CN1778826A - 新的多异氰酸酯混合物,其制备方法及其在涂料组合物中的应用 - Google Patents
新的多异氰酸酯混合物,其制备方法及其在涂料组合物中的应用 Download PDFInfo
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- CN1778826A CN1778826A CNA2005101255672A CN200510125567A CN1778826A CN 1778826 A CN1778826 A CN 1778826A CN A2005101255672 A CNA2005101255672 A CN A2005101255672A CN 200510125567 A CN200510125567 A CN 200510125567A CN 1778826 A CN1778826 A CN 1778826A
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- polyisocyanates
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G18/00—Polymeric products of isocyanates or isothiocyanates
- C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
- C08G18/70—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the isocyanates or isothiocyanates used
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G18/00—Polymeric products of isocyanates or isothiocyanates
- C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
- C08G18/28—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the compounds used containing active hydrogen
- C08G18/67—Unsaturated compounds having active hydrogen
- C08G18/671—Unsaturated compounds having only one group containing active hydrogen
- C08G18/672—Esters of acrylic or alkyl acrylic acid having only one group containing active hydrogen
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
- C08F220/00—Copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and only one being terminated by only one carboxyl radical or a salt, anhydride ester, amide, imide or nitrile thereof
- C08F220/02—Monocarboxylic acids having less than ten carbon atoms; Derivatives thereof
- C08F220/04—Acids; Metal salts or ammonium salts thereof
- C08F220/06—Acrylic acid; Methacrylic acid; Metal salts or ammonium salts thereof
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G18/00—Polymeric products of isocyanates or isothiocyanates
- C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
- C08G18/28—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the compounds used containing active hydrogen
- C08G18/40—High-molecular-weight compounds
- C08G18/62—Polymers of compounds having carbon-to-carbon double bonds
- C08G18/6216—Polymers of alpha-beta ethylenically unsaturated carboxylic acids or of derivatives thereof
- C08G18/622—Polymers of esters of alpha-beta ethylenically unsaturated carboxylic acids
- C08G18/6225—Polymers of esters of acrylic or methacrylic acid
- C08G18/6229—Polymers of hydroxy groups containing esters of acrylic or methacrylic acid with aliphatic polyalcohols
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G18/00—Polymeric products of isocyanates or isothiocyanates
- C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
- C08G18/28—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the compounds used containing active hydrogen
- C08G18/40—High-molecular-weight compounds
- C08G18/62—Polymers of compounds having carbon-to-carbon double bonds
- C08G18/6216—Polymers of alpha-beta ethylenically unsaturated carboxylic acids or of derivatives thereof
- C08G18/625—Polymers of alpha-beta ethylenically unsaturated carboxylic acids; hydrolyzed polymers of esters of these acids
- C08G18/6254—Polymers of alpha-beta ethylenically unsaturated carboxylic acids and of esters of these acids containing hydroxy groups
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G18/00—Polymeric products of isocyanates or isothiocyanates
- C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
- C08G18/70—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the isocyanates or isothiocyanates used
- C08G18/81—Unsaturated isocyanates or isothiocyanates
- C08G18/8108—Unsaturated isocyanates or isothiocyanates having only one isocyanate or isothiocyanate group
- C08G18/8116—Unsaturated isocyanates or isothiocyanates having only one isocyanate or isothiocyanate group esters of acrylic or alkylacrylic acid having only one isocyanate or isothiocyanate group
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D133/00—Coating compositions based on homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by only one carboxyl radical, or of salts, anhydrides, esters, amides, imides, or nitriles thereof; Coating compositions based on derivatives of such polymers
- C09D133/04—Homopolymers or copolymers of esters
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D175/00—Coating compositions based on polyureas or polyurethanes; Coating compositions based on derivatives of such polymers
- C09D175/04—Polyurethanes
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10T—TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
- Y10T428/00—Stock material or miscellaneous articles
- Y10T428/31504—Composite [nonstructural laminate]
- Y10T428/31551—Of polyamidoester [polyurethane, polyisocyanate, polycarbamate, etc.]
