CN1315309A - Cell-activating agent for biological and medicinal fertilizer and its preparing process - Google Patents
Cell-activating agent for biological and medicinal fertilizer and its preparing process Download PDFInfo
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Abstract
A cell-activating agent as biological-medicinal fertilizer for the agricultural crops (rice, wheat, etc), cotton, vegetable, fruit tree, etc. contains methamino abamectin benzoate, potassium dihydrogen phosphate, chelated trace elements and 8 Chinese medicinal materials including flavescent sophora root, nux vomica seed, etc.. Its features high effect on germinating, growing root, developing, bearing fruit, and preventing and eliminating diseases and pests.
Description
The present invention relates to agricultural plants medicine fertilizer, especially a kind of cell-activating agent for biological and medicinal fertilizer and preparation technology thereof.
At present China's agricultural is as main field plant culture element basically with chemical pesticide or fertilizer.Through application practice for a long time, people have recognized the harm of chemical pesticide and fertilizer.To such an extent as to the international and domestic research that has generally begun biological plant fertilizer or agricultural chemicals.The inventor has also carried out intensive research in this respect, the state of the art in this field is had understanding more clearly, and invented as patent of invention projects such as activating agent for animal and plant cells, biological plant insecticides.By theoretical investigation and application practice, feel the utilization of China's Chinese medicinal materials on plant not enough, utilize cell-activating agent for biological and medicinal fertilizer and the preparation technology thereof of Chinese medicine so invented for conditioning agent, by retrieval, do not find that other people is constructed yet.
The object of the present invention is to provide a kind of cell-activating agent for biological and medicinal fertilizer and preparation technology thereof who utilizes Chinese medicinal materials for additive, this product as fertilizer sources can effectively promote the growth of plant, and the disease and pest of plant can effectively be prevented and treat to its property of medicine that includes.
The object of the present invention is achieved like this:
Its weight proportion of this cell-activating agent for biological and medicinal fertilizer is:
Emamectin-benzoate 0.15-0.25%
Potassium primary phosphate 7-9%
Dipotassium hydrogen phosphate 6-7%
Xanthohumic acid is received 3-4%
Chelated microelement (zinc, molybdenum, iron, manganese, copper, boron) 6-8%
Kuh-seng 2-3%
Trypterygine 2-3.5%
Nux vomica 1-2.5%
Fructus Toosendan 3-4%
Kosam seeds 3-4.5%
Vicious 3-4%
Black false hellebore 3-4.5%
Radix Alangii 2.5-3.5%
Emulsifying agent 2.5-3.5%
Sanitas 0.2-0.6%
Stablizer 0.4-0.6%
Other add ethanol to 100%.
Preparation technology is (by a finished product per ton):
(1) inject 100 kilograms of ethanol in one ton of high speed reactor, behind the heat temperature raising to 85 ℃, add 100 kilograms of SODLUM FULVATE filtrates, stirred 35 minutes in 15 minutes at every interval, stirs altogether three times;
(2) after the high speed temperature of reaction kettle was reduced to 80 ℃, adding kuh-seng, trypterygine, nux vomica, Fructus