DE1161419B - Verfahren zur Herstellung von Alkylwasserstoff-polysiloxanemulsionen - Google Patents
Verfahren zur Herstellung von Alkylwasserstoff-polysiloxanemulsionenInfo
- Publication number
- DE1161419B DE1161419B DEF35646A DEF0035646A DE1161419B DE 1161419 B DE1161419 B DE 1161419B DE F35646 A DEF35646 A DE F35646A DE F0035646 A DEF0035646 A DE F0035646A DE 1161419 B DE1161419 B DE 1161419B
- Authority
- DE
- Germany
- Prior art keywords
- emulsions
- carboxylic acids
- alkyl hydrogen
- preparation
- emulsion
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- 239000000839 emulsion Substances 0.000 title claims description 30
- -1 alkyl hydrogen Chemical compound 0.000 title claims description 20
- 229910052739 hydrogen Inorganic materials 0.000 title claims description 15
- 239000001257 hydrogen Substances 0.000 title claims description 15
- 229920001296 polysiloxane Polymers 0.000 title claims description 13
- 238000000034 method Methods 0.000 title claims description 4
- 238000002360 preparation method Methods 0.000 title description 4
- 150000001735 carboxylic acids Chemical class 0.000 claims description 8
- 239000000203 mixture Substances 0.000 claims description 7
- 125000005210 alkyl ammonium group Chemical group 0.000 claims description 5
- 239000003995 emulsifying agent Substances 0.000 claims description 5
- 238000004519 manufacturing process Methods 0.000 claims description 3
- 125000002924 primary amino group Chemical group [H]N([H])* 0.000 claims description 3
- 150000003839 salts Chemical class 0.000 claims description 3
- 150000003973 alkyl amines Chemical class 0.000 claims description 2
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 description 9
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 description 6
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 6
- 239000007789 gas Substances 0.000 description 5
- 239000003921 oil Substances 0.000 description 5
- 238000003756 stirring Methods 0.000 description 5
- 239000000243 solution Substances 0.000 description 4
- XOAAWQZATWQOTB-UHFFFAOYSA-N taurine Chemical compound NCCS(O)(=O)=O XOAAWQZATWQOTB-UHFFFAOYSA-N 0.000 description 4
- KXDHJXZQYSOELW-UHFFFAOYSA-N Carbamic acid Chemical class NC(O)=O KXDHJXZQYSOELW-UHFFFAOYSA-N 0.000 description 3
- OFOBLEOULBTSOW-UHFFFAOYSA-N Malonic acid Chemical compound OC(=O)CC(O)=O OFOBLEOULBTSOW-UHFFFAOYSA-N 0.000 description 3
- 150000001412 amines Chemical class 0.000 description 3
- 239000000872 buffer Substances 0.000 description 3
- SXPWTBGAZSPLHA-UHFFFAOYSA-M cetalkonium chloride Chemical compound [Cl-].CCCCCCCCCCCCCCCC[N+](C)(C)CC1=CC=CC=C1 SXPWTBGAZSPLHA-UHFFFAOYSA-M 0.000 description 3
- 229960000228 cetalkonium chloride Drugs 0.000 description 3
- 239000003795 chemical substances by application Substances 0.000 description 3
- KRKNYBCHXYNGOX-UHFFFAOYSA-N citric acid Chemical compound OC(=O)CC(O)(C(O)=O)CC(O)=O KRKNYBCHXYNGOX-UHFFFAOYSA-N 0.000 description 3
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 3
- SLXKOJJOQWFEFD-UHFFFAOYSA-N 6-aminohexanoic acid Chemical compound NCCCCCC(O)=O SLXKOJJOQWFEFD-UHFFFAOYSA-N 0.000 description 2
- QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 description 2
- WHUUTDBJXJRKMK-UHFFFAOYSA-N Glutamic acid Natural products OC(=O)C(N)CCC(O)=O WHUUTDBJXJRKMK-UHFFFAOYSA-N 0.000 description 2
- 125000000217 alkyl group Chemical group 0.000 description 2
- 235000001014 amino acid Nutrition 0.000 description 2
- 150000001413 amino acids Chemical class 0.000 description 2
- 229960002684 aminocaproic acid Drugs 0.000 description 2
- 150000001875 compounds Chemical class 0.000 description 2
- KPUWHANPEXNPJT-UHFFFAOYSA-N disiloxane Chemical class [SiH3]O[SiH3] KPUWHANPEXNPJT-UHFFFAOYSA-N 0.000 description 2
- 235000013922 glutamic acid Nutrition 0.000 description 2
- 239000004220 glutamic acid Substances 0.000 description 2
- 238000005470 impregnation Methods 0.000 description 2
- 238000005259 measurement Methods 0.000 description 2
- 125000002496 methyl group Chemical group [H]C([H])([H])* 0.000 description 2