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- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Health & Medical Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Wood Science & Technology (AREA)
- Polyurethanes Or Polyureas (AREA)
- Addition Polymer Or Copolymer, Post-Treatments, Or Chemical Modifications (AREA)
- Sealing Material Composition (AREA)
Abstract
Description
PIC | 乙酸丁酯[g] | DesmodurN3300[g] | DesmodurN3600[g] | HEA[g] | HEMA[g] | Peroxan[g] | T[℃] |
123456789101112131415161718 | 7575-7575--7575-7575------ | 412.25412.25679.00408.00408.00672.00672.00-------676.62668.78-- | -------412.25412.25679.00408.00408.00672.00672.00--676.62668.78 | 12.1112.1119.9516.1516.1526.6026.6012.1112.1119.9516.1516.1526.6026.60---- | --------------22.3329.8222.3329.82 | 0.640.641.050.850.g51.401.400.640.641.050.850.850.850.851.051.401.051.40 | 130100130130100130100130100130130100130100130130130130 |
PIC | 固体含量[wt%] | 粘度,在23℃下[mPa·s] | NCO含量[wt%] | Hazen色值{APHA} |
123456789101112131415161718 | 84.785.299.985.084.699.999.885.384.7100.085.185.499.910099.899.999.9100 | 59372613,012948151027,30892,0622503143703440664848912,311895812,51130326706 | 16.816.820.016.316.619.518.517.817.821.117.417.420.620.520.820.421.020.5 | 0000111111601190810211911 |
成分 | wt%,固体/固体 |
Dabco 33LVBYK 331BYK 141Tinuvin 292 | (PU催化剂,自Air products,10%在乙0.3酸丁酯中)(流动控制剂,自BYK-Chemie Wesel,DE,0.350%在乙酸丁酯中)(硅氧烷消泡剂,自BYK-Chemie Wesel,0.03DE,3%在11∶2烷基苯/异丁醇中)(光稳定剂,自Ciba Geigy Basel,CH,1.050%在二甲苯中) |
基于多异氰酸酯的清漆 | PIC 1 | PIC 2 | PIC 4 | PIC 5 | PIC 8 | PIC 9 | PIC 11 | PIC 12 | B1 | B2 |
粘度 即刻在1h后在2h后在3h后在4h后在5h后在6h后 | 24242526262728 | 24262626262729 | 25252526272828 | 25252626262828 | 25252526262728 | 25252525262727 | 24252525262728 | 25252525262828 | 25252526272729 | 25252627272728 |
光泽(∠20°)光雾度 | 91<10 | 91<10 | 9014 | 9110 | 9014 | 9012 | 91<10 | 92<10 | 92<10 | 92<10 |
干燥(h) T1T2T3T4 | 1.55.05.57.5 | 1.54.55.57.0 | 1.54.05.07.5 | 1.04.05.07.5 | 2.05.56.58.0 | 2.05.56.58.0 | 2.05.57.08.0 | 2.05.56.08.0 | 2.05.58.0>8 | 2.58.0>8>8 |
摆杆阻尼 即刻(s)在30min后,在 +1d RT60℃下4dRT7dRT | 37131167171 | 39141177181 | 38127167173 | 36130166170 | 58137157161 | 51134157163 | 34124151162 | 31112148152 | 32124164164 | 2198141145 |
耐水性 1)2) 即刻在30min后,在 +1d RT60℃下4dRT7dRT16h50℃ | 20000 | 20000 | 20000 | 20000 | 20000 | 20000 | 20000 | 20000 | 30000 | 40000 |
基于多异氰酸酯的清漆 | PIC 1 | PIC 2 | PIC 4 | PIC 5 | PIC 8 | PIC 9 | PIC 11 | PIC 12 | B1 | B2 |
耐超级 即刻汽油性1)2)在30min后,在 +1d RT60℃下4dRT7dRT16h 50℃ | 42000 | 41-2000 | 41-2000 | 42000 | 420-100 | 420-100 | 41-2000 | 42000 | 4-52-3000 | 4-52-30-100 |
耐MPA性1)2) 即刻在30min后,在 +1d RT60℃下4d RT7d RT16h 50℃ | 42111 | 4310-10-1 | 42000 | 42111 | 43111 | 42111 | 43111 | 43111 | 53111 | 54111 |
耐 即刻二甲苯性1)2)在30min后,在 +1d RT60℃下4dRT7d RT16h 50℃ | 43110-1 | 4310-10-1 | 420-10-10-1 | 42100 | 43110 | 42110 | 4310-10 | 43000 | 53110-1 | 54100 |
硫酸,2% 2% 7d RT浓度1)2)氢氧化钠溶液, 7d RT2%浓度1)2) | 00 | 00 | 00 | 00 | 00 | 00 | 00 | 00 | 00 | 00 |
Claims (8)
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
DE200410056849 DE102004056849A1 (de) | 2004-11-25 | 2004-11-25 | Neue Polyisocyanatgemische, ein Verfahren zu ihrer Herstellung und ihre Verwendung als Härterkomponente in Polyurethanlacken |
