DD266561A5 - Verfahren zur gewinnung von magnesiumsulfaten - Google Patents
Verfahren zur gewinnung von magnesiumsulfaten Download PDFInfo
- Publication number
- DD266561A5 DD266561A5 DD87308575A DD30857587A DD266561A5 DD 266561 A5 DD266561 A5 DD 266561A5 DD 87308575 A DD87308575 A DD 87308575A DD 30857587 A DD30857587 A DD 30857587A DD 266561 A5 DD266561 A5 DD 266561A5
- Authority
- DD
- German Democratic Republic
- Prior art keywords
- nacl
- magnesium
- subjected
- magnesium sulfate
- kcl
- Prior art date
Links
- CSNNHWWHGAXBCP-UHFFFAOYSA-L Magnesium sulfate Chemical compound [Mg+2].[O-][S+2]([O-])([O-])[O-] CSNNHWWHGAXBCP-UHFFFAOYSA-L 0.000 title claims abstract description 62
- 238000000034 method Methods 0.000 title claims abstract description 31
- 235000019341 magnesium sulphate Nutrition 0.000 title claims abstract description 26
- 229910052943 magnesium sulfate Inorganic materials 0.000 title claims abstract description 24
- FAPWRFPIFSIZLT-UHFFFAOYSA-M Sodium chloride Chemical compound [Na+].[Cl-] FAPWRFPIFSIZLT-UHFFFAOYSA-M 0.000 claims abstract description 41
- 235000002639 sodium chloride Nutrition 0.000 claims abstract description 39
- 239000011780 sodium chloride Substances 0.000 claims abstract description 25
- 238000000926 separation method Methods 0.000 claims abstract description 16
- 150000003839 salts Chemical class 0.000 claims abstract description 15
- 239000012141 concentrate Substances 0.000 claims abstract description 13
- 229910052928 kieserite Inorganic materials 0.000 claims abstract description 13
- 239000000463 material Substances 0.000 claims abstract description 11
- 239000001103 potassium chloride Substances 0.000 claims abstract description 9
- 229910052925 anhydrite Inorganic materials 0.000 claims abstract description 8
- OSGAYBCDTDRGGQ-UHFFFAOYSA-L calcium sulfate Chemical compound [Ca+2].[O-]S([O-])(=O)=O OSGAYBCDTDRGGQ-UHFFFAOYSA-L 0.000 claims abstract description 8
- 229910052500 inorganic mineral Inorganic materials 0.000 claims abstract description 6
- 235000010755 mineral Nutrition 0.000 claims abstract description 6
- 239000011707 mineral Substances 0.000 claims abstract description 6
- 239000011833 salt mixture Substances 0.000 claims abstract description 6
- 239000002699 waste material Substances 0.000 claims abstract description 5
- LFCFXZHKDRJMNS-UHFFFAOYSA-L magnesium;sulfate;hydrate Chemical compound O.[Mg+2].[O-]S([O-])(=O)=O LFCFXZHKDRJMNS-UHFFFAOYSA-L 0.000 claims abstract description 4
- 238000009291 froth flotation Methods 0.000 claims abstract 3
- 238000002425 crystallisation Methods 0.000 claims abstract 2
- 229960003390 magnesium sulfate Drugs 0.000 claims description 12
- WCUXLLCKKVVCTQ-UHFFFAOYSA-M potassium chloride Inorganic materials [Cl-].[K+] WCUXLLCKKVVCTQ-UHFFFAOYSA-M 0.000 claims description 12
- 238000005188 flotation Methods 0.000 claims description 11
- 239000000047 product Substances 0.000 claims description 8
- 239000003795 chemical substances by application Substances 0.000 claims description 4