- IWZKICVEHNUQTL-UHFFFAOYSA-M potassium hydrogen phthalate Chemical compound [K+].OC(=O)C1=CC=CC=C1C([O-])=O IWZKICVEHNUQTL-UHFFFAOYSA-M 0.000 description 2
- 239000005871 repellent Substances 0.000 description 2
- 229960003080 taurine Drugs 0.000 description 2
- 238000012360 testing method Methods 0.000 description 2
- 239000004753 textile Substances 0.000 description 2
- QXSZNDIIPUOQMB-UHFFFAOYSA-N 1,1,2,2-tetrabromoethane Chemical compound BrC(Br)C(Br)Br QXSZNDIIPUOQMB-UHFFFAOYSA-N 0.000 description 1
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical group [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 1
- DHMQDGOQFOQNFH-UHFFFAOYSA-N Glycine Chemical compound NCC(O)=O DHMQDGOQFOQNFH-UHFFFAOYSA-N 0.000 description 1
- 239000004372 Polyvinyl alcohol Substances 0.000 description 1
- 229960000583 acetic acid Drugs 0.000 description 1
- 239000000654 additive Substances 0.000 description 1
- 150000001350 alkyl halides Chemical class 0.000 description 1
- 230000003139 buffering effect Effects 0.000 description 1
- FOCAUTSVDIKZOP-UHFFFAOYSA-N chloroacetic acid Chemical compound OC(=O)CCl FOCAUTSVDIKZOP-UHFFFAOYSA-N 0.000 description 1
- 238000003776 cleavage reaction Methods 0.000 description 1
- 239000000084 colloidal system Substances 0.000 description 1
- 230000000052 comparative effect Effects 0.000 description 1
- 239000003431 cross linking reagent Substances 0.000 description 1
- 238000011161 development Methods 0.000 description 1
- 235000014113 dietary fatty acids Nutrition 0.000 description 1
- 238000010790 dilution Methods 0.000 description 1
- 239000012895 dilution Substances 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 230000008030 elimination Effects 0.000 description 1
- 238000003379 elimination reaction Methods 0.000 description 1
- 150000002148 esters Chemical class 0.000 description 1
- 238000002474 experimental method Methods 0.000 description 1
- 239000000194 fatty acid Substances 0.000 description 1
- 229930195729 fatty acid Natural products 0.000 description 1
- 150000004665 fatty acids Chemical class 0.000 description 1
- 230000002349 favourable effect Effects 0.000 description 1
- 239000002657 fibrous material Substances 0.000 description 1
- 239000012362 glacial acetic acid Substances 0.000 description 1
- 235000013905 glycine and its sodium salt Nutrition 0.000 description 1
- 238000010438 heat treatment Methods 0.000 description 1
- XMBWDFGMSWQBCA-UHFFFAOYSA-N hydrogen iodide Chemical compound I XMBWDFGMSWQBCA-UHFFFAOYSA-N 0.000 description 1
- 230000003301 hydrolyzing effect Effects 0.000 description 1
- VZCYOOQTPOCHFL-UPHRSURJSA-N maleic acid Chemical compound OC(=O)\C=C/C(O)=O VZCYOOQTPOCHFL-UPHRSURJSA-N 0.000 description 1
- 239000011976 maleic acid Substances 0.000 description 1
- 239000003960 organic solvent Substances 0.000 description 1
- 229920000642 polymer Polymers 0.000 description 1
- 229920002451 polyvinyl alcohol Polymers 0.000 description 1
- 150000003141 primary amines Chemical class 0.000 description 1
- 230000001681 protective effect Effects 0.000 description 1
- 230000009257 reactivity Effects 0.000 description 1
- 230000007017 scission Effects 0.000 description 1
- 150000003335 secondary amines Chemical class 0.000 description 1
- 238000005204 segregation Methods 0.000 description 1
- 239000000344 soap Substances 0.000 description 1
- 239000001509 sodium citrate Substances 0.000 description 1
- NLJMYIDDQXHKNR-UHFFFAOYSA-K sodium citrate Chemical compound O.O.[Na+].[Na+].[Na+].[O-]C(=O)CC(O)(CC([O-])=O)C([O-])=O NLJMYIDDQXHKNR-UHFFFAOYSA-K 0.000 description 1
- 230000000087 stabilizing effect Effects 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- IIACRCGMVDHOTQ-UHFFFAOYSA-N sulfamic acid Chemical compound NS(O)(=O)=O IIACRCGMVDHOTQ-UHFFFAOYSA-N 0.000 description 1
- VZCYOOQTPOCHFL-UHFFFAOYSA-N trans-butenedioic acid Natural products OC(=O)C=CC(O)=O VZCYOOQTPOCHFL-UHFFFAOYSA-N 0.000 description 1
- 229910052845 zircon Inorganic materials 0.000 description 1
