CN1646670A - 酯化脂肪酸的方法和设备 - Google Patents

酯化脂肪酸的方法和设备 Download PDF

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Publication number
CN1646670A
CN1646670A CNA03808273XA CN03808273A CN1646670A CN 1646670 A CN1646670 A CN 1646670A CN A03808273X A CNA03808273X A CN A03808273XA CN 03808273 A CN03808273 A CN 03808273A CN 1646670 A CN1646670 A CN 1646670A
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CN
China
Prior art keywords
reaction section
pressure
reaction
fatty acids
esterification
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Pending
Application number
CNA03808273XA
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English (en)
Chinese (zh)
Inventor
N·艾尔格恩
P·潘宁
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Energea Umwelttechnologie GmbH
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Energea Umwelttechnologie GmbH
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Filing date
Publication date
Application filed by Energea Umwelttechnologie GmbH filed Critical Energea Umwelttechnologie GmbH
Publication of CN1646670A publication Critical patent/CN1646670A/zh
Pending legal-status Critical Current

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    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11C—FATTY ACIDS FROM FATS, OILS OR WAXES; CANDLES; FATS, OILS OR FATTY ACIDS BY CHEMICAL MODIFICATION OF FATS, OILS, OR FATTY ACIDS OBTAINED THEREFROM
    • C11C3/00—Fats, oils, or fatty acids by chemical modification of fats, oils, or fatty acids obtained therefrom
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11C—FATTY ACIDS FROM FATS, OILS OR WAXES; CANDLES; FATS, OILS OR FATTY ACIDS BY CHEMICAL MODIFICATION OF FATS, OILS, OR FATTY ACIDS OBTAINED THEREFROM
    • C11C3/00—Fats, oils, or fatty acids by chemical modification of fats, oils, or fatty acids obtained therefrom
    • C11C3/003—Fats, oils, or fatty acids by chemical modification of fats, oils, or fatty acids obtained therefrom by esterification of fatty acids with alcohols
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C67/00—Preparation of carboxylic acid esters
    • C07C67/08—Preparation of carboxylic acid esters by reacting carboxylic acids or symmetrical anhydrides with the hydroxy or O-metal group of organic compounds
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11C—FATTY ACIDS FROM FATS, OILS OR WAXES; CANDLES; FATS, OILS OR FATTY ACIDS BY CHEMICAL MODIFICATION OF FATS, OILS, OR FATTY ACIDS OBTAINED THEREFROM
    • C11C3/00—Fats, oils, or fatty acids by chemical modification of fats, oils, or fatty acids obtained therefrom
    • C11C3/04—Fats, oils, or fatty acids by chemical modification of fats, oils, or fatty acids obtained therefrom by esterification of fats or fatty oils

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • General Chemical & Material Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Wood Science & Technology (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Fats And Perfumes (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
CNA03808273XA 2002-04-12 2003-04-07 酯化脂肪酸的方法和设备 Pending CN1646670A (zh)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
AT0056902A AT504727A1 (de) 2002-04-12 2002-04-12 Verfahren und anlage zur veresterung von fettsäuren
ATA569/2002 2002-04-12

Publications (1)

Publication Number Publication Date
CN1646670A true CN1646670A (zh) 2005-07-27

Family

ID=29220186

Family Applications (1)

Application Number Title Priority Date Filing Date
CNA03808273XA Pending CN1646670A (zh) 2002-04-12 2003-04-07 酯化脂肪酸的方法和设备

Country Status (18)

Country Link
US (2) US7256301B2 (enExample)
EP (1) EP1495099A1 (enExample)
JP (1) JP2005528472A (enExample)
KR (1) KR20040101446A (enExample)
CN (1) CN1646670A (enExample)
AT (1) AT504727A1 (enExample)
AU (1) AU2003218521B2 (enExample)
BR (1) BR0309199A (enExample)
CA (1) CA2480901A1 (enExample)
EA (1) EA007630B1 (enExample)
HR (1) HRP20041057A2 (enExample)
MX (1) MXPA04010015A (enExample)
NO (1) NO20044930L (enExample)
PL (1) PL371212A1 (enExample)
RS (1) RS90004A (enExample)
UA (1) UA78767C2 (enExample)
WO (1) WO2003087278A1 (enExample)
ZA (1) ZA200408018B (enExample)

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1919973B (zh) * 2006-09-08 2011-04-06 浙江赞宇科技股份有限公司 一种连续式制备生物柴油的方法
CN105176696A (zh) * 2008-04-01 2015-12-23 Sk化学株式会社 使用脂肪酸制备脂肪酸烷基酯的方法