- 230000003750 conditioning effect Effects 0.000 claims description 4
- 239000006260 foam Substances 0.000 claims description 4
- BMQVDVJKPMGHDO-UHFFFAOYSA-K magnesium;potassium;chloride;sulfate;trihydrate Chemical compound O.O.O.[Mg+2].[Cl-].[K+].[O-]S([O-])(=O)=O BMQVDVJKPMGHDO-UHFFFAOYSA-K 0.000 claims description 4
- 238000004090 dissolution Methods 0.000 claims description 3
- 229910052936 alkali metal sulfate Inorganic materials 0.000 claims description 2
- 239000000470 constituent Substances 0.000 claims description 2
- WZISDKTXHMETKG-UHFFFAOYSA-H dimagnesium;dipotassium;trisulfate Chemical compound [Mg+2].[Mg+2].[K+].[K+].[O-]S([O-])(=O)=O.[O-]S([O-])(=O)=O.[O-]S([O-])(=O)=O WZISDKTXHMETKG-UHFFFAOYSA-H 0.000 claims description 2
- 229940076230 magnesium sulfate monohydrate Drugs 0.000 claims description 2
- 239000007858 starting material Substances 0.000 claims 3
- 239000003153 chemical reaction reagent Substances 0.000 claims 2
- WRUGWIBCXHJTDG-UHFFFAOYSA-L magnesium sulfate heptahydrate Chemical compound O.O.O.O.O.O.O.[Mg+2].[O-]S([O-])(=O)=O WRUGWIBCXHJTDG-UHFFFAOYSA-L 0.000 claims 2
- 229910001514 alkali metal chloride Inorganic materials 0.000 claims 1
- 150000008051 alkyl sulfates Chemical class 0.000 claims 1
- 229940045714 alkyl sulfonate alkylating agent Drugs 0.000 claims 1
- 150000008052 alkyl sulfonates Chemical class 0.000 claims 1
- 239000000428 dust Substances 0.000 claims 1
- 238000002360 preparation method Methods 0.000 claims 1
- 239000002994 raw material Substances 0.000 claims 1
- 238000005406 washing Methods 0.000 claims 1
- 238000011084 recovery Methods 0.000 abstract description 6
- 239000002351 wastewater Substances 0.000 abstract description 3
- 229920006395 saturated elastomer Polymers 0.000 abstract description 2
- FYYHWMGAXLPEAU-UHFFFAOYSA-N Magnesium Chemical compound [Mg] FYYHWMGAXLPEAU-UHFFFAOYSA-N 0.000 abstract 1
- 238000001816 cooling Methods 0.000 abstract 1
- 230000008025 crystallization Effects 0.000 abstract 1
- 239000011777 magnesium Substances 0.000 abstract 1
- 229910052749 magnesium Inorganic materials 0.000 abstract 1
- 239000000243 solution Substances 0.000 description 7
- 235000011164 potassium chloride Nutrition 0.000 description 5
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 5
- VEXZGXHMUGYJMC-UHFFFAOYSA-M Chloride anion Chemical compound [Cl-] VEXZGXHMUGYJMC-UHFFFAOYSA-M 0.000 description 4
- KWYUFKZDYYNOTN-UHFFFAOYSA-M Potassium hydroxide Chemical compound [OH-].[K+] KWYUFKZDYYNOTN-UHFFFAOYSA-M 0.000 description 4
- 235000014113 dietary fatty acids Nutrition 0.000 description 4
- 239000000194 fatty acid Substances 0.000 description 4
- 229930195729 fatty acid Natural products 0.000 description 4
- 150000004665 fatty acids Chemical class 0.000 description 4
- 229940072033 potash Drugs 0.000 description 4
- BWHMMNNQKKPAPP-UHFFFAOYSA-L potassium carbonate Substances [K+].[K+].[O-]C([O-])=O BWHMMNNQKKPAPP-UHFFFAOYSA-L 0.000 description 4
- 235000015320 potassium carbonate Nutrition 0.000 description 4
