CU22612A3 - Método para recobrar níquel a partir de mineral laterítico conteniendo ni-fe-mg con alto contenido de magnesio - Google Patents
Método para recobrar níquel a partir de mineral laterítico conteniendo ni-fe-mg con alto contenido de magnesioInfo
- Publication number
- CU22612A3 CU22612A3 CU1996062A CU1996062A CU22612A3 CU 22612 A3 CU22612 A3 CU 22612A3 CU 1996062 A CU1996062 A CU 1996062A CU 1996062 A CU1996062 A CU 1996062A CU 22612 A3 CU22612 A3 CU 22612A3
- Authority
- CU
- Cuba
- Prior art keywords
- nickel
- hcl
- washing
- magnesium content
- high magnesium
- Prior art date
Links
- PXHVJJICTQNCMI-UHFFFAOYSA-N Nickel Chemical compound [Ni] PXHVJJICTQNCMI-UHFFFAOYSA-N 0.000 title abstract 14
- 229910052759 nickel Inorganic materials 0.000 title abstract 7
- 229910052500 inorganic mineral Inorganic materials 0.000 title abstract 5
- 239000011707 mineral Substances 0.000 title abstract 5
- FYYHWMGAXLPEAU-UHFFFAOYSA-N Magnesium Chemical compound [Mg] FYYHWMGAXLPEAU-UHFFFAOYSA-N 0.000 title abstract 2
- 239000011777 magnesium Substances 0.000 title abstract 2
- 229910052749 magnesium Inorganic materials 0.000 title abstract 2
- 238000000034 method Methods 0.000 title abstract 2
- 229910001710 laterite Inorganic materials 0.000 title 1
- 239000011504 laterite Substances 0.000 title 1
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 abstract 4
- 235000010755 mineral Nutrition 0.000 abstract 4
- 238000005406 washing Methods 0.000 abstract 3
- GRYLNZFGIOXLOG-UHFFFAOYSA-N Nitric acid Chemical compound O[N+]([O-])=O GRYLNZFGIOXLOG-UHFFFAOYSA-N 0.000 abstract 2
- 239000002253 acid Substances 0.000 abstract 2
- 229910052742 iron Inorganic materials 0.000 abstract 2
- 229910017604 nitric acid Inorganic materials 0.000 abstract 2
- 239000011347 resin Substances 0.000 abstract 2
- 229920005989 resin Polymers 0.000 abstract 2
- 238000000926 separation method Methods 0.000 abstract 2
- TWRXJAOTZQYOKJ-UHFFFAOYSA-L Magnesium chloride Chemical class [Mg+2].[Cl-].[Cl-] TWRXJAOTZQYOKJ-UHFFFAOYSA-L 0.000 abstract 1
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 abstract 1
- 238000010521 absorption reaction Methods 0.000 abstract 1
- 235000011147 magnesium chloride Nutrition 0.000 abstract 1
- 239000007787 solid Substances 0.000 abstract 1
- 235000011149 sulphuric acid Nutrition 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
- C22B26/00—Obtaining alkali, alkaline earth metals or magnesium
- C22B26/20—Obtaining alkaline earth metals or magnesium
- C22B26/22—Obtaining magnesium
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
- C22B23/00—Obtaining nickel or cobalt
- C22B23/04—Obtaining nickel or cobalt by wet processes
- C22B23/0407—Leaching processes
- C22B23/0415—Leaching processes with acids or salt solutions except ammonium salts solutions
- C22B23/0423—Halogenated acids or salts thereof
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
- C22B3/00—Extraction of metal compounds from ores or concentrates by wet processes
- C22B3/20—Treatment or purification of solutions, e.g. obtained by leaching
- C22B3/42—Treatment or purification of solutions, e.g. obtained by leaching by ion-exchange extraction
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P10/00—Technologies related to metal processing
- Y02P10/20—Recycling
Landscapes
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Organic Chemistry (AREA)
- Materials Engineering (AREA)
- Mechanical Engineering (AREA)
- Metallurgy (AREA)
- Manufacturing & Machinery (AREA)
- Life Sciences & Earth Sciences (AREA)
- Environmental & Geological Engineering (AREA)
- General Life Sciences & Earth Sciences (AREA)
- Geology (AREA)
- Geochemistry & Mineralogy (AREA)
- Manufacture And Refinement Of Metals (AREA)
Abstract
La presente invención se relaciona con un método para recobrar níquel a partir de mineral laterítico, con alto contenido de magnesio, el cual además contiene hierro. Los minerales referidos como minerales saprolíticos son sometidos a lavado mediante drenaje con un ácido mineral, a partir de un grupo consistente de ácido clorhídrico (HCl), sulfúrico (H2SO4) ó nítrico (HNO3), siendo en HCl el preferido. Siguiendo el lavado con drenaje, empleando HCl, la solución impregnada obtenida es separada a partir de los sólidos no disueltos y el níquel es preferentemente recobrado mediante el contacto de dicha solución con una resina selectiva para la absorción del níquel. El refinado restante que contiene cloruros de hierro y magnesio puede ser sometido a pirohidrólisis para producir sus respectivos óxidos y HCl libre reciclarlos en el sistema de lavado. El níquel es extraído a partir de la resina usando una solución de separación de dicho ácido y el níquel es posteriormente extraído a partir de la solución de separación cargada de níquel.
