DE102009041120A1 - Verfahren zur Reinigung von stark mit Verseifungsprodukten belastetem Fettsäurealkylester - Google Patents

Verfahren zur Reinigung von stark mit Verseifungsprodukten belastetem Fettsäurealkylester Download PDF

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Publication number
DE102009041120A1
DE102009041120A1 DE102009041120A DE102009041120A DE102009041120A1 DE 102009041120 A1 DE102009041120 A1 DE 102009041120A1 DE 102009041120 A DE102009041120 A DE 102009041120A DE 102009041120 A DE102009041120 A DE 102009041120A DE 102009041120 A1 DE102009041120 A1 DE 102009041120A1
Authority
DE
Germany
Prior art keywords
fatty acid
phase
acid alkyl
glycerol
alkyl ester
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Ceased
Application number
DE102009041120A
Other languages
German (de)
English (en)
Inventor
Rudolf Dr. Bönsch
Eckhard Dr. Seidel
Helmut Saft
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Air Liquide Global E&C Solutions Germany GmbH
Original Assignee
Lurgi GmbH
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Lurgi GmbH filed Critical Lurgi GmbH
Priority to DE102009041120A priority Critical patent/DE102009041120A1/de
Priority to IN960DEN2012 priority patent/IN2012DN00960A/en
Priority to CN201080040847.2A priority patent/CN102549131B/zh
Priority to PCT/DE2010/000702 priority patent/WO2011032528A1/de
Priority to PL10739841T priority patent/PL2478081T3/pl
Priority to US13/394,878 priority patent/US8604228B2/en
Priority to EP10739841.4A priority patent/EP2478081B1/de
Publication of DE102009041120A1 publication Critical patent/DE102009041120A1/de
Ceased legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11C—FATTY ACIDS FROM FATS, OILS OR WAXES; CANDLES; FATS, OILS OR FATTY ACIDS BY CHEMICAL MODIFICATION OF FATS, OILS, OR FATTY ACIDS OBTAINED THEREFROM
    • C11C3/00—Fats, oils, or fatty acids by chemical modification of fats, oils, or fatty acids obtained therefrom
    • C11C3/003—Fats, oils, or fatty acids by chemical modification of fats, oils, or fatty acids obtained therefrom by esterification of fatty acids with alcohols
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10L—FUELS NOT OTHERWISE PROVIDED FOR; NATURAL GAS; SYNTHETIC NATURAL GAS OBTAINED BY PROCESSES NOT COVERED BY SUBCLASSES C10G OR C10K; LIQUIFIED PETROLEUM GAS; USE OF ADDITIVES TO FUELS OR FIRES; FIRE-LIGHTERS
    • C10L1/00—Liquid carbonaceous fuels
    • C10L1/02—Liquid carbonaceous fuels essentially based on components consisting of carbon, hydrogen, and oxygen only
    • C10L1/026—Liquid carbonaceous fuels essentially based on components consisting of carbon, hydrogen, and oxygen only for compression ignition
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11C—FATTY ACIDS FROM FATS, OILS OR WAXES; CANDLES; FATS, OILS OR FATTY ACIDS BY CHEMICAL MODIFICATION OF FATS, OILS, OR FATTY ACIDS OBTAINED THEREFROM
    • C11C1/00—Preparation of fatty acids from fats, fatty oils, or waxes; Refining the fatty acids
    • C11C1/08—Refining
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G2300/00—Aspects relating to hydrocarbon processing covered by groups C10G1/00 - C10G99/00
    • C10G2300/10—Feedstock materials
    • C10G2300/1011—Biomass
    • C10G2300/1014—Biomass of vegetal origin
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G2300/00—Aspects relating to hydrocarbon processing covered by groups C10G1/00 - C10G99/00
    • C10G2300/10—Feedstock materials
    • C10G2300/1011—Biomass
    • C10G2300/1018—Biomass of animal origin
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G2300/00—Aspects relating to hydrocarbon processing covered by groups C10G1/00 - C10G99/00
    • C10G2300/20—Characteristics of the feedstock or the products
    • C10G2300/201—Impurities
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02E—REDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
    • Y02E50/00—Technologies for the production of fuel of non-fossil origin
    • Y02E50/10—Biofuels, e.g. bio-diesel
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P30/00—Technologies relating to oil refining and petrochemical industry
    • Y02P30/20—Technologies relating to oil refining and petrochemical industry using bio-feedstock

Landscapes

  • Chemical & Material Sciences (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • General Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Chemistry (AREA)
  • Wood Science & Technology (AREA)
  • Microbiology (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Fats And Perfumes (AREA)
DE102009041120A 2009-09-15 2009-09-15 Verfahren zur Reinigung von stark mit Verseifungsprodukten belastetem Fettsäurealkylester Ceased DE102009041120A1 (de)

Priority Applications (7)

Application Number Priority Date Filing Date Title
DE102009041120A DE102009041120A1 (de) 2009-09-15 2009-09-15 Verfahren zur Reinigung von stark mit Verseifungsprodukten belastetem Fettsäurealkylester
IN960DEN2012 IN2012DN00960A (https=) 2009-09-15 2010-06-22
CN201080040847.2A CN102549131B (zh) 2009-09-15 2010-06-22 带有大量皂化产物的脂肪酸烷基酯的纯化方法
PCT/DE2010/000702 WO2011032528A1 (de) 2009-09-15 2010-06-22 Verfahren zur reinigung von stark mit verseifungsprodukten belastetem fettsäurealkylester
PL10739841T PL2478081T3 (pl) 2009-09-15 2010-06-22 Sposób oczyszczania estrów alkilowych kwasów tłuszczowych silnie obciążonych produktami zmydlania
US13/394,878 US8604228B2 (en) 2009-09-15 2010-06-22 Method for purifying fatty acid alkyl ester greatly loaded with saponification products
EP10739841.4A EP2478081B1 (de) 2009-09-15 2010-06-22 Verfahren zur reinigung von stark mit verseifungsprodukten belastetem fettsäurealkylester

