DE1277245B - Verfahren zur Herstellung von Perchloraethylen - Google Patents
Verfahren zur Herstellung von PerchloraethylenInfo
- Publication number
- DE1277245B DE1277245B DED48658A DED0048658A DE1277245B DE 1277245 B DE1277245 B DE 1277245B DE D48658 A DED48658 A DE D48658A DE D0048658 A DED0048658 A DE D0048658A DE 1277245 B DE1277245 B DE 1277245B
- Authority
- DE
- Germany
- Prior art keywords
- reaction
- dichloroethane
- trichlorethylene
- perchlorethylene
- tetrachloroethane
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- CYTYCFOTNPOANT-UHFFFAOYSA-N Perchloroethylene Chemical group ClC(Cl)=C(Cl)Cl CYTYCFOTNPOANT-UHFFFAOYSA-N 0.000 title claims description 25
- 238000000034 method Methods 0.000 title claims description 25
- 229950011008 tetrachloroethylene Drugs 0.000 title claims description 24
- 238000004519 manufacturing process Methods 0.000 title description 9
- QPFMBZIOSGYJDE-UHFFFAOYSA-N 1,1,2,2-tetrachloroethane Chemical compound ClC(Cl)C(Cl)Cl QPFMBZIOSGYJDE-UHFFFAOYSA-N 0.000 claims description 33
- 238000006243 chemical reaction Methods 0.000 claims description 31
- WSLDOOZREJYCGB-UHFFFAOYSA-N 1,2-Dichloroethane Chemical compound ClCCCl WSLDOOZREJYCGB-UHFFFAOYSA-N 0.000 claims description 25
- XSTXAVWGXDQKEL-UHFFFAOYSA-N Trichloroethylene Chemical group ClC=C(Cl)Cl XSTXAVWGXDQKEL-UHFFFAOYSA-N 0.000 claims description 22
- ZAMOUSCENKQFHK-UHFFFAOYSA-N Chlorine atom Chemical compound [Cl] ZAMOUSCENKQFHK-UHFFFAOYSA-N 0.000 claims description 15
- 239000000460 chlorine Substances 0.000 claims description 15
- 229910052801 chlorine Inorganic materials 0.000 claims description 15
- 239000003054 catalyst Substances 0.000 claims description 12
- 238000005660 chlorination reaction Methods 0.000 claims description 11
- 238000003776 cleavage reaction Methods 0.000 claims description 4
- 238000001816 cooling Methods 0.000 claims description 4
- 230000017525 heat dissipation Effects 0.000 claims description 2
- 238000002360 preparation method Methods 0.000 claims description 2
- 238000001179 sorption measurement Methods 0.000 claims 1
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 8
- 239000006227 byproduct Substances 0.000 description 6
- 239000011148 porous material Substances 0.000 description 4
- 230000015572 biosynthetic process Effects 0.000 description 3
- 239000007789 gas Substances 0.000 description 3
- 239000001257 hydrogen Substances 0.000 description 3
- 229910052739 hydrogen Inorganic materials 0.000 description 3
- IXCSERBJSXMMFS-UHFFFAOYSA-N hydrogen chloride Substances Cl.Cl IXCSERBJSXMMFS-UHFFFAOYSA-N 0.000 description 3
- 229910000041 hydrogen chloride Inorganic materials 0.000 description 3
- 239000000203 mixture Substances 0.000 description 3
- OTMSDBZUPAUEDD-UHFFFAOYSA-N Ethane Chemical compound CC OTMSDBZUPAUEDD-UHFFFAOYSA-N 0.000 description 2
- VGGSQFUCUMXWEO-UHFFFAOYSA-N Ethene Chemical compound C=C VGGSQFUCUMXWEO-UHFFFAOYSA-N 0.000 description 2
- 239000005977 Ethylene Substances 0.000 description 2
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 description 2
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 description 2
- BZHJMEDXRYGGRV-UHFFFAOYSA-N Vinyl chloride Chemical group ClC=C BZHJMEDXRYGGRV-UHFFFAOYSA-N 0.000 description 2
- 239000003245 coal Substances 0.000 description 2
- 229960003750 ethyl chloride Drugs 0.000 description 2
- 238000010438 heat treatment Methods 0.000 description 2
- 239000011541 reaction mixture Substances 0.000 description 2
- -1 trichlorethylene hydrogen chloride Chemical compound 0.000 description 2
- YKGVOMJRTXLEJY-UHFFFAOYSA-N 1,1,2-trichloroethene;hydrochloride Chemical group Cl.ClC=C(Cl)Cl YKGVOMJRTXLEJY-UHFFFAOYSA-N 0.000 description 1
- DWHAJXWMMQKTNR-UHFFFAOYSA-N C(CCl)Cl.[Cl] Chemical compound C(CCl)Cl.[Cl] DWHAJXWMMQKTNR-UHFFFAOYSA-N 0.000 description 1