- GFQYVLUOOAAOGM-UHFFFAOYSA-N zirconium(iv) silicate Chemical compound [Zr+4].[O-][Si]([O-])([O-])[O-] GFQYVLUOOAAOGM-UHFFFAOYSA-N 0.000 description 1
Classifications
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
- D06M15/19—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with synthetic macromolecular compounds
- D06M15/37—Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
- D06M15/643—Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds containing silicon in the main chain
- D06M15/6436—Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds containing silicon in the main chain containing amino groups
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K5/00—Use of organic ingredients
- C08K5/16—Nitrogen-containing compounds
- C08K5/17—Amines; Quaternary ammonium compounds
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L83/00—Compositions of macromolecular compounds obtained by reactions forming in the main chain of the macromolecule a linkage containing silicon with or without sulfur, nitrogen, oxygen or carbon only; Compositions of derivatives of such polymers
- C08L83/04—Polysiloxanes
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G77/00—Macromolecular compounds obtained by reactions forming a linkage containing silicon with or without sulfur, nitrogen, oxygen or carbon in the main chain of the macromolecule
- C08G77/04—Polysiloxanes
- C08G77/12—Polysiloxanes containing silicon bound to hydrogen
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G77/00—Macromolecular compounds obtained by reactions forming a linkage containing silicon with or without sulfur, nitrogen, oxygen or carbon in the main chain of the macromolecule
- C08G77/04—Polysiloxanes
- C08G77/22—Polysiloxanes containing silicon bound to organic groups containing atoms other than carbon, hydrogen and oxygen
- C08G77/24—Polysiloxanes containing silicon bound to organic groups containing atoms other than carbon, hydrogen and oxygen halogen-containing groups
Landscapes
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Health & Medical Sciences (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Organic Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Textile Engineering (AREA)
- Treatments For Attaching Organic Compounds To Fibrous Goods (AREA)
- Colloid Chemistry (AREA)
- Compositions Of Macromolecular Compounds (AREA)
Priority Applications (9)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| BE626395D BE626395A (US07655688-20100202-C00086.png) | 1961-12-23 | ||
| NL286535D NL286535A (US07655688-20100202-C00086.png) | 1961-12-23 | ||
| DEF35646A DE1161419B (de) | 1961-12-23 | 1961-12-23 | Verfahren zur Herstellung von Alkylwasserstoff-polysiloxanemulsionen |
| CH1356962A CH439724A (de) | 1961-12-23 | 1962-11-20 | Verfahren zur Herstellung Alkylwasserstoffpolysiloxane enthaltender wässeriger Emulsionen |
| AT944462A AT247602B (de) | 1961-12-23 | 1962-12-03 | Verfahren zur Herstellung Alkylwasserstoffpolysiloxane enthaltender wässeriger Emmulsionen |
| NL62286535A NL140554B (nl) | 1961-12-23 | 1962-12-10 | Werkwijze voor de bereiding van alkylwaterstofpolysiloxanen bevattende waterrijke emulsies, werkwijze voor het waterafstotend maken van textielmateriaal, alsmede verkregen waterafstotend gemaakte gevormde textielvoortbrengselen. |
| US244002A US3306759A (en) | 1961-12-23 | 1962-12-12 | Alkyl-hydrogen-polysiloxane emulsions |
| GB47128/62A GB967614A (en) | 1961-12-23 | 1962-12-20 | Alkyl-hydrogen-polysiloxane emulsions |
| FR919384A FR1341924A (fr) | 1961-12-23 | 1962-12-21 | émulsions d'alkylhydrogénopolysiloxane |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DEF35646A DE1161419B (de) | 1961-12-23 | 1961-12-23 | Verfahren zur Herstellung von Alkylwasserstoff-polysiloxanemulsionen |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| DE1161419B true DE1161419B (de) | 1964-01-16 |
Family
ID=7096087
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DEF35646A Pending DE1161419B (de) | 1961-12-23 | 1961-12-23 | Verfahren zur Herstellung von Alkylwasserstoff-polysiloxanemulsionen |