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US08/502,923 US5571308A (en) | 1995-07-17 | 1995-07-17 | Method for recovering nickel from high magnesium-containing Ni-Fe-Mg lateritic ore |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CU22612A3 true CU22612A3 (es) | 2000-02-10 |
Family
ID=23999980
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CU1996062A CU22612A3 (es) | 1995-07-17 | 1996-07-09 | Método para recobrar níquel a partir de mineral laterítico conteniendo ni-fe-mg con alto contenido de magnesio |
Country Status (18)
| Country | Link |
|---|---|
| US (1) | US5571308A (es) |
| EP (1) | EP0862659B1 (es) |
| AT (1) | ATE195153T1 (es) |
| AU (1) | AU705253B2 (es) |
| BR (1) | BR9609735A (es) |
| CA (1) | CA2224218C (es) |
| CO (1) | CO4560492A1 (es) |
| CU (1) | CU22612A3 (es) |
| DE (1) | DE69609624T2 (es) |
| DK (1) | DK0862659T3 (es) |
| ES (1) | ES2152025T3 (es) |
| GR (1) | GR3034662T3 (es) |
| GT (1) | GT199600044A (es) |
| OA (1) | OA10651A (es) |
| PT (1) | PT862659E (es) |
| RU (1) | RU2149910C1 (es) |
| WO (1) | WO1997004139A1 (es) |
| YU (1) | YU38796A (es) |
Families Citing this family (55)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US5626648A (en) * | 1995-07-17 | 1997-05-06 | Bhp Minerals International Inc. | Recovery of nickel from bioleach solution |
| US5976218A (en) * | 1996-05-10 | 1999-11-02 | Henkel Corporation | Process for the recovery of nickel |
| AUPO837197A0 (en) | 1997-08-01 | 1997-08-28 | Centaur Mining & Exploration Limited | Selective precipitation of nickel and cobalt |
| JPH11335821A (ja) * | 1998-05-20 | 1999-12-07 | Japan Energy Corp | 磁性薄膜形成用Ｎｉ−Ｆｅ合金スパッタリングターゲット、磁性薄膜および磁性薄膜形成用Ｎｉ−Ｆｅ合金スパッタリングターゲットの製造方法 |
| NO313244B1 (no) * | 1998-07-08 | 2002-09-02 | Crew Dev Corp | Fremgangsmåte for isolering og produksjon av magnesitt eller magnesiumklorid |
| US6350420B1 (en) * | 1999-10-15 | 2002-02-26 | Bhp Minerals International, Inc. | Resin-in-pulp method for recovery of nickel and cobalt |
| US6261527B1 (en) | 1999-11-03 | 2001-07-17 | Bhp Minerals International Inc. | Atmospheric leach process for the recovery of nickel and cobalt from limonite and saprolite ores |
| US6387239B1 (en) * | 1999-11-17 | 2002-05-14 | Bhp Minerals International, Inc. | Recovery of metals from ore |
| US6395061B1 (en) | 2000-03-07 | 2002-05-28 | Bhp Minerals International Inc. | Process for organic acid bioleaching of ore |
| US6312500B1 (en) | 2000-03-30 | 2001-11-06 | Bhp Minerals International Inc. | Heap leaching of nickel containing ore |
| WO2002008477A1 (en) * | 2000-07-21 | 2002-01-31 | Nichromet Extraction Inc. | Method for recovering nickel and cobalt from laterite ores |
| US6379637B1 (en) * | 2000-10-31 | 2002-04-30 | Walter Curlook | Direct atmospheric leaching of highly-serpentinized saprolitic nickel laterite ores with sulphuric acid |