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
DE102009041120A DE102009041120A1 (de) 2009-09-15 2009-09-15 Verfahren zur Reinigung von stark mit Verseifungsprodukten belastetem Fettsäurealkylester

Publications (1)

Publication Number Publication Date
DE102009041120A1 true DE102009041120A1 (de) 2011-03-24

Family

ID=42989376

Family Applications (1)

Application Number Title Priority Date Filing Date
DE102009041120A Ceased DE102009041120A1 (de) 2009-09-15 2009-09-15 Verfahren zur Reinigung von stark mit Verseifungsprodukten belastetem Fettsäurealkylester

Country Status (7)

Country Link
US (1) US8604228B2 (https=)
EP (1) EP2478081B1 (https=)
CN (1) CN102549131B (https=)
DE (1) DE102009041120A1 (https=)
IN (1) IN2012DN00960A (https=)
PL (1) PL2478081T3 (https=)
WO (1) WO2011032528A1 (https=)

Families Citing this family (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104230045B (zh) * 2014-08-21 2015-11-18 波鹰(厦门)科技有限公司 一种高盐含甘油废水中氯化钠及甘油的分离方法

Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE4301686C1 (de) 1993-01-22 1994-03-31 Chem & Pharm Patent Hold Ltd Verfahren zur Herstellung von Fettsäureestern niederer Alkohole
AT397966B (de) * 1993-01-25 1994-08-25 Wimmer Theodor Verfahren zur herstellung von fettsäureestern niederer einwertiger alkohole
WO2006043281A1 (en) * 2004-10-20 2006-04-27 Council Of Scientific And Industrial Research Improved process for the preparation of fatty acid methyl ester (biodiesel) from triglyceride oil through transesterification
DE102006044467A1 (de) 2006-09-21 2008-04-10 Lurgi Ag Verfahren zur kontinuierlichen Herstellung von Fettsäure-Methylester oder Fettsäure-Ethylester
DE102007056703A1 (de) * 2007-11-24 2009-06-04 Lurgi Gmbh Verfahren zum Herstellen von Fettsäureester bzw. Fettsäureethylester

Family Cites Families (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1810761A (zh) * 2005-01-28 2006-08-02 上海日器环保设备工程有限公司 脂肪酸烷基酯的制造方法
BRPI0503631B1 (pt) * 2005-08-19 2015-07-21 Petróleo Brasileiro S.A. - Petrobras Processo para a produção de biodiesel
RU2441864C2 (ru) * 2006-01-12 2012-02-10 Агератек Аб Способ очистки алкильных эфиров жирных кислот и применение агентов для облегчения такой очистки
US20080040970A1 (en) 2006-03-30 2008-02-21 Thomas Anthony Davanzo Systems for producing biodiesel and processes for using the same

Patent Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE4301686C1 (de) 1993-01-22 1994-03-31 Chem & Pharm Patent Hold Ltd Verfahren zur Herstellung von Fettsäureestern niederer Alkohole
AT397966B (de) * 1993-01-25 1994-08-25 Wimmer Theodor Verfahren zur herstellung von fettsäureestern niederer einwertiger alkohole
WO2006043281A1 (en) * 2004-10-20 2006-04-27 Council Of Scientific And Industrial Research Improved process for the preparation of fatty acid methyl ester (biodiesel) from triglyceride oil through transesterification
DE102006044467A1 (de) 2006-09-21 2008-04-10 Lurgi Ag Verfahren zur kontinuierlichen Herstellung von Fettsäure-Methylester oder Fettsäure-Ethylester
DE102006044467B4 (de) 2006-09-21 2008-07-17 Lurgi Gmbh Verfahren zur kontinuierlichen Herstellung von Fettsäure-Methylester oder Fettsäure-Ethylester
DE102007056703A1 (de) * 2007-11-24 2009-06-04 Lurgi Gmbh Verfahren zum Herstellen von Fettsäureester bzw. Fettsäureethylester

Non-Patent Citations (2)

* Cited by examiner, † Cited by third party
Title
CA 2626129 A 1 (Fam WO2006/043281A1)
Norm EN 14214

Also Published As

Publication number Publication date
EP2478081A1 (de) 2012-07-25
WO2011032528A1 (de) 2011-03-24
EP2478081B1 (de) 2019-08-14
PL2478081T3 (pl) 2020-04-30
US20120203017A1 (en) 2012-08-09
CN102549131A (zh) 2012-07-04
US8604228B2 (en) 2013-12-10
CN102549131B (zh) 2016-04-20
IN2012DN00960A (https=) 2015-04-10

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Legal Events

Date Code Title Description
OP8 Request for examination as to paragraph 44 patent law
R081 Change of applicant/patentee

Owner name: AIR LIQUIDE GLOBAL E&C SOLUTIONS GERMANY GMBH, DE

Free format text: FORMER OWNER: LURGI GMBH, 60439 FRANKFURT, DE

Effective date: 20140505

R002 Refusal decision in examination/registration proceedings
R003 Refusal decision now final