DE10351088A1 - Verfahren zum Herstellen von fluormethyl-substituierten Heterocyclen - Google Patents

Verfahren zum Herstellen von fluormethyl-substituierten Heterocyclen Download PDF

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Publication number
DE10351088A1
DE10351088A1 DE10351088A DE10351088A DE10351088A1 DE 10351088 A1 DE10351088 A1 DE 10351088A1 DE 10351088 A DE10351088 A DE 10351088A DE 10351088 A DE10351088 A DE 10351088A DE 10351088 A1 DE10351088 A1 DE 10351088A1
Authority
DE
Germany
Prior art keywords
alkyl
chlorine
fluorine
alkoxy
carbonyl
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Withdrawn
Application number
DE10351088A
Other languages
German (de)
English (en)
Inventor
Reinhard Dr. Lantzsch
Sergiy Dipl.-Chem. Dr. Pazenok
Frank Memmel
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Bayer CropScience AG
Original Assignee
Bayer CropScience AG
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Bayer CropScience AG filed Critical Bayer CropScience AG
Priority to DE10351088A priority Critical patent/DE10351088A1/de
Priority to US10/576,742 priority patent/US7501527B2/en
Priority to CN2004800322480A priority patent/CN1875006B/zh
Priority to DK04765988.3T priority patent/DK1682515T3/en
Priority to EP04765988.3A priority patent/EP1682515B1/de
Priority to KR1020067008293A priority patent/KR101123745B1/ko
Priority to PCT/EP2004/011809 priority patent/WO2005044804A1/de
Priority to JP2006537130A priority patent/JP4936895B2/ja
Priority to ES04765988.3T priority patent/ES2524597T3/es
Priority to BRPI0416112-2A priority patent/BRPI0416112A/pt
Priority to TW093132853A priority patent/TWI359141B/zh
Publication of DE10351088A1 publication Critical patent/DE10351088A1/de
Priority to IL175148A priority patent/IL175148A/en
Priority to MXPA06004605 priority patent/MXPA06004605A/es
Priority to IN1990DE2006 priority patent/IN2006DE01990A/en
Withdrawn legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D263/00—Heterocyclic compounds containing 1,3-oxazole or hydrogenated 1,3-oxazole rings
    • C07D263/02—Heterocyclic compounds containing 1,3-oxazole or hydrogenated 1,3-oxazole rings not condensed with other rings
    • C07D263/30—Heterocyclic compounds containing 1,3-oxazole or hydrogenated 1,3-oxazole rings not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members
    • C07D263/34—Heterocyclic compounds containing 1,3-oxazole or hydrogenated 1,3-oxazole rings not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members with hetero atoms or with carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals, directly attached to ring carbon atoms
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D231/00—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings
    • C07D231/02—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings
    • C07D231/10—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members
    • C07D231/14—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members with hetero atoms or with carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals, directly attached to ring carbon atoms
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D277/00—Heterocyclic compounds containing 1,3-thiazole or hydrogenated 1,3-thiazole rings
    • C07D277/02—Heterocyclic compounds containing 1,3-thiazole or hydrogenated 1,3-thiazole rings not condensed with other rings
    • C07D277/20—Heterocyclic compounds containing 1,3-thiazole or hydrogenated 1,3-thiazole rings not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members
    • C07D277/22—Heterocyclic compounds containing 1,3-thiazole or hydrogenated 1,3-thiazole rings not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members with only hydrogen atoms, hydrocarbon or substituted hydrocarbon radicals, directly attached to ring carbon atoms
    • C07D277/30—Radicals substituted by carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Plural Heterocyclic Compounds (AREA)
  • Heterocyclic Carbon Compounds Containing A Hetero Ring Having Nitrogen And Oxygen As The Only Ring Hetero Atoms (AREA)
  • Nitrogen And Oxygen Or Sulfur-Condensed Heterocyclic Ring Systems (AREA)
  • Agricultural Chemicals And Associated Chemicals (AREA)
DE10351088A 2003-10-31 2003-10-31 Verfahren zum Herstellen von fluormethyl-substituierten Heterocyclen Withdrawn DE10351088A1 (de)

Priority Applications (14)