| AUPR207200A0 (en) * | 2000-12-13 | 2001-01-11 | QNI Limited | Hydroxide solids enrichment by slurry contact |
| US7329396B2 (en) * | 2003-05-16 | 2008-02-12 | Jaguar Nickel Inc. | Process for the recovery of value metals from material containing base metal oxides |
| AU2003903632A0 (en) * | 2003-07-14 | 2003-07-31 | Qni Technology Pty Ltd | Process for recovery of nickel and cobalt by heap leaching of low grade nickel or cobalt containing material |
| MXPA06010821A (es) * | 2004-03-25 | 2006-12-19 | Intec Ltd | Recuperacion de metales a partir de materiales metaliferos oxidados. |
| CA2571492A1 (en) * | 2004-06-28 | 2006-01-05 | Skye Resources Inc. | Method for nickel and cobalt recovery from laterite ores by reaction with concentrated acid water leaching |
| KR20070041770A (ko) * | 2004-08-02 | 2007-04-19 | 스카이 리소스 아이앤씨 | 대기 및 중간압 침출의 조합에 의해 라테라이트광석으로부터 니켈 및 코발트를 회수하는 방법 |
| AU2005297143B8 (en) * | 2004-10-21 | 2010-04-01 | Anglo Operations Limited | Leaching process in the presence of hydrochloric acid for the recovery of a value metal from an ore |
| UA88928C2 (uk) * | 2004-10-21 | 2009-12-10 | Англо Оперейшенс Лимитед | Спосіб вилуговування цінних металів з руди в присутності хлористоводневої кислоти |
| JP5374041B2 (ja) * | 2005-03-22 | 2013-12-25 | アングロ オペレーションズ リミティッド | 鉱石（ｏｒａ）からの有価金属回収のための塩酸存在下での浸出方法 |
| JP2009510258A (ja) * | 2005-09-30 | 2009-03-12 | ビーエイチピー ビリトン イノベーション ピーティーワイ エルティーディー | 大気圧でラテライト鉱石を浸出するための方法 |
| AU2007288109B2 (en) | 2006-08-23 | 2011-09-15 | Bhp Billiton Ssm Development Pty Ltd | Production of metallic nickel with low iron content |
| WO2008138039A1 (en) * | 2007-05-14 | 2008-11-20 | Bhp Billiton Ssm Development Pty Ltd | Nickel recovery from a high ferrous content laterite ore |
| US20090056502A1 (en) * | 2007-08-29 | 2009-03-05 | Vale Inco Limited | Hydrometallurgical process for recovery of nickel and cobalt |
| US8961649B2 (en) * | 2007-08-29 | 2015-02-24 | Vale Canada Limited | System and method for extracting base metal values from oxide ores |
| WO2009079715A1 (en) | 2007-12-24 | 2009-07-02 | Bhp Billiton Ssm Development Pty Ltd | Selectively leaching cobalt from lateritic ores |
| US8454723B2 (en) * | 2008-06-16 | 2013-06-04 | Bhp Billiton Ssm Development Pty Ltd. | Saprolite neutralisation of heap leach process |
| US8173086B2 (en) * | 2009-07-14 | 2012-05-08 | Vale S.A. | Process of recovery of base metals from oxide ores |
| AR077697A1 (es) * | 2009-08-03 | 2011-09-14 | Anglo Operations Ltd | Proceso para la lixiviacion de un metal de valor a partir de un mineral que contiene hierro |
| AU2011215764B2 (en) * | 2010-02-10 | 2013-12-05 | Asarco Llc | Ion exchange cobalt recovery |
| US8361191B2 (en) | 2010-04-01 | 2013-01-29 | Search Minerals, Inc. | Low acid leaching of nickel and cobalt from lean iron-containing nickel ores |
| WO2011120127A1 (en) * | 2010-04-01 | 2011-10-06 | Search Minerals Inc. | Low acid leaching of nickel and cobalt from lean iron-containing nickel ores |
