DE1235932B - Vorrichtung zur Herstellung von Chlorderivaten der Cyanursaeure - Google Patents
Vorrichtung zur Herstellung von Chlorderivaten der CyanursaeureInfo
- Publication number
- DE1235932B DE1235932B DEO9988A DEO0009988A DE1235932B DE 1235932 B DE1235932 B DE 1235932B DE O9988 A DEO9988 A DE O9988A DE O0009988 A DEO0009988 A DE O0009988A DE 1235932 B DE1235932 B DE 1235932B
- Authority
- DE
- Germany
- Prior art keywords
- chlorination
- zone
- chlorine
- line
- cyanuric acid
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- 238000004519 manufacturing process Methods 0.000 title claims description 8
- 239000002253 acid Substances 0.000 title claims description 7
- 125000001309 chloro group Chemical class Cl* 0.000 title 1
- 238000005660 chlorination reaction Methods 0.000 claims description 35
- 239000000460 chlorine Substances 0.000 claims description 21
- ZAMOUSCENKQFHK-UHFFFAOYSA-N Chlorine atom Chemical compound [Cl] ZAMOUSCENKQFHK-UHFFFAOYSA-N 0.000 claims description 19
- 229910052801 chlorine Inorganic materials 0.000 claims description 19
- ZFSLODLOARCGLH-UHFFFAOYSA-N isocyanuric acid Chemical compound OC1=NC(O)=NC(O)=N1 ZFSLODLOARCGLH-UHFFFAOYSA-N 0.000 claims description 12
- 230000001105 regulatory effect Effects 0.000 claims description 10
- 239000011541 reaction mixture Substances 0.000 claims description 8
- 238000001914 filtration Methods 0.000 claims description 7
- 238000007872 degassing Methods 0.000 claims description 6
- 150000001804 chlorine Chemical class 0.000 claims description 4
- 239000002826 coolant Substances 0.000 claims description 3
- 239000012452 mother liquor Substances 0.000 claims description 3
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 claims 6
- 238000000926 separation method Methods 0.000 claims 1
- 239000000243 solution Substances 0.000 description 18
- 238000006243 chemical reaction Methods 0.000 description 6
- 239000003513 alkali Substances 0.000 description 5
- 239000000047 product Substances 0.000 description 5
- 239000002585 base Substances 0.000 description 4
- 238000001816 cooling Methods 0.000 description 4
- 239000013078 crystal Substances 0.000 description 4
- 150000007973 cyanuric acids Chemical class 0.000 description 4
- CEJLBZWIKQJOAT-UHFFFAOYSA-N dichloroisocyanuric acid Chemical compound ClN1C(=O)NC(=O)N(Cl)C1=O CEJLBZWIKQJOAT-UHFFFAOYSA-N 0.000 description 4
- YRIZYWQGELRKNT-UHFFFAOYSA-N 1,3,5-trichloro-1,3,5-triazinane-2,4,6-trione Chemical compound ClN1C(=O)N(Cl)C(=O)N(Cl)C1=O YRIZYWQGELRKNT-UHFFFAOYSA-N 0.000 description 3
- 239000007864 aqueous solution Substances 0.000 description 3
- 239000002002 slurry Substances 0.000 description 3
- 239000000110 cooling liquid Substances 0.000 description 2
- WQYVRQLZKVEZGA-UHFFFAOYSA-N hypochlorite Chemical compound Cl[O-] WQYVRQLZKVEZGA-UHFFFAOYSA-N 0.000 description 2
- QWPPOHNGKGFGJK-UHFFFAOYSA-N hypochlorous acid Chemical compound ClO QWPPOHNGKGFGJK-UHFFFAOYSA-N 0.000 description 2
- 238000012544 monitoring process Methods 0.000 description 2
- BASFCYQUMIYNBI-UHFFFAOYSA-N platinum Chemical compound [Pt] BASFCYQUMIYNBI-UHFFFAOYSA-N 0.000 description 2
- XAEFZNCEHLXOMS-UHFFFAOYSA-M potassium benzoate Chemical compound [K+].[O-]C(=O)C1=CC=CC=C1 XAEFZNCEHLXOMS-UHFFFAOYSA-M 0.000 description 2
- 239000012266 salt solution Substances 0.000 description 2
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 1
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 1
- VEXZGXHMUGYJMC-UHFFFAOYSA-M Chloride anion Chemical compound [Cl-] VEXZGXHMUGYJMC-UHFFFAOYSA-M 0.000 description 1
- KZBUYRJDOAKODT-UHFFFAOYSA-N Chlorine Chemical compound ClCl KZBUYRJDOAKODT-UHFFFAOYSA-N 0.000 description 1
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 description 1
- RTAQQCXQSZGOHL-UHFFFAOYSA-N Titanium Chemical compound [Ti] RTAQQCXQSZGOHL-UHFFFAOYSA-N 0.000 description 1
- 230000002378 acidificating effect Effects 0.000 description 1
- 229910001854 alkali hydroxide Inorganic materials 0.000 description 1
- 150000008044 alkali metal hydroxides Chemical class 0.000 description 1
- 238000013459 approach Methods 0.000 description 1
- 229940075397 calomel Drugs 0.000 description 1
- 239000007795 chemical reaction product Substances 0.000 description 1
- 230000006835 compression Effects 0.000 description 1
- 238000007906 compression Methods 0.000 description 1
- 238000010924 continuous production Methods 0.000 description 1