Application Number Priority Date Filing Date Title
DE10351088A DE10351088A1 (de) 2003-10-31 2003-10-31 Verfahren zum Herstellen von fluormethyl-substituierten Heterocyclen
JP2006537130A JP4936895B2 (ja) 2003-10-31 2004-10-19 フルオロメチル−置換された複素環
ES04765988.3T ES2524597T3 (es) 2003-10-31 2004-10-19 Procedimiento para la preparación de heterociclos sustituidos con fluorometilo
DK04765988.3T DK1682515T3 (en) 2003-10-31 2004-10-19 PROCEDURE FOR PREPARING FLUORMETHYL-SUBSTITUTED HETEROCYCLES
EP04765988.3A EP1682515B1 (de) 2003-10-31 2004-10-19 Verfahren zum herstellen von fluormethyl-substituierten heterocyclen
KR1020067008293A KR101123745B1 (ko) 2003-10-31 2004-10-19 플루오로메틸-치환된 헤테로사이클의 제조방법
PCT/EP2004/011809 WO2005044804A1 (de) 2003-10-31 2004-10-19 Verfahren zum herstellen von fluormethyl-substituierten heterocyclen
US10/576,742 US7501527B2 (en) 2003-10-31 2004-10-19 Method for the production of fluoromethyl-substituted heterocycles
CN2004800322480A CN1875006B (zh) 2003-10-31 2004-10-19 氟甲基取代的杂环的制备方法
BRPI0416112-2A BRPI0416112A (pt) 2003-10-31 2004-10-19 preparação de heterociclos substituìdo por fluormetila
TW093132853A TWI359141B (en) 2003-10-31 2004-10-29 Preparation of fluoromethyl-substituted heterocycl
IL175148A IL175148A (en) 2003-10-31 2006-04-25 Process for the preparation of alkyl esters of lumethyl pyrazoles
MXPA06004605 MXPA06004605A (es) 2003-10-31 2006-04-25 Procedimiento para la obtencion de heterociclos substituidos por fluormet
IN1990DE2006 IN2006DE01990A (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html) 2003-10-31 2006-09-06

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
DE10351088A DE10351088A1 (de) 2003-10-31 2003-10-31 Verfahren zum Herstellen von fluormethyl-substituierten Heterocyclen

Publications (1)

Publication Number Publication Date
DE10351088A1 true DE10351088A1 (de) 2005-06-02

Family

ID=34530016

Family Applications (1)

Application Number Title Priority Date Filing Date
DE10351088A Withdrawn DE10351088A1 (de) 2003-10-31 2003-10-31 Verfahren zum Herstellen von fluormethyl-substituierten Heterocyclen

Country Status (14)

Country Link
US (1) US7501527B2 (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html)
EP (1) EP1682515B1 (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html)
JP (1) JP4936895B2 (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html)
KR (1) KR101123745B1 (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html)
CN (1) CN1875006B (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html)
BR (1) BRPI0416112A (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html)
DE (1) DE10351088A1 (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html)
DK (1) DK1682515T3 (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html)
ES (1) ES2524597T3 (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html)
IL (1) IL175148A (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html)
IN (1) IN2006DE01990A (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html)
MX (1) MXPA06004605A (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html)
TW (1) TWI359141B (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html)
WO (1) WO2005044804A1 (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html)

Families Citing this family (19)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
ATE455105T1 (de) * 2006-11-03 2010-01-15 Basf Se Verfahren zur herstellung von difluormethylpyrazolylcarboxylaten
KR20090107506A (ko) * 2006-12-21 2009-10-13 바스프 에스이 플루오로메틸-치환된 헤테로시클릭 화합물의 제조 방법
EP2164831B1 (de) 2007-06-01 2013-07-17 Basf Se Verfahren zur herstellung n-substituierter (3-dihalomethyl-1-methyl-pyrazol-4-yl)carboxamide
ATE520667T1 (de) * 2007-06-15 2011-09-15 Basf Se Verfahren zur herstellung difluormethylsubstituierter pyrazolverbindungen
EP2181087B1 (en) 2007-08-16 2015-10-14 Solvay Sa Process for the preparation of esters of 4-fluorosubstituted 3-oxo-alcanoic acids
UA102386C2 (ru) 2008-02-29 2013-07-10 Басф Се Способ получения алкил-2-алкоксимэтилен-4,4-дифтор-3-оксобутиратов
CN102015653B (zh) 2008-05-02 2013-09-11 巴斯夫欧洲公司 制备卤素取代的2-(氨基亚甲基)-3-氧代丁酸酯的方法
US8314233B2 (en) 2008-05-02 2012-11-20 Basf Se Process for preparing 2-(aminomethylidene)-4,4-difluoro-3-oxobutyric esters
EA019312B1 (ru) 2008-05-05 2014-02-28 Басф Се Способ получения 1,3,4-замещённых пиразольных соединений
MX317270B (es) * 2008-05-08 2014-01-20 Basf Se Procedimiento para la obtencion de arilcarboxamidas.
EP2307384B1 (en) 2008-07-21 2012-04-25 Basf Se Process for preparing 1,3-disubstituted pyrazolecarboxylic esters
US8981116B2 (en) 2010-07-23 2015-03-17 Solvay Sa Process for the preparation of esters of 1-substituted-3-fluoroalkyl-pyrazole-4-carboxylic acids
FR2975992B1 (fr) * 2011-06-01 2013-11-08 Rhodia Operations Procede de preparation d'un compose fluoromethylpyrazole sous forme acide carboxylique ou derivee
FR2975990B1 (fr) 2011-06-01 2013-05-24 Rhodia Operations Procede de preparation d'un compose organique fluore
US20140128617A1 (en) * 2011-06-21 2014-05-08 Wahed Ahmed Moradi Method for producing pyrazolylcarboxanilides
CN105008330A (zh) * 2013-02-15 2015-10-28 先正达参股股份有限公司 用于制备双-二卤代烷基吡唑的方法
DK3046908T3 (en) * 2013-09-20 2017-10-02 Bayer Cropscience Ag METHOD FOR PREPARING 5-FLOUR-1-ALKYL-3-FLOURALKYL-1H-PYRAZOL-4-CARBALDEHYDE.
CN106045910B (zh) 2016-08-15 2017-10-10 浙江永太科技股份有限公司 一种3‑(二氟甲基)‑1‑甲基‑1h‑吡唑‑4‑羧酸的合成方法
CN115572210B (zh) * 2022-12-08 2023-03-21 暨南大学 一种(1,2,2,2-四氟乙基)芳烃衍生物及其制备方法和应用