| CA2740249C (en) | 2010-05-25 | 2015-08-04 | Dow Global Technologies Llc | A process for separating copper and nickel from cobalt containing solutions |
| AU2012212348B2 (en) * | 2011-02-01 | 2016-08-18 | Vale S.A. | Direct purification of a nickel laterite leaching effluent |
| US20120204680A1 (en) * | 2011-02-11 | 2012-08-16 | Emc Metals Corporation | System and Method for Recovery of Nickel Values From Nickel-Containing Ores |
| CN103534367A (zh) | 2011-03-18 | 2014-01-22 | 奥贝特铝业有限公司 | 从含铝材料中回收稀土元素的方法 |
| US9382600B2 (en) | 2011-09-16 | 2016-07-05 | Orbite Technologies Inc. | Processes for preparing alumina and various other products |
| WO2013086606A1 (en) * | 2011-12-12 | 2013-06-20 | Process Research Ortech Inc. | Separation of iron from value metals in leaching of laterite ores |
| EP2802675B1 (en) | 2012-01-10 | 2020-03-11 | Orbite Aluminae Inc. | Processes for treating red mud |
| WO2013165735A1 (en) | 2012-05-01 | 2013-11-07 | Dow Global Technologies Llc | Nickel and cobalt recovery using continuous ion exchange |
| CA3038320C (en) * | 2012-08-24 | 2021-08-03 | Orbite Technologies Inc. | Process for treating magnesium-bearing ores |
| CA2885255C (en) * | 2012-09-26 | 2015-12-22 | Orbite Aluminae Inc. | Processes for preparing alumina and magnesium chloride by hc1 leaching of various materials |
| WO2014047672A1 (en) * | 2012-09-28 | 2014-04-03 | Direct Nickel Pty Ltd | Method for the recovery of metals from nickel bearing ores and concentrates |
| RU2532871C1 (ru) * | 2013-04-23 | 2014-11-10 | Иван Иванович Калиниченко | Способ переработки окисленных никелевых руд |
| CN103553155B (zh) * | 2013-11-12 | 2016-08-31 | 金川集团股份有限公司 | 一种处理红土矿中间产物的方法 |
| CN104805282A (zh) * | 2014-01-28 | 2015-07-29 | 广西银亿科技矿冶有限公司 | 一种红土镍矿硫酸熟化堆浸方法 |
| FI20145949A (fi) * | 2014-10-29 | 2016-04-30 | Outotec Finland Oy | Menetelmä kullan talteenottamiseksi |
| RU2618595C1 (ru) * | 2016-03-24 | 2017-05-04 | Федеральное государственное бюджетное учреждение науки Институт металлургии Уральского отделения Российской академии наук (ИМЕТ УрО РАН) | Способ извлечения никеля из окисленных никелевых руд |
| CN109763001A (zh) * | 2019-03-20 | 2019-05-17 | 金川集团股份有限公司 | 一种用于氢氧化镍钴盐酸浸出液离子除锌的偏心搅拌离子交换槽 |
| CA3147352A1 (en) | 2019-08-13 | 2021-02-18 | California Institute Of Technology | Process to make calcium oxide or ordinary portland cement from calcium bearing rocks and minerals |
| FI129345B (en) | 2019-12-19 | 2021-12-15 | Crisolteq Ltd | A method for treating a pickling acid regeneration precipitate |
| RU2720703C1 (ru) * | 2019-12-30 | 2020-05-12 | Акционерное общество «Государственный научный центр-Научно-исследовательский институт атомных реакторов» | Способ выделения Ni-63 из облученной мишени и очистки его от примесей |
| BR102022002760B1 (pt) * | 2022-02-14 | 2023-02-07 | Lorintech Tecnologia S.A | Processo de beneficiamento de um concentrado de minério de níquel |