- YGSDEFSMJLZEOE-UHFFFAOYSA-N salicylic acid Chemical compound OC(=O)C1=CC=CC=C1O YGSDEFSMJLZEOE-UHFFFAOYSA-N 0.000 description 4
- 239000000203 mixture Substances 0.000 description 3
- 239000000126 substance Substances 0.000 description 3
- -1 alkyl sulphate Chemical compound 0.000 description 2
- JVTAAEKCZFNVCJ-UHFFFAOYSA-N lactic acid Chemical compound CC(O)C(O)=O JVTAAEKCZFNVCJ-UHFFFAOYSA-N 0.000 description 2
- PALNZFJYSCMLBK-UHFFFAOYSA-K magnesium;potassium;trichloride;hexahydrate Chemical compound O.O.O.O.O.O.[Mg+2].[Cl-].[Cl-].[Cl-].[K+] PALNZFJYSCMLBK-UHFFFAOYSA-K 0.000 description 2
- 239000012452 mother liquor Substances 0.000 description 2
- FJKROLUGYXJWQN-UHFFFAOYSA-N papa-hydroxy-benzoic acid Natural products OC(=O)C1=CC=C(O)C=C1 FJKROLUGYXJWQN-UHFFFAOYSA-N 0.000 description 2
- 229960004889 salicylic acid Drugs 0.000 description 2
- 239000012047 saturated solution Substances 0.000 description 2
- 239000002904 solvent Substances 0.000 description 2
- USFZMSVCRYTOJT-UHFFFAOYSA-N Ammonium acetate Chemical compound N.CC(O)=O USFZMSVCRYTOJT-UHFFFAOYSA-N 0.000 description 1
- 239000005695 Ammonium acetate Substances 0.000 description 1
- ZLMJMSJWJFRBEC-UHFFFAOYSA-N Potassium Chemical compound [K] ZLMJMSJWJFRBEC-UHFFFAOYSA-N 0.000 description 1
- 241000219793 Trifolium Species 0.000 description 1
- 235000019257 ammonium acetate Nutrition 0.000 description 1
- 229940043376 ammonium acetate Drugs 0.000 description 1
- 150000008064 anhydrides Chemical class 0.000 description 1
- 239000002585 base Substances 0.000 description 1
- 238000005422 blasting Methods 0.000 description 1
- 238000006243 chemical reaction Methods 0.000 description 1
- 150000001805 chlorine compounds Chemical class 0.000 description 1
- 239000004927 clay Substances 0.000 description 1
- 230000003247 decreasing effect Effects 0.000 description 1
- 238000010494 dissociation reaction Methods 0.000 description 1
- 230000005593 dissociations Effects 0.000 description 1
- 238000000605 extraction Methods 0.000 description 1
- 230000002349 favourable effect Effects 0.000 description 1
- 239000003337 fertilizer Substances 0.000 description 1
- 238000001914 filtration Methods 0.000 description 1
- 239000012467 final product Substances 0.000 description 1
- 239000013505 freshwater Substances 0.000 description 1
- 230000036571 hydration Effects 0.000 description 1
- 238000006703 hydration reaction Methods 0.000 description 1
- JEIPFZHSYJVQDO-UHFFFAOYSA-N iron(III) oxide Inorganic materials O=[Fe]O[Fe]=O JEIPFZHSYJVQDO-UHFFFAOYSA-N 0.000 description 1
- 239000004310 lactic acid Substances 0.000 description 1
- 235000014655 lactic acid Nutrition 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 229920002401 polyacrylamide Polymers 0.000 description 1
- 229910052700 potassium Inorganic materials 0.000 description 1
- 239000011591 potassium Substances 0.000 description 1
- 238000000746 purification Methods 0.000 description 1
- 238000010992 reflux Methods 0.000 description 1
- 235000012239 silicon dioxide Nutrition 0.000 description 1
- 229930186775 staminol Natural products 0.000 description 1
