DE1212074B - Verfahren zur Herstellung von fluessigem Polythioformaldehyd - Google Patents
Verfahren zur Herstellung von fluessigem PolythioformaldehydInfo
- Publication number
- DE1212074B DE1212074B DES90135A DES0090135A DE1212074B DE 1212074 B DE1212074 B DE 1212074B DE S90135 A DES90135 A DE S90135A DE S0090135 A DES0090135 A DE S0090135A DE 1212074 B DE1212074 B DE 1212074B
- Authority
- DE
- Germany
- Prior art keywords
- liquid
- polythioformaldehyde
- hydrogen sulfide
- reaction
- products
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- 239000007788 liquid Substances 0.000 title claims description 19
- 238000000034 method Methods 0.000 title claims description 10
- 238000004519 manufacturing process Methods 0.000 title description 4
- WSFSSNUMVMOOMR-UHFFFAOYSA-N Formaldehyde Chemical compound O=C WSFSSNUMVMOOMR-UHFFFAOYSA-N 0.000 claims description 31
- RWSOTUBLDIXVET-UHFFFAOYSA-N Dihydrogen sulfide Chemical compound S RWSOTUBLDIXVET-UHFFFAOYSA-N 0.000 claims description 10
- 238000006243 chemical reaction Methods 0.000 claims description 9
- 229910000037 hydrogen sulfide Inorganic materials 0.000 claims description 9
- 239000008098 formaldehyde solution Substances 0.000 claims description 5
- 238000001816 cooling Methods 0.000 claims description 3
- 238000002360 preparation method Methods 0.000 claims description 2
- 239000000047 product Substances 0.000 description 16
- NINIDFKCEFEMDL-UHFFFAOYSA-N Sulfur Chemical compound [S] NINIDFKCEFEMDL-UHFFFAOYSA-N 0.000 description 6
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 6
- 239000007789 gas Substances 0.000 description 6
- 239000001301 oxygen Substances 0.000 description 6
- 229910052760 oxygen Inorganic materials 0.000 description 6
- 239000000243 solution Substances 0.000 description 6
- 229910052717 sulfur Inorganic materials 0.000 description 6
- 239000011593 sulfur Substances 0.000 description 6
- 239000011541 reaction mixture Substances 0.000 description 5
- 229920006395 saturated elastomer Polymers 0.000 description 4
- 239000000203 mixture Substances 0.000 description 3
- 239000000126 substance Substances 0.000 description 3
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 3
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 2
- DBTDEFJAFBUGPP-UHFFFAOYSA-N Methanethial Chemical compound S=C DBTDEFJAFBUGPP-UHFFFAOYSA-N 0.000 description 2
- 150000001875 compounds Chemical class 0.000 description 2
- 150000004662 dithiols Chemical class 0.000 description 2
- 238000002329 infrared spectrum Methods 0.000 description 2
- CXWGKAYMVASWDQ-UHFFFAOYSA-N 1,2-dithiane Chemical compound C1CCSSC1 CXWGKAYMVASWDQ-UHFFFAOYSA-N 0.000 description 1
- 239000002253 acid Substances 0.000 description 1
- 150000007513 acids Chemical class 0.000 description 1
- 239000008346 aqueous phase Substances 0.000 description 1
- 239000007864 aqueous solution Substances 0.000 description 1
- 150000001923 cyclic compounds Chemical class 0.000 description 1
- 238000010908 decantation Methods 0.000 description 1
- LOZWAPSEEHRYPG-UHFFFAOYSA-N dithiane Natural products C1CSCCS1 LOZWAPSEEHRYPG-UHFFFAOYSA-N 0.000 description 1
- 229920001971 elastomer Polymers 0.000 description 1
- 239000008246 gaseous mixture Substances 0.000 description 1
- 238000010438 heat treatment Methods 0.000 description 1
- 230000007062 hydrolysis Effects 0.000 description 1
- 238000006460 hydrolysis reaction Methods 0.000 description 1
- 239000007791 liquid phase Substances 0.000 description 1
- 239000012263 liquid product Substances 0.000 description 1
- 229910052757 nitrogen Inorganic materials 0.000 description 1
- 239000012044 organic layer Substances 0.000 description 1
- 230000001590 oxidative effect Effects 0.000 description 1
- 125000004430 oxygen atom Chemical group O* 0.000 description 1
- 238000006068 polycondensation reaction Methods 0.000 description 1
- 229920000642 polymer Polymers 0.000 description 1
- 238000006116 polymerization reaction Methods 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