Country Status (7)
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4179426A (en) * | 1977-01-18 | 1979-12-18 | Bayer Aktiengesellschaft | Stable alkylhydridopolysiloxane emulsions |
| DE3215936A1 (de) * | 1982-04-29 | 1983-11-03 | Chemische Fabrik Pfersee Gmbh, 8900 Augsburg | Waessrige textilbehandlungsflotte und deren stabilisierung |
| US6184406B1 (en) | 1997-07-11 | 2001-02-06 | Wacker-Chemie Gmbh | Aqueous emulsions containing organohydropolysiloxanes |
Families Citing this family (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE2631419A1 (de) * | 1975-07-16 | 1977-02-03 | Procter & Gamble Europ | Zusammensetzungen fuer die textilbehandlung |
| GB1570983A (en) * | 1976-06-26 | 1980-07-09 | Dow Corning Ltd | Process for treating fibres |
| US4748104A (en) * | 1986-11-10 | 1988-05-31 | Macdermid, Incorporated | Selective metallization process and additive method for manufactured printed circuit boards |
| US5126072A (en) * | 1987-10-21 | 1992-06-30 | General Electric Company | Stable, two package water emulsions of silicone hydride fluids |
| US5086146A (en) * | 1990-09-07 | 1992-02-04 | Dow Corning Corporation | Methylalkoxy-methylalkyl cyclosiloxane copolymer |
| US5074912A (en) * | 1990-09-07 | 1991-12-24 | Dow Corning Corporation | Siloxane masonry water repellent emulsions |
| US20090163606A1 (en) * | 2007-12-20 | 2009-06-25 | Glen Harold Kirby | Additives for controlled dispersion of aqueous suspensions and suspension comprising such additives |
| US20090170962A1 (en) * | 2007-12-20 | 2009-07-02 | Glen Harold Kirby | Methods for controlling dispersion of aqueous suspensions |
| JP5128978B2 (ja) * | 2008-02-07 | 2013-01-23 | 玉理化学株式会社 | 毛髪コンディショニング剤およびこれを用いた毛髪のコンディショニング方法 |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE900018C (de) * | 1952-08-07 | 1953-12-17 | Goldschmidt Ag Th | Verfahren zur Herstellung von waessrigen Emulsionen von Polysiloxanen |
| FR1125918A (fr) * | 1954-09-03 | 1956-11-12 | Perfectionnements aux compositions à base de silicone |
Family Cites Families (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| BE527292A (US07655688-20100202-C00086.png) * | 1953-03-16 | |||
| DE1125878B (de) * | 1954-03-13 | 1962-03-22 | Wacker Chemie Gmbh | Impraegnierungsmittel auf der Basis von Organopolysiloxanen mit Haertungsmittel fuerTextilien aus Natur- und Kunstfasern |
-
0
- BE BE626395D patent/BE626395A/xx unknown
- NL NL286535D patent/NL286535A/xx unknown
-
1961
- 1961-12-23 DE DEF35646A patent/DE1161419B/de active Pending
-
1962
- 1962-11-20 CH CH1356962A patent/CH439724A/de unknown
- 1962-12-03 AT AT944462A patent/AT247602B/de active
- 1962-12-10 NL NL62286535A patent/NL140554B/xx not_active IP Right Cessation
- 1962-12-12 US US244002A patent/US3306759A/en not_active Expired - Lifetime
- 1962-12-20 GB GB47128/62A patent/GB967614A/en not_active Expired
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE900018C (de) * | 1952-08-07 | 1953-12-17 | Goldschmidt Ag Th | Verfahren zur Herstellung von waessrigen Emulsionen von Polysiloxanen |
| FR1125918A (fr) * | 1954-09-03 | 1956-11-12 | Perfectionnements aux compositions à base de silicone |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4179426A (en) * | 1977-01-18 | 1979-12-18 | Bayer Aktiengesellschaft | Stable alkylhydridopolysiloxane emulsions |
| DE3215936A1 (de) * | 1982-04-29 | 1983-11-03 | Chemische Fabrik Pfersee Gmbh, 8900 Augsburg | Waessrige textilbehandlungsflotte und deren stabilisierung |
| US6184406B1 (en) | 1997-07-11 | 2001-02-06 | Wacker-Chemie Gmbh | Aqueous emulsions containing organohydropolysiloxanes |
Also Published As
| Publication number | Publication date |
|---|---|
| GB967614A (en) | 1964-08-26 |
| NL140554B (nl) | 1973-12-17 |
| CH439724A (de) | 1967-07-15 |
| BE626395A (US07655688-20100202-C00086.png) | |
| US3306759A (en) | 1967-02-28 |
| AT247602B (de) | 1966-06-27 |
| NL286535A (US07655688-20100202-C00086.png) |
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