- 229910021653 sulphate ion Inorganic materials 0.000 description 1
- 239000000725 suspension Substances 0.000 description 1
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B03—SEPARATION OF SOLID MATERIALS USING LIQUIDS OR USING PNEUMATIC TABLES OR JIGS; MAGNETIC OR ELECTROSTATIC SEPARATION OF SOLID MATERIALS FROM SOLID MATERIALS OR FLUIDS; SEPARATION BY HIGH-VOLTAGE ELECTRIC FIELDS
- B03C—MAGNETIC OR ELECTROSTATIC SEPARATION OF SOLID MATERIALS FROM SOLID MATERIALS OR FLUIDS; SEPARATION BY HIGH-VOLTAGE ELECTRIC FIELDS
- B03C7/00—Separating solids from solids by electrostatic effect
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B03—SEPARATION OF SOLID MATERIALS USING LIQUIDS OR USING PNEUMATIC TABLES OR JIGS; MAGNETIC OR ELECTROSTATIC SEPARATION OF SOLID MATERIALS FROM SOLID MATERIALS OR FLUIDS; SEPARATION BY HIGH-VOLTAGE ELECTRIC FIELDS
- B03B—SEPARATING SOLID MATERIALS USING LIQUIDS OR USING PNEUMATIC TABLES OR JIGS
- B03B9/00—General arrangement of separating plant, e.g. flow sheets
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B03—SEPARATION OF SOLID MATERIALS USING LIQUIDS OR USING PNEUMATIC TABLES OR JIGS; MAGNETIC OR ELECTROSTATIC SEPARATION OF SOLID MATERIALS FROM SOLID MATERIALS OR FLUIDS; SEPARATION BY HIGH-VOLTAGE ELECTRIC FIELDS
- B03C—MAGNETIC OR ELECTROSTATIC SEPARATION OF SOLID MATERIALS FROM SOLID MATERIALS OR FLUIDS; SEPARATION BY HIGH-VOLTAGE ELECTRIC FIELDS
- B03C7/00—Separating solids from solids by electrostatic effect
- B03C7/003—Pretreatment of the solids prior to electrostatic separation
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B03—SEPARATION OF SOLID MATERIALS USING LIQUIDS OR USING PNEUMATIC TABLES OR JIGS; MAGNETIC OR ELECTROSTATIC SEPARATION OF SOLID MATERIALS FROM SOLID MATERIALS OR FLUIDS; SEPARATION BY HIGH-VOLTAGE ELECTRIC FIELDS
- B03D—FLOTATION; DIFFERENTIAL SEDIMENTATION
- B03D1/00—Flotation
- B03D1/02—Froth-flotation processes
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01D—COMPOUNDS OF ALKALI METALS, i.e. LITHIUM, SODIUM, POTASSIUM, RUBIDIUM, CAESIUM, OR FRANCIUM
- C01D5/00—Sulfates or sulfites of sodium, potassium or alkali metals in general
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01F—COMPOUNDS OF THE METALS BERYLLIUM, MAGNESIUM, ALUMINIUM, CALCIUM, STRONTIUM, BARIUM, RADIUM, THORIUM, OR OF THE RARE-EARTH METALS
- C01F5/00—Compounds of magnesium
- C01F5/40—Magnesium sulfates
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Life Sciences & Earth Sciences (AREA)
- Geology (AREA)
- Compounds Of Alkaline-Earth Elements, Aluminum Or Rare-Earth Metals (AREA)
- Manufacture And Refinement Of Metals (AREA)
- Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
- Transition And Organic Metals Composition Catalysts For Addition Polymerization (AREA)
- Curing Cements, Concrete, And Artificial Stone (AREA)
- Diaphragms For Electromechanical Transducers (AREA)
- Eye Examination Apparatus (AREA)