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PL341110A1 (en) 1997-11-24 2001-03-26 Energea Umwelttechnologie Gmbh Method of obtaining methyl esters of fatty acids and system therefor
AT504727A1 (de) 2002-04-12 2008-07-15 Energea Umwelttechnologie Gmbh Verfahren und anlage zur veresterung von fettsäuren
MY150129A (en) * 2004-04-09 2013-11-29 Archer Daniels Midland Co Method of preparing fatty acid alkyl esters from waste or recycled fatty acid stock
JP2006036817A (ja) * 2004-07-22 2006-02-09 Kimura Chem Plants Co Ltd 脂肪酸エステルの製造方法および製造装置
KR100799597B1 (ko) * 2006-04-07 2008-01-30 (주)두웰테크놀로지 고효율 환형 반응기를 이용한 대체 연료 제조 장치 및 방법
PL2013319T3 (pl) 2006-04-28 2019-07-31 Sk Chemicals Co., Ltd. Sposób wytwarzania estru alkilowego kwasu tłuszczowego z użyciem destylatu kwasu tłuszczowego
US7767839B2 (en) * 2006-08-24 2010-08-03 Philadelphia Fry-O-Diesel, Inc. Process of making alkyl esters of free fatty acids
JP2008207135A (ja) * 2007-02-27 2008-09-11 National Univ Corp Shizuoka Univ 水熱酸化分解処理装置
US8052848B2 (en) * 2007-06-26 2011-11-08 The Penn State Research Foundation Ultrasonic and microwave methods for enhancing the rate of a chemical reaction and apparatus for such methods
DE102008007431A1 (de) * 2008-02-01 2009-08-13 Bayer Technology Services Gmbh Verbessertes Verfahren zur heterogen katalysierten Veresterung von Fettsäuren
CA2701136C (en) * 2007-11-30 2013-01-08 Her Majesty The Queen In Right Of Canada As Represented By The Minister Of Natural Resources Canada Vapour phase esterification of free fatty acids
KR101554607B1 (ko) 2008-11-07 2015-09-22 에스케이케미칼주식회사 지방산을 이용한 지방산알킬에스테르의 제조방법 및 장치
ITNA20090024A1 (it) * 2009-05-08 2010-11-09 Eurochem Engineering S R L Uso di reattori innovativi per reazioni multifasiche liquido-liquido.
DE102009044168A1 (de) * 2009-10-02 2011-04-07 Green Finance Ag Verfahren und Vorrichtung zur kontinuierlichen Herstellung von Alkylestern höherer Fettsäuren
MY151440A (en) 2009-10-29 2014-05-30 Malaysian Palm Oil Board Mpob A method of converting free fatty acid (ffa) from oil to methyl ester
JP2014040527A (ja) * 2012-08-22 2014-03-06 Osaka Prefecture Univ 脂肪酸アルキルエステルの精製方法
KR102327852B1 (ko) 2013-07-22 2021-11-18 에스케이에코프라임 주식회사 지방을 이용한 지방산알킬에스테르의 제조방법
US9328054B1 (en) 2013-09-27 2016-05-03 Travis Danner Method of alcoholisis of fatty acids and fatty acid gyicerides
WO2017042750A1 (en) 2015-09-11 2017-03-16 Enc Bioenergy Lda. Glycerol ester production from wastes containing organic oils and/or fats
PT109991A (pt) 2017-03-24 2018-09-24 Univ Do Porto Catalisadores heterogéneos, processo de preparação e sua aplicação no processo de produção de ésteres alquílicos deácidos gordos.
FI128952B (en) * 2019-09-26 2021-03-31 Neste Oyj Preparation of renewable alkenes including metathesis
FI128954B (en) 2019-09-26 2021-03-31 Neste Oyj Preparation of renewable base oil including metathesis
FI128953B (en) 2019-09-26 2021-03-31 Neste Oyj Production of renewable chemicals including metathesis and microbial oxidation
US11944955B2 (en) 2021-06-25 2024-04-02 Petróleo Brasileiro S.A.—Petrobras Process of obtaining a catalyst, catalyst and pre-treatment process of acidic raw materials
CN113563977B (zh) * 2021-07-21 2022-08-16 湖北天基生物能源科技发展有限公司 一种废弃油脂的处理系统和处理方法
BR102021016123A2 (pt) 2021-08-16 2023-02-23 Petróleo Brasileiro S.A. - Petrobras Processo para produção de biodiesel a partir de cargas ácidas