- 238000007796 conventional method Methods 0.000 description 1
- 238000002425 crystallisation Methods 0.000 description 1
- 230000008025 crystallization Effects 0.000 description 1
- ZOMNIUBKTOKEHS-UHFFFAOYSA-L dimercury dichloride Chemical compound Cl[Hg][Hg]Cl ZOMNIUBKTOKEHS-UHFFFAOYSA-L 0.000 description 1
- 238000009826 distribution Methods 0.000 description 1
- 239000012467 final product Substances 0.000 description 1
- 239000006260 foam Substances 0.000 description 1
- -1 glass Chemical compound 0.000 description 1
- 239000011521 glass Substances 0.000 description 1
- 229910002804 graphite Inorganic materials 0.000 description 1
- 239000010439 graphite Substances 0.000 description 1
- 238000010438 heat treatment Methods 0.000 description 1
- 238000002347 injection Methods 0.000 description 1
- 239000007924 injection Substances 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 230000007257 malfunction Effects 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 238000005259 measurement Methods 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 229910052697 platinum Inorganic materials 0.000 description 1
- 239000012429 reaction media Substances 0.000 description 1
- 150000003839 salts Chemical class 0.000 description 1
- 239000007921 spray Substances 0.000 description 1
- 238000003756 stirring Methods 0.000 description 1
- 229910052572 stoneware Inorganic materials 0.000 description 1
- 238000003860 storage Methods 0.000 description 1
- 229910052715 tantalum Inorganic materials 0.000 description 1
- GUVRBAGPIYLISA-UHFFFAOYSA-N tantalum atom Chemical compound [Ta] GUVRBAGPIYLISA-UHFFFAOYSA-N 0.000 description 1
- 229910052719 titanium Inorganic materials 0.000 description 1
- 239000010936 titanium Substances 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D251/00—Heterocyclic compounds containing 1,3,5-triazine rings
- C07D251/02—Heterocyclic compounds containing 1,3,5-triazine rings not condensed with other rings
- C07D251/12—Heterocyclic compounds containing 1,3,5-triazine rings not condensed with other rings having three double bonds between ring members or between ring members and non-ring members
- C07D251/26—Heterocyclic compounds containing 1,3,5-triazine rings not condensed with other rings having three double bonds between ring members or between ring members and non-ring members with only hetero atoms directly attached to ring carbon atoms
- C07D251/30—Only oxygen atoms
- C07D251/36—Only oxygen atoms having halogen atoms directly attached to ring nitrogen atoms
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| FR31004864 | 1963-03-04 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| DE1235932B true DE1235932B (de) | 1967-03-09 |
Family
ID=9691898
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DEO9988A Pending DE1235932B (de) | 1963-03-04 | 1964-02-27 | Vorrichtung zur Herstellung von Chlorderivaten der Cyanursaeure |
Country Status (6)
| Country | Link |
|---|---|
| BE (1) | BE644030A (enrdf_load_stackoverflow) |
| CH (1) | CH419156A (enrdf_load_stackoverflow) |
| DE (1) | DE1235932B (enrdf_load_stackoverflow) |
| GB (2) | GB1062821A (enrdf_load_stackoverflow) |
| LU (1) | LU45470A1 (enrdf_load_stackoverflow) |
| NL (1) | NL144934B (enrdf_load_stackoverflow) |
Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| FR1285286A (fr) * | 1960-12-19 | 1962-02-23 | Azote Office Nat Ind | Préparation d'acide trichlorocyanurique |
-
1964
- 1964-02-18 NL NL6401489A patent/NL144934B/xx not_active IP Right Cessation
- 1964-02-19 BE BE644030D patent/BE644030A/xx unknown
- 1964-02-20 LU LU45470A patent/LU45470A1/xx unknown
- 1964-02-27 DE DEO9988A patent/DE1235932B/de active Pending
- 1964-03-03 GB GB899264A patent/GB1062821A/en not_active Expired
- 1964-03-03 GB GB4386266A patent/GB1068007A/en not_active Expired
- 1964-03-04 CH CH272964A patent/CH419156A/fr unknown
Patent Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| FR1285286A (fr) * | 1960-12-19 | 1962-02-23 | Azote Office Nat Ind | Préparation d'acide trichlorocyanurique |
Also Published As
| Publication number | Publication date |
|---|---|
| CH419156A (fr) | 1966-08-31 |
| GB1068007A (en) | 1967-05-10 |
| BE644030A (enrdf_load_stackoverflow) | 1964-06-15 |
| LU45470A1 (enrdf_load_stackoverflow) | 1964-04-20 |
| GB1062821A (en) | 1967-03-22 |
| NL144934B (nl) | 1975-02-17 |
| NL6401489A (enrdf_load_stackoverflow) | 1964-09-07 |
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