| JP2024031543A (ja) * | 2022-08-26 | 2024-03-07 | プライムプラネットエナジー＆ソリューションズ株式会社 | 疎水性深共晶溶媒の再生方法、およびニッケル浸出方法 |
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| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4097575A (en) * | 1976-11-05 | 1978-06-27 | Amax Inc. | Roast-neutralization-leach technique for the treatment of laterite ore |
| US5178666A (en) * | 1991-12-03 | 1993-01-12 | Inco Limited | Low temperature thermal upgrading of lateritic ores |
| FI93974C (fi) * | 1992-06-18 | 1995-06-26 | Outokumpu Harjavalta Metals Oy | Menetelmä sulfidisten, vaikeasti sulatettavien nikkelirikasteiden tai vastaavien seosten hyödyntämiseksi |
-
1995
- 1995-07-17 US US08/502,923 patent/US5571308A/en not_active Expired - Lifetime
-
1996
- 1996-05-08 PT PT96915562T patent/PT862659E/pt unknown
- 1996-05-08 DE DE1996609624 patent/DE69609624T2/de not_active Expired - Fee Related
- 1996-05-08 RU RU98102860A patent/RU2149910C1/ru active
- 1996-05-08 AT AT96915562T patent/ATE195153T1/de not_active IP Right Cessation
- 1996-05-08 AU AU57310/96A patent/AU705253B2/en not_active Expired
- 1996-05-08 ES ES96915562T patent/ES2152025T3/es not_active Expired - Lifetime
- 1996-05-08 DK DK96915562T patent/DK0862659T3/da active
- 1996-05-08 WO PCT/US1996/006431 patent/WO1997004139A1/en active IP Right Grant
- 1996-05-08 BR BR9609735A patent/BR9609735A/pt not_active IP Right Cessation
- 1996-05-08 EP EP96915562A patent/EP0862659B1/en not_active Expired - Lifetime
- 1996-05-08 CA CA002224218A patent/CA2224218C/en not_active Expired - Lifetime
- 1996-06-24 GT GT199600044A patent/GT199600044A/es unknown
- 1996-06-26 YU YU38796A patent/YU38796A/sh unknown
- 1996-07-09 CU CU1996062A patent/CU22612A3/es not_active IP Right Cessation
- 1996-07-16 CO CO96037399A patent/CO4560492A1/es unknown
-
1998
- 1998-01-09 OA OA9800002A patent/OA10651A/en unknown
-
2000
- 2000-10-23 GR GR20000402352T patent/GR3034662T3/el unknown
Also Published As
| Publication number | Publication date |
|---|---|
| RU2149910C1 (ru) | 2000-05-27 |
| ES2152025T3 (es) | 2001-01-16 |
| DE69609624D1 (de) | 2000-09-07 |
| BR9609735A (pt) | 1999-03-16 |
| CA2224218A1 (en) | 1997-02-06 |
| EP0862659B1 (en) | 2000-08-02 |
| PT862659E (pt) | 2000-11-30 |
| OA10651A (en) | 2001-05-03 |
| EP0862659A1 (en) | 1998-09-09 |
| EP0862659A4 (es) | 1998-09-09 |
| US5571308A (en) | 1996-11-05 |
| CO4560492A1 (es) | 1998-02-10 |
| DK0862659T3 (da) | 2000-12-18 |
| GT199600044A (es) | 1996-06-24 |
| CA2224218C (en) | 2009-08-04 |
| GR3034662T3 (en) | 2001-01-31 |
| MX9800533A (es) | 1998-05-31 |
| YU38796A (sh) | 1998-08-14 |
| WO1997004139A1 (en) | 1997-02-06 |
| DE69609624T2 (de) | 2000-11-23 |
| AU5731096A (en) | 1997-02-18 |
| AU705253B2 (en) | 1999-05-20 |
| ATE195153T1 (de) | 2000-08-15 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| MK | Ceased due to expiration of term |