DE1158516B - Verfahren zur Herstellung von Alkylaluminiumsesquichlorid - Google Patents
Verfahren zur Herstellung von AlkylaluminiumsesquichloridInfo
- Publication number
- DE1158516B DE1158516B DES72763A DES0072763A DE1158516B DE 1158516 B DE1158516 B DE 1158516B DE S72763 A DES72763 A DE S72763A DE S0072763 A DES0072763 A DE S0072763A DE 1158516 B DE1158516 B DE 1158516B
- Authority
- DE
- Germany
- Prior art keywords
- aluminum
- reaction
- sesquichloride
- ticl
- ethyl
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- 238000000034 method Methods 0.000 title claims description 8
- 125000005234 alkyl aluminium group Chemical group 0.000 title claims description 4
- 238000006243 chemical reaction Methods 0.000 claims description 38
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 claims description 35
- 229910052782 aluminium Inorganic materials 0.000 claims description 30
- XJDNKRIXUMDJCW-UHFFFAOYSA-J titanium tetrachloride Chemical compound Cl[Ti](Cl)(Cl)Cl XJDNKRIXUMDJCW-UHFFFAOYSA-J 0.000 claims description 8
- 125000001495 ethyl group Chemical group [H]C([H])([H])C([H])([H])* 0.000 claims description 7
- 125000004177 diethyl group Chemical group [H]C([H])([H])C([H])([H])* 0.000 claims description 6
- WADSLQQIOJIXTB-UHFFFAOYSA-L dichloroalumane Chemical compound Cl[AlH]Cl WADSLQQIOJIXTB-UHFFFAOYSA-L 0.000 claims description 5
- 150000001348 alkyl chlorides Chemical class 0.000 claims description 2
- 238000004519 manufacturing process Methods 0.000 claims description 2
- HYZXMVILOKSUKA-UHFFFAOYSA-K chloro(dimethyl)alumane;dichloro(methyl)alumane Chemical compound C[Al](C)Cl.C[Al](Cl)Cl HYZXMVILOKSUKA-UHFFFAOYSA-K 0.000 claims 1
- 239000000203 mixture Substances 0.000 description 15
- VSCWAEJMTAWNJL-UHFFFAOYSA-K aluminium trichloride Chemical compound Cl[Al](Cl)Cl VSCWAEJMTAWNJL-UHFFFAOYSA-K 0.000 description 6
- 241001676573 Minium Species 0.000 description 4
- 239000007795 chemical reaction product Substances 0.000 description 4
- HRYZWHHZPQKTII-UHFFFAOYSA-N chloroethane Chemical compound CCCl HRYZWHHZPQKTII-UHFFFAOYSA-N 0.000 description 4
- 229960003750 ethyl chloride Drugs 0.000 description 4
- 239000007789 gas Substances 0.000 description 4
- 239000002994 raw material Substances 0.000 description 4
- VEXZGXHMUGYJMC-UHFFFAOYSA-M Chloride anion Chemical compound [Cl-] VEXZGXHMUGYJMC-UHFFFAOYSA-M 0.000 description 3
- -1 alkyl aluminum halide Chemical class 0.000 description 3
- 239000003999 initiator Substances 0.000 description 3
- 238000010521 absorption reaction Methods 0.000 description 2
- YNLAOSYQHBDIKW-UHFFFAOYSA-M diethylaluminium chloride Chemical compound CC[Al](Cl)CC YNLAOSYQHBDIKW-UHFFFAOYSA-M 0.000 description 2
- 239000000047 product Substances 0.000 description 2
- 239000011541 reaction mixture Substances 0.000 description 2
- WSLDOOZREJYCGB-UHFFFAOYSA-N 1,2-Dichloroethane Chemical compound ClCCCl WSLDOOZREJYCGB-UHFFFAOYSA-N 0.000 description 1
- QGZKDVFQNNGYKY-UHFFFAOYSA-O Ammonium Chemical compound [NH4+] QGZKDVFQNNGYKY-UHFFFAOYSA-O 0.000 description 1
- 230000004913 activation Effects 0.000 description 1
- 238000013459 approach Methods 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 239000006227 byproduct Substances 0.000 description 1
- 239000003054 catalyst Substances 0.000 description 1
- 230000003197 catalytic effect Effects 0.000 description 1
- SOGXWMAAMKKQCB-UHFFFAOYSA-M chloroalumane Chemical compound Cl[AlH2] SOGXWMAAMKKQCB-UHFFFAOYSA-M 0.000 description 1
- 238000011109 contamination Methods 0.000 description 1
- 125000003963 dichloro group Chemical group Cl* 0.000 description 1
- UAIZDWNSWGTKFZ-UHFFFAOYSA-L ethylaluminum(2+);dichloride Chemical compound CC[Al](Cl)Cl UAIZDWNSWGTKFZ-UHFFFAOYSA-L 0.000 description 1
- 238000002474 experimental method Methods 0.000 description 1
- 239000012299 nitrogen atmosphere Substances 0.000 description 1
- 238000006116 polymerization reaction Methods 0.000 description 1
- 239000004711 α-olefin Substances 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
- C07F5/00—Compounds containing elements of Groups 3 or 13 of the Periodic Table
- C07F5/06—Aluminium compounds
- C07F5/061—Aluminium compounds with C-aluminium linkage
- C07F5/064—Aluminium compounds with C-aluminium linkage compounds with an Al-Halogen linkage
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Catalysts (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| FR819881A FR1258294A (fr) | 1960-02-29 | 1960-02-29 | Perfectionnement au procédé d'alkylation de l'aluminium |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| DE1158516B true DE1158516B (de) | 1963-12-05 |
Family
ID=8726005
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DES72763A Pending DE1158516B (de) | 1960-02-29 | 1961-02-28 | Verfahren zur Herstellung von Alkylaluminiumsesquichlorid |
Country Status (4)
| Country | Link |
|---|---|
| BE (1) | BE600749A (fr) |
| DE (1) | DE1158516B (fr) |
| FR (1) | FR1258294A (fr) |
| GB (1) | GB906229A (fr) |
Families Citing this family (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN112480159A (zh) * | 2020-12-31 | 2021-03-12 | 江苏爱姆欧光电材料有限公司 | 一种倍半甲基氯化铝的连续生产工艺 |
Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE1059450B (de) * | 1956-07-26 | 1959-06-18 | Distillers Co Yeast Ltd | Verfahren zur Herstellung von Alkylaluminiumsesquichloriden |
-
1960
- 1960-02-29 FR FR819881A patent/FR1258294A/fr not_active Expired
-
1961
- 1961-02-28 DE DES72763A patent/DE1158516B/de active Pending
- 1961-02-28 BE BE600749A patent/BE600749A/fr unknown
- 1961-02-28 GB GB726761A patent/GB906229A/en not_active Expired
Patent Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE1059450B (de) * | 1956-07-26 | 1959-06-18 | Distillers Co Yeast Ltd | Verfahren zur Herstellung von Alkylaluminiumsesquichloriden |
Also Published As
| Publication number | Publication date |
|---|---|
| GB906229A (en) | 1962-09-19 |
| BE600749A (fr) | 1961-06-16 |
| FR1258294A (fr) | 1961-04-14 |
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