DE102004056849.9 | 2004-11-25 |
Publications (2)
Publication Number | Publication Date |
---|---|
CN1778826A true CN1778826A (zh) | 2006-05-31 |
CN1778826B CN1778826B (zh) | 2012-12-05 |
Family
ID=35986232
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
CN2005101255672A Expired - Fee Related CN1778826B (zh) | 2004-11-25 | 2005-11-25 | 新的多异氰酸酯混合物,其制备方法及其在涂料组合物中的应用 |
Country Status (13)
Country | Link |
---|---|
US (2) | US20060111539A1 (zh) |
EP (1) | EP1661929B1 (zh) |
JP (1) | JP2006152294A (zh) |
KR (1) | KR20060058653A (zh) |
CN (1) | CN1778826B (zh) |
AT (1) | ATE517138T1 (zh) |
AU (1) | AU2005237163A1 (zh) |
CA (1) | CA2527548C (zh) |
DE (1) | DE102004056849A1 (zh) |
ES (1) | ES2367901T3 (zh) |
HK (1) | HK1092488A1 (zh) |
MX (1) | MXPA05012607A (zh) |
PL (1) | PL1661929T3 (zh) |
Cited By (7)
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CN102533092A (zh) * | 2010-12-30 | 2012-07-04 | 拜耳材料科技(中国)有限公司 | 一种聚氨酯涂料成膜物、聚氨酯涂料及其应用 |
CN101600750B (zh) * | 2006-09-22 | 2013-03-20 | 佩什托普法国公司 | 多异氰酸酯组合物用于具有提高的亮度的涂料的用途 |
CN109071764A (zh) * | 2015-04-21 | 2018-12-21 | 科思创德国股份有限公司 | 疏水改性的聚异氰脲酸酯塑料及其制造方法 |
CN110997836A (zh) * | 2017-08-09 | 2020-04-10 | 巴斯夫涂料有限公司 | 双组分(2k)清漆和用具有增强视觉外观的双组分(2k)清漆涂布基底的方法 |
CN111320930A (zh) * | 2020-04-09 | 2020-06-23 | 武汉仕全兴聚氨酯科技有限公司 | 无溶剂聚氨酯潮气固化型涂料及其制备方法 |
CN111349212A (zh) * | 2020-04-09 | 2020-06-30 | 武汉仕全兴聚氨酯科技有限公司 | 无溶剂有色多异氰酸酯固化剂及其制备方法与用途 |
CN117429157A (zh) * | 2023-10-18 | 2024-01-23 | 华川建设集团有限公司 | 一种环保涂料装饰型建筑墙体及其制备方法 |
Families Citing this family (13)
Publication number | Priority date | Publication date | Assignee | Title |
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DE102004056849A1 (de) * | 2004-11-25 | 2006-06-08 | Bayer Materialscience Ag | Neue Polyisocyanatgemische, ein Verfahren zu ihrer Herstellung und ihre Verwendung als Härterkomponente in Polyurethanlacken |
DE102005053678A1 (de) * | 2005-11-10 | 2007-05-16 | Bayer Materialscience Ag | Hydrophile Polyisocyanatgemische |
DE102006044035A1 (de) * | 2006-09-14 | 2008-03-27 | Basf Coatings Ag | Calciumhydrogenphosphathaltige Beschichtungszusammensetzung, Verfahren zu ihrer Herstellung, ihre Verwendung und mit ihr beschichtete Substrate |
US20080132724A1 (en) * | 2006-12-04 | 2008-06-05 | Bayer Materialscience Llc | Allophanate modified isocyanates which contain reactive unsaturation |
AU2008228842B2 (en) * | 2007-03-21 | 2014-01-16 | Avery Dennison Corporation | Pressure sensitive adhesives |
EP2236531A1 (de) | 2009-03-31 | 2010-10-06 | Bayer MaterialScience AG | Neue wäßrige 2K PUR-Beschichtungssysteme für verbesserten Korrosionsschutz |
FR2944009B1 (fr) * | 2009-04-01 | 2012-09-07 | Lafarge Sa | Copolymeres superplastifiants reducteurs de viscosite. |
WO2014085701A1 (en) | 2012-11-29 | 2014-06-05 | Entegris, Inc. | Single use dispense head with key code |
CN103709975B (zh) * | 2013-11-29 | 2016-07-06 | 中国科学院长春应用化学研究所 | 用于复合氟塑料薄膜的聚氨酯胶粘剂及其制备方法 |
US20160289456A1 (en) * | 2015-04-03 | 2016-10-06 | Rust Bullet, Llc | No voc paint |
CN111848531A (zh) * | 2019-04-29 | 2020-10-30 | 科思创德国股份有限公司 | 聚氨酯硬质泡沫 |
JP2023553750A (ja) * | 2020-12-18 | 2023-12-25 | ベーアーエスエフ・エスエー | (シクロ)脂肪族ジイソシアネートのポリイソシアネートを含む色安定性硬化剤組成物 |
