publication date |
|---|---|
| CH457385A (de) | 1968-06-15 |
| BE630363A (enrdf_load_stackoverflow) | |
| GB1014361A (en) | 1965-12-22 |
| ES285966A1 (es) | 1963-08-16 |
| AT238151B (de) | 1965-01-25 |
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