- 241001026509 Kata Species 0.000 description 1
- 238000009825 accumulation Methods 0.000 description 1
- HSFWRNGVRCDJHI-UHFFFAOYSA-N alpha-acetylene Natural products C#C HSFWRNGVRCDJHI-UHFFFAOYSA-N 0.000 description 1
- 229910052799 carbon Inorganic materials 0.000 description 1
- 230000003197 catalytic effect Effects 0.000 description 1
- 239000007795 chemical reaction product Substances 0.000 description 1
- 150000008280 chlorinated hydrocarbons Chemical class 0.000 description 1
- 150000001804 chlorine Chemical class 0.000 description 1
- HRYZWHHZPQKTII-UHFFFAOYSA-N chloroethane Chemical compound CCCl HRYZWHHZPQKTII-UHFFFAOYSA-N 0.000 description 1
- 238000010276 construction Methods 0.000 description 1
- 230000003247 decreasing effect Effects 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- DKQVJMREABFYNT-UHFFFAOYSA-N ethene Chemical group C=C.C=C DKQVJMREABFYNT-UHFFFAOYSA-N 0.000 description 1
- 125000002534 ethynyl group Chemical group [H]C#C* 0.000 description 1
- 239000012530 fluid Substances 0.000 description 1
- CKAPSXZOOQJIBF-UHFFFAOYSA-N hexachlorobenzene Chemical compound ClC1=C(Cl)C(Cl)=C(Cl)C(Cl)=C1Cl CKAPSXZOOQJIBF-UHFFFAOYSA-N 0.000 description 1
- VHHHONWQHHHLTI-UHFFFAOYSA-N hexachloroethane Chemical compound ClC(Cl)(Cl)C(Cl)(Cl)Cl VHHHONWQHHHLTI-UHFFFAOYSA-N 0.000 description 1
- 150000002431 hydrogen Chemical class 0.000 description 1
- 239000011261 inert gas Substances 0.000 description 1
- 238000009434 installation Methods 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 239000000155 melt Substances 0.000 description 1
- 239000002184 metal Substances 0.000 description 1
- 229910052751 metal Inorganic materials 0.000 description 1
- 229910001510 metal chloride Inorganic materials 0.000 description 1
- 238000004886 process control Methods 0.000 description 1
- 239000000047 product Substances 0.000 description 1
- 150000003839 salts Chemical class 0.000 description 1
- 229920006395 saturated elastomer Polymers 0.000 description 1
- 238000007086 side reaction Methods 0.000 description 1
- 239000007858 starting material Substances 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 230000001629 suppression Effects 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C17/00—Preparation of halogenated hydrocarbons
- C07C17/093—Preparation of halogenated hydrocarbons by replacement by halogens
- C07C17/10—Preparation of halogenated hydrocarbons by replacement by halogens of hydrogen atoms
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| AT483465A AT273057B (de) | 1965-05-26 | 1965-05-26 | Verfahren zur Herstellung von Perchloräthylen |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| DE1277245B true DE1277245B (de) | 1968-09-12 |
Family
ID=3568874
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DED48658A Pending DE1277245B (de) | 1965-05-26 | 1965-11-16 | Verfahren zur Herstellung von Perchloraethylen |
Country Status (5)
| Country | Link |
|---|---|
| AT (1) | AT273057B (enExample) |
| CH (1) | CH485622A (enExample) |
| DE (1) | DE1277245B (enExample) |
| FR (1) | FR1456362A (enExample) |
| NL (1) | NL151974B (enExample) |
-
1965
- 1965-05-26 AT AT483465A patent/AT273057B/de active
- 1965-11-16 DE DED48658A patent/DE1277245B/de active Pending
- 1965-12-06 FR FR41088A patent/FR1456362A/fr not_active Expired
-
1966
- 1966-01-12 CH CH36966A patent/CH485622A/de not_active IP Right Cessation
- 1966-05-25 NL NL6607204A patent/NL151974B/xx not_active IP Right Cessation
Also Published As
| Publication number | Publication date |
|---|---|
| NL151974B (nl) | 1977-01-17 |
| NL6607204A (enExample) | 1966-11-28 |
| AT273057B (de) | 1969-07-25 |
| CH485622A (de) | 1970-02-15 |
| FR1456362A (fr) | 1966-10-21 |
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