Family Cites Families (11)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS6357568A (ja) * 1982-04-16 1988-03-12 ザ　ダウ　ケミカル　カンパニ− 液相ハロゲン交換反応における触媒再使用
DE3400168A1 (de) * 1984-01-04 1985-07-11 Bayer Ag, 5090 Leverkusen 5-halogenalkyl-1,3,4-thiadiazol-2-yloxyacetamide
DE3934924C2 (de) * 1989-10-20 1994-01-27 Huels Chemische Werke Ag Verfahren zur Herstellung von 4-Alkoxycarbonyl-3-chlormethyl-2H-pyrazolen
US5126275A (en) * 1990-09-19 1992-06-30 Miles Inc. Analytical method using tetrazolium salt indicators having a reflectance plateau
US5093347A (en) * 1991-01-28 1992-03-03 Monsanto Company 3-difluoromethylpyrazolecarboxamide fungicides, compositions and use
US5223526A (en) * 1991-12-06 1993-06-29 Monsanto Company Pyrazole carboxanilide fungicides and use
DE4231517A1 (de) * 1992-09-21 1994-03-24 Basf Ag Carbonsäureanilide, Verfahren zu ihrer Herstellung und sie enthaltende Mittel zur Bekämpfung von Schadpilzen
DE19544800A1 (de) * 1995-12-01 1997-06-05 Bayer Ag Verfahren zur Herstellung von 1,3-Dimethyl-5-fluor-pyrazol-4-carboxaniliden
DE19629828A1 (de) * 1996-07-24 1998-01-29 Bayer Ag Carbanilide
JP3533134B2 (ja) * 1999-02-15 2004-05-31 三井化学株式会社 フッ素化剤及びその製法と使用
DE10215292A1 (de) * 2002-02-19 2003-08-28 Bayer Cropscience Ag Disubstitutierte Pyrazolylcarbocanilide

Also Published As

Publication number Publication date
CN1875006A (zh) 2006-12-06
MXPA06004605A (es) 2006-07-20
ES2524597T3 (es) 2014-12-10
EP1682515B1 (de) 2014-10-01
IL175148A0 (en) 2006-09-05
DK1682515T3 (en) 2014-11-17
KR20060094534A (ko) 2006-08-29
TWI359141B (en) 2012-03-01
US20060276656A1 (en) 2006-12-07
JP4936895B2 (ja) 2012-05-23
TW200530189A (en) 2005-09-16
WO2005044804A1 (de) 2005-05-19
IL175148A (en) 2015-03-31
JP2007509871A (ja) 2007-04-19
BRPI0416112A (pt) 2007-01-02
EP1682515A1 (de) 2006-07-26
IN2006DE01990A (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html) 2007-07-13
CN1875006B (zh) 2011-12-21
US7501527B2 (en) 2009-03-10
KR101123745B1 (ko) 2012-03-15

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Legal Events

Date Code Title Description
8127 New person/name/address of the applicant

Owner name: BAYER CROPSCIENCE AG, 40789 MONHEIM, DE

8141 Disposal/no request for examination