DE111384C - - Google Patents

Info

Publication number

DE111384C

DE111384C DENDAT111384D DE111384DA DE111384C DE 111384 C DE111384 C DE 111384C DE NDAT111384 D DENDAT111384 D DE NDAT111384D DE 111384D A DE111384D A DE 111384DA DE 111384 C DE111384 C DE 111384C

Authority

DE

Germany

Prior art keywords

nitrobenzyl

azoxybenzylidene

toluidine

bases

nitrobenzylaniline

Prior art date

Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)

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• PAYRUJLWNCNPSJ-UHFFFAOYSA-N Aniline Chemical compound NC1=CC=CC=C1 PAYRUJLWNCNPSJ-UHFFFAOYSA-N 0.000 claims description 8
• QBSRKOBMKFOHOS-UHFFFAOYSA-N n-benzyl-4-nitroaniline Chemical compound C1=CC([N+](=O)[O-])=CC=C1NCC1=CC=CC=C1 QBSRKOBMKFOHOS-UHFFFAOYSA-N 0.000 claims description 4
• NINIDFKCEFEMDL-UHFFFAOYSA-N Sulfur Chemical compound [S] NINIDFKCEFEMDL-UHFFFAOYSA-N 0.000 claims description 2
• WPJTZCLHFWRBBC-UHFFFAOYSA-N n-benzyl-2-methyl-4-nitroaniline Chemical compound CC1=CC([N+]([O-])=O)=CC=C1NCC1=CC=CC=C1 WPJTZCLHFWRBBC-UHFFFAOYSA-N 0.000 claims description 2
• 239000011593 sulfur Substances 0.000 claims description 2
• 229910052717 sulfur Inorganic materials 0.000 claims description 2
• JILLTPMLOFHSQV-UHFFFAOYSA-N CC1(CC=C(NCC2=CC=CC=C2)C=C1)[N+](=O)[O-] Chemical compound CC1(CC=C(NCC2=CC=CC=C2)C=C1)[N+](=O)[O-] JILLTPMLOFHSQV-UHFFFAOYSA-N 0.000 claims 1
• YSCKLEJDBQLRSW-UHFFFAOYSA-N [N+](=O)([O-])C1=C(C(=C(NCC2=CC=CC=C2)C=C1)C)C Chemical group [N+](=O)([O-])C1=C(C(=C(NCC2=CC=CC=C2)C=C1)C)C YSCKLEJDBQLRSW-UHFFFAOYSA-N 0.000 claims 1
• 125000006503 p-nitrobenzyl group Chemical group [H]C1=C([H])C(=C([H])C([H])=C1[N+]([O-])=O)C([H])([H])* 0.000 claims 1
• HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 6
• UHOVQNZJYSORNB-UHFFFAOYSA-N Benzene Chemical compound C1=CC=CC=C1 UHOVQNZJYSORNB-UHFFFAOYSA-N 0.000 description 3
• LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 3
• YXFVVABEGXRONW-UHFFFAOYSA-N Toluene Chemical compound CC1=CC=CC=C1 YXFVVABEGXRONW-UHFFFAOYSA-N 0.000 description 3
• 239000002253 acid Substances 0.000 description 2
• 150000007513 acids Chemical class 0.000 description 2
• 238000006243 chemical reaction Methods 0.000 description 2
• 150000001875 compounds Chemical class 0.000 description 2
• 239000000975 dye Substances 0.000 description 2
• 229910052500 inorganic mineral Inorganic materials 0.000 description 2
• 239000007788 liquid Substances 0.000 description 2
• 239000011707 mineral Substances 0.000 description 2
• 235000010755 mineral Nutrition 0.000 description 2
• KWYUFKZDYYNOTN-UHFFFAOYSA-M potassium hydroxide Inorganic materials [OH-].[K+] KWYUFKZDYYNOTN-UHFFFAOYSA-M 0.000 description 2
• 235000011121 sodium hydroxide Nutrition 0.000 description 2
• CDULGHZNHURECF-UHFFFAOYSA-N 2,3-dimethylaniline 2,4-dimethylaniline 2,5-dimethylaniline 2,6-dimethylaniline 3,4-dimethylaniline 3,5-dimethylaniline Chemical group CC1=CC=C(N)C(C)=C1.CC1=CC=C(C)C(N)=C1.CC1=CC(C)=CC(N)=C1.CC1=CC=C(N)C=C1C.CC1=CC=CC(N)=C1C.CC1=CC=CC(C)=C1N CDULGHZNHURECF-UHFFFAOYSA-N 0.000 description 1
• FFRBMBIXVSCUFS-UHFFFAOYSA-N 2,4-dinitro-1-naphthol Chemical compound C1=CC=C2C(O)=C([N+]([O-])=O)C=C([N+]([O-])=O)C2=C1 FFRBMBIXVSCUFS-UHFFFAOYSA-N 0.000 description 1
• HUMNYLRZRPPJDN-UHFFFAOYSA-N benzenecarboxaldehyde Natural products O=CC1=CC=CC=C1 HUMNYLRZRPPJDN-UHFFFAOYSA-N 0.000 description 1
• 238000009835 boiling Methods 0.000 description 1
• 239000003518 caustics Substances 0.000 description 1
• 238000001311 chemical methods and process Methods 0.000 description 1
• 238000003776 cleavage reaction Methods 0.000 description 1
• 238000001816 cooling Methods 0.000 description 1
• 239000013067 intermediate product Substances 0.000 description 1
• 239000000155 melt Substances 0.000 description 1
• 238000002844 melting Methods 0.000 description 1
• 230000008018 melting Effects 0.000 description 1
• 239000012452 mother liquor Substances 0.000 description 1
• 230000003647 oxidation Effects 0.000 description 1
• 238000007254 oxidation reaction Methods 0.000 description 1
• QNGNSVIICDLXHT-UHFFFAOYSA-N para-ethylbenzaldehyde Natural products CCC1=CC=C(C=O)C=C1 QNGNSVIICDLXHT-UHFFFAOYSA-N 0.000 description 1
• 230000007017 scission Effects 0.000 description 1
• 238000005245 sintering Methods 0.000 description 1
• 239000002904 solvent Substances 0.000 description 1
• AAAQKTZKLRYKHR-UHFFFAOYSA-N triphenylmethane Chemical compound C1=CC=CC=C1C(C=1C=CC=CC=1)C1=CC=CC=C1 AAAQKTZKLRYKHR-UHFFFAOYSA-N 0.000 description 1
• XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1