- Emergency Protection Circuit Devices (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE19863637226 DE3637226A1 (de) | 1986-11-03 | 1986-11-03 | Verfahren zur gewinnung von magnesiumsulfaten |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| DD266561A5 true DD266561A5 (de) | 1989-04-05 |
Family
ID=6312957
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DD87308575A DD266561A5 (de) | 1986-11-03 | 1987-11-02 | Verfahren zur gewinnung von magnesiumsulfaten |
Country Status (8)
| Country | Link |
|---|---|
| EP (1) | EP0266599B1 (enrdf_load_stackoverflow) |
| AT (1) | ATE75701T1 (enrdf_load_stackoverflow) |
| DD (1) | DD266561A5 (enrdf_load_stackoverflow) |
| DE (1) | DE3637226A1 (enrdf_load_stackoverflow) |
| DK (1) | DK562887A (enrdf_load_stackoverflow) |
| FI (1) | FI874851A7 (enrdf_load_stackoverflow) |
| NO (1) | NO874554L (enrdf_load_stackoverflow) |
| PT (1) | PT86046B (enrdf_load_stackoverflow) |
Families Citing this family (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101549210B (zh) * | 2008-04-03 | 2011-04-13 | 上海瑞惠机械设备制造有限公司 | 烟气湿式氧化镁脱硫废液回收方法 |
Family Cites Families (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE1158912B (de) * | 1961-10-16 | 1963-12-12 | Zentrale Forschungsstelle Fuer | Flotationsverfahren zur Gewinnung von Natriumchlorid und Kieserit aus den in Klaerapparaten und am Schlammfilter ausgeschiedenen Rueckstandsschlaemmen |
| DE1201782B (de) * | 1964-06-24 | 1965-09-30 | Stockhausen & Cie Chem Fab | Verfahren zur Flotation von Kieserit |
| DE3146295C1 (de) * | 1981-11-23 | 1983-04-07 | Kali Und Salz Ag, 3500 Kassel | "Verfahren zur elektrostatischen Trennung von gemahlenen Kalirohsalzen" |
| DE3334665C1 (de) * | 1983-09-24 | 1984-10-04 | Kali Und Salz Ag, 3500 Kassel | Verfahren zur elektrostatischen Aufbereitung von Kieserit und Langbeinit enthaltenden Kalirohsalzen |
-
1986
- 1986-11-03 DE DE19863637226 patent/DE3637226A1/de active Granted
-
1987
- 1987-10-16 AT AT87115132T patent/ATE75701T1/de not_active IP Right Cessation
- 1987-10-16 EP EP87115132A patent/EP0266599B1/de not_active Expired - Lifetime
- 1987-10-27 DK DK562887A patent/DK562887A/da not_active Application Discontinuation
- 1987-10-30 PT PT86046A patent/PT86046B/pt not_active IP Right Cessation
- 1987-11-02 NO NO874554A patent/NO874554L/no unknown
- 1987-11-02 DD DD87308575A patent/DD266561A5/de not_active IP Right Cessation
- 1987-11-03 FI FI874851A patent/FI874851A7/fi not_active Application Discontinuation
Also Published As
| Publication number | Publication date |
|---|---|
| DE3637226A1 (de) | 1988-05-19 |
| EP0266599A2 (de) | 1988-05-11 |
| EP0266599B1 (de) | 1992-05-06 |
| FI874851A0 (fi) | 1987-11-03 |
| DK562887D0 (da) | 1987-10-27 |
| PT86046B (pt) | 1990-07-31 |
| DE3637226C2 (enrdf_load_stackoverflow) | 1990-09-20 |
| ATE75701T1 (de) | 1992-05-15 |
| NO874554D0 (no) | 1987-11-02 |
| EP0266599A3 (en) | 1989-10-11 |
| FI874851L (fi) | 1988-05-04 |
| FI874851A7 (fi) | 1988-05-04 |
| NO874554L (no) | 1988-05-04 |
| DK562887A (da) | 1988-05-04 |
| PT86046A (en) | 1987-11-01 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| ENJ | Ceased due to non-payment of renewal fee |