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US2583206A (en) 1949-12-01 1952-01-22 Separator Ab Apparatus for homogenizing
US2766273A (en) * 1951-05-04 1956-10-09 Pfizer & Co C Esterification of acids
US3614069A (en) 1969-09-22 1971-10-19 Fibra Sonics Multiple frequency ultrasonic method and apparatus for improved cavitation, emulsification and mixing
JPS6025478B2 (ja) 1977-03-17 1985-06-18 花王株式会社 脂肪酸低級アルコ−ルエステルの製造法
JPS55149395A (en) 1979-05-09 1980-11-20 Kao Corp Continuous purification of oil and fat
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DE3339051A1 (de) 1983-10-28 1985-05-09 Henkel KGaA, 4000 Düsseldorf Verfahren zur verbesserten destillativen aufarbeitung von glycerin
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US5514820A (en) 1989-09-29 1996-05-07 Henkel Kommanditgesellschaft Auf Aktien Continuous process for the production of lower alkyl esters
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DE59103713D1 (de) 1991-09-02 1995-01-12 Primavesi Markus Verfahren und Vorrichtung zur kontinuierlichen Herstellung von Fettsäureestern.
US5324853A (en) * 1993-01-19 1994-06-28 Exxon Chemical Patents Inc. Process for the production of plasticizer and polyolesters
US5388905A (en) 1993-03-30 1995-02-14 Or-Tec, Inc. Polymer mixing/activation system
US5424467A (en) 1993-07-14 1995-06-13 Idaho Research Foundation Method for purifying alcohol esters
AT399336B (de) 1993-07-14 1995-04-25 Martin Mag Dr Mittelbach Verfahren zur herstellung von fettsäurealkylestern
US5482633A (en) 1993-10-12 1996-01-09 Cargill, Incorporated Process for removing vegetable oil waxes by fast cooling vegetable oil and using a porous non-metallic inorganic filter
DE4338111A1 (de) 1993-11-08 1995-05-11 Henkel Kgaa Verfahren zur Herstellung von Fettsäureniedrigalkylestern
US5645696A (en) 1994-11-21 1997-07-08 Lucky Ltd. Process for preparing unsaturated carboxylic acid esters and apparatus for preparing the same
US5945529A (en) * 1996-07-19 1999-08-31 The Procter & Gamble Company Synthesis of polyol fatty acid polyesters using column with inert gas stripping
JP3579757B2 (ja) * 1996-08-10 2004-10-20 チッソ株式会社 反応槽及びカルボン酸エステル製造方法
US6174501B1 (en) * 1997-10-31 2001-01-16 The Board Of Regents Of The University Of Nebraska System and process for producing biodiesel fuel with reduced viscosity and a cloud point below thirty-two (32) degrees fahrenheit
US6015440A (en) 1997-10-31 2000-01-18 Board Of Regents Of The University Of Nebraska Process for producing biodiesel fuel with reduced viscosity and a cloud point below thirty-two (32) degrees fahrenheit
PL341110A1 (en) 1997-11-24 2001-03-26 Energea Umwelttechnologie Gmbh Method of obtaining methyl esters of fatty acids and system therefor
US5938328A (en) * 1998-07-07 1999-08-17 Atlantic Richfield Company Packed bed static mixer
AT410443B (de) * 2000-11-08 2003-04-25 Wimmer Theodor Verfahren zur herstellung von fettsäureestern niederer alkohole
AT504727A1 (de) 2002-04-12 2008-07-15 Energea Umwelttechnologie Gmbh Verfahren und anlage zur veresterung von fettsäuren

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1919973B (zh) * 2006-09-08 2011-04-06 浙江赞宇科技股份有限公司 一种连续式制备生物柴油的方法
CN105176696A (zh) * 2008-04-01 2015-12-23 Sk化学株式会社 使用脂肪酸制备脂肪酸烷基酯的方法

Also Published As

Publication number Publication date
KR20040101446A (ko) 2004-12-02
AU2003218521B2 (en) 2009-05-28
EA007630B1 (ru) 2006-12-29
ZA200408018B (en) 2005-10-05
EA200401356A1 (ru) 2005-04-28
US7256301B2 (en) 2007-08-14
MXPA04010015A (es) 2004-12-13
EP1495099A1 (de) 2005-01-12
WO2003087278A1 (de) 2003-10-23
HRP20041057A2 (en) 2005-06-30
US20050065357A1 (en) 2005-03-24
JP2005528472A (ja) 2005-09-22
AU2003218521A1 (en) 2003-10-27
BR0309199A (pt) 2005-02-09
AT504727A1 (de) 2008-07-15
RS90004A (sr) 2006-12-15
US20070185341A1 (en) 2007-08-09
NO20044930L (no) 2004-11-11
PL371212A1 (en) 2005-06-13
CA2480901A1 (en) 2003-10-23
UA78767C2 (en) 2007-04-25

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