CN114163612B (zh) * | 2021-11-23 | 2023-07-11 | 万华化学集团股份有限公司 | 一种封闭型多异氰酸酯组合物及其制备方法和用途 |
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DE10043433A1 (de) * | 2000-09-04 | 2002-03-21 | Bayer Ag | Wäßrige 2-K-PUR-Systeme |
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DE10238146A1 (de) * | 2002-08-15 | 2004-02-26 | Basf Ag | Wasseremulgierbare Isocyanate mit verbesserten Eigenschaften |
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DE102004056849A1 (de) * | 2004-11-25 | 2006-06-08 | Bayer Materialscience Ag | Neue Polyisocyanatgemische, ein Verfahren zu ihrer Herstellung und ihre Verwendung als Härterkomponente in Polyurethanlacken |
DE102005053678A1 (de) * | 2005-11-10 | 2007-05-16 | Bayer Materialscience Ag | Hydrophile Polyisocyanatgemische |
-
2004
- 2004-11-25 DE DE200410056849 patent/DE102004056849A1/de not_active Withdrawn
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2005
- 2005-11-12 ES ES05024749T patent/ES2367901T3/es active Active
- 2005-11-12 EP EP20050024749 patent/EP1661929B1/de not_active Not-in-force
- 2005-11-12 AT AT05024749T patent/ATE517138T1/de active
- 2005-11-12 PL PL05024749T patent/PL1661929T3/pl unknown
- 2005-11-22 MX MXPA05012607A patent/MXPA05012607A/es active IP Right Grant
- 2005-11-22 JP JP2005337102A patent/JP2006152294A/ja active Pending
- 2005-11-22 CA CA 2527548 patent/CA2527548C/en not_active Expired - Fee Related
- 2005-11-23 US US11/286,717 patent/US20060111539A1/en not_active Abandoned
- 2005-11-24 KR KR1020050113123A patent/KR20060058653A/ko not_active Application Discontinuation
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- 2005-11-25 CN CN2005101255672A patent/CN1778826B/zh not_active Expired - Fee Related
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Cited By (7)
Publication number | Priority date | Publication date | Assignee | Title |
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CN101600750B (zh) * | 2006-09-22 | 2013-03-20 | 佩什托普法国公司 | 多异氰酸酯组合物用于具有提高的亮度的涂料的用途 |
CN102533092A (zh) * | 2010-12-30 | 2012-07-04 | 拜耳材料科技(中国)有限公司 | 一种聚氨酯涂料成膜物、聚氨酯涂料及其应用 |
CN109071764A (zh) * | 2015-04-21 | 2018-12-21 | 科思创德国股份有限公司 | 疏水改性的聚异氰脲酸酯塑料及其制造方法 |
CN110997836A (zh) * | 2017-08-09 | 2020-04-10 | 巴斯夫涂料有限公司 | 双组分(2k)清漆和用具有增强视觉外观的双组分(2k)清漆涂布基底的方法 |
CN111320930A (zh) * | 2020-04-09 | 2020-06-23 | 武汉仕全兴聚氨酯科技有限公司 | 无溶剂聚氨酯潮气固化型涂料及其制备方法 |
CN111349212A (zh) * | 2020-04-09 | 2020-06-30 | 武汉仕全兴聚氨酯科技有限公司 | 无溶剂有色多异氰酸酯固化剂及其制备方法与用途 |
CN117429157A (zh) * | 2023-10-18 | 2024-01-23 | 华川建设集团有限公司 | 一种环保涂料装饰型建筑墙体及其制备方法 |
Also Published As
Publication number | Publication date |
---|---|
JP2006152294A (ja) | 2006-06-15 |
EP1661929A1 (de) | 2006-05-31 |
AU2005237163A1 (en) | 2006-06-08 |
MXPA05012607A (es) | 2007-07-09 |
US20060111539A1 (en) | 2006-05-25 |
CA2527548C (en) | 2013-10-29 |
EP1661929B1 (de) | 2011-07-20 |
US20100076152A1 (en) | 2010-03-25 |
US8063144B2 (en) | 2011-11-22 |
ES2367901T3 (es) | 2011-11-10 |
HK1092488A1 (en) | 2007-02-09 |
CA2527548A1 (en) | 2006-05-25 |
DE102004056849A1 (de) | 2006-06-08 |
ATE517138T1 (de) | 2011-08-15 |
CN1778826B (zh) | 2012-12-05 |
PL1661929T3 (pl) | 2011-11-30 |
KR20060058653A (ko) | 2006-05-30 |
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