- 238000004073 vulcanization Methods 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C321/00—Thiols, sulfides, hydropolysulfides or polysulfides
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
- C08F36/00—Homopolymers and copolymers of compounds having one or more unsaturated aliphatic radicals, at least one having two or more carbon-to-carbon double bonds
- C08F36/02—Homopolymers and copolymers of compounds having one or more unsaturated aliphatic radicals, at least one having two or more carbon-to-carbon double bonds the radical having only two carbon-to-carbon double bonds
- C08F36/04—Homopolymers and copolymers of compounds having one or more unsaturated aliphatic radicals, at least one having two or more carbon-to-carbon double bonds the radical having only two carbon-to-carbon double bonds conjugated
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G75/00—Macromolecular compounds obtained by reactions forming a linkage containing sulfur with or without nitrogen, oxygen, or carbon in the main chain of the macromolecule
- C08G75/02—Polythioethers
- C08G75/10—Polythioethers from sulfur or sulfur-containing compounds and aldehydes or ketones
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L21/00—Compositions of unspecified rubbers
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Health & Medical Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Phenolic Resins Or Amino Resins (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| FR928770A FR1362500A (fr) | 1963-03-21 | 1963-03-21 | Polythioformaldéhydes liquides |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| DE1212074B true DE1212074B (de) | 1966-03-10 |
Family
ID=8799761
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DES90135A Pending DE1212074B (de) | 1963-03-21 | 1964-03-20 | Verfahren zur Herstellung von fluessigem Polythioformaldehyd |
Country Status (8)
| Country | Link |
|---|---|
| US (1) | US3326982A (enrdf_load_html_response) |
| BE (1) | BE645515A (enrdf_load_html_response) |
| DE (1) | DE1212074B (enrdf_load_html_response) |
| FR (1) | FR1362500A (enrdf_load_html_response) |
| GB (1) | GB1028101A (enrdf_load_html_response) |
| LU (1) | LU45710A1 (enrdf_load_html_response) |
| NL (1) | NL6402979A (enrdf_load_html_response) |
| OA (1) | OA00027A (enrdf_load_html_response) |
Families Citing this family (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| FR1465475A (fr) * | 1965-10-26 | 1967-01-13 | Aquitaine Petrole | Mercapto trithiométhylène et sa préparation |
| FR1527701A (fr) * | 1966-05-09 | 1968-06-07 | Aquitaine Petrole | Perfectionnement à la préparation de dithiols polythioéthers |
Family Cites Families (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CA639724A (en) * | 1962-04-10 | E.I. Du Pont De Nemours And Company | Crystalline poly(methylene sulfide) and process for its preparation | |
| US1991765A (en) * | 1932-01-23 | 1935-02-19 | Dupont Viscoloid Company | Aldehyde-hydrogen sulphide reaction product |
| US3070580A (en) * | 1959-07-16 | 1962-12-25 | Du Pont | Crystalline poly (methylene sulfide) and process for its preparation |
| US3056841A (en) * | 1961-09-06 | 1962-10-02 | Du Pont | Process for preparing mercapto-terminated thiomethylene compounds |
-
1963
- 1963-03-21 FR FR928770A patent/FR1362500A/fr not_active Expired
-
1964
- 1964-03-20 DE DES90135A patent/DE1212074B/de active Pending
- 1964-03-20 GB GB11895/64A patent/GB1028101A/en not_active Expired
- 1964-03-20 LU LU45710A patent/LU45710A1/xx unknown
- 1964-03-20 NL NL6402979A patent/NL6402979A/xx unknown
- 1964-03-20 BE BE645515A patent/BE645515A/xx unknown
- 1964-03-20 US US353598A patent/US3326982A/en not_active Expired - Lifetime
- 1964-03-21 OA OA50031A patent/OA00027A/xx unknown
Also Published As
| Publication number | Publication date |
|---|---|
| FR1362500A (fr) | 1964-06-05 |
| NL6402979A (enrdf_load_html_response) | 1964-09-22 |
| BE645515A (enrdf_load_html_response) | 1964-09-21 |
| US3326982A (en) | 1967-06-20 |
| GB1028101A (en) | 1966-05-04 |
| LU45710A1 (enrdf_load_html_response) | 1964-09-20 |
| OA00027A (fr) | 1966-01-15 |
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