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Krystalická forma Enzalutamidu s kyselinou bromovodíkovou
CZ32371U1
Czechia
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Markéta Slavíková Luděk Ridvan Ondřej Dammer
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Description
translated from
| Forma | ||
| ethanol:voda 3:1 | bílé krystaly | Rl+HBr sůl |
| 4-methyl-2-pentanon | bílé krystaly | HBr sůl |
| aceton | žlutohnědé krystaly | HBr sůl |
| acetonitril | roztok | |
| ethylacetát | bílé krystaly | HBr sůl |
| methanol | bílé krystaly | HBr sůl + R2 |
| toluen | bílé krystaly | HBr sůl +R1 |
| rozpouštědlo | XRPD | krystaly |
| 2-butanon | Sůl | Bílé |
| Aceton | Sůl | Hnědooranžové |
| Ethylacetát | Sůl | Bílé |
| Methanol | R2 | Bílé |
| Poloha [°20] | Mezirovinná vzdálenost [Á] [Á]=0,lnm | Relativní intenzita [%] |
| 4,66 | 18,950 | 17,8 |
| 7,58 | 11,657 | 34,2 |
| 9,34 | 9,464 | 100,0 |
| 11,10 | 7,967 | 45,3 |
| 12,63 | 7,003 | 19,8 |
| 14,04 | 6,303 | 69,0 |
| 14,25 | 6,210 | 10,0 |
| 15,26 | 5,801 | 24,6 |
| 16,35 | 5,418 | 44,9 |
| 18,61 | 4,764 | 11,8 |
| 19,71 | 4,501 | 13,7 |
| 21,20 | 4,187 | 6,9 |
| 22,33 | 3,977 | 17,8 |
| 23,09 | 3,848 | 19,3 |
| 23,69 | 3,752 | 7,4 |
| 23,86 | 3,727 | 5,5 |
| 24,17 | 3,680 | 8,0 |
| 24,50 | 3,630 | 6,2 |
| 25,44 | 3,498 | 4,6 |
| 26,64 | 3,344 | 21,0 |
| 27,46 | 3,245 | 2,4 |
| 28,72 | 3,106 | 11,8 |
| 29,98 | 2,979 | 2,9 |
| 31,34 | 2,852 | 4,0 |
| 33,67 | 2,659 | 4,5 |
| 37,48 | 2,398 | 1,8 |
| 37,94 | 2,369 | 3,1 |
| rozpouštědlo | ml | 48% HBr (ml) | mg/výtěžek | XRPD | Krystaly barva |
| 2-butanon | 2 | 0,26 | 780/66,4% | Sůl | Bílé |
| Aceton | 2 | 0,26 | 1022/87% | Sůl | Hnědooranžové |
| Ethylacetát | 4+2 | 0,26+0,26 | 563/48% | Sůl | Bílé |
| Methanol | 5+3 | 0,26+0,26 | 722/72,2% | R2 | Bílé |
Claims (2)
Hide Dependent
translated from
- NÁROKY NA OCHRANU5 1. Krystalická forma enzalutamidu hydrobromidu charakterizovaná reflexemi v rentgenovém RTG práškovém záznamu s použitím záření CuKa: 9,3; 14,0; 16,3; 23,1 a26,6 ± 0.2° 2-theta.
- 2. Krystalická forma enzalutamidu hydrobromidu podle nároku 1 charakterizovaná dalšími ίο následujícími reflexemi v RTG práškovém záznamu: 7,6; 11,1; 15,3; 19,7; 22,3 a 28,7 ±0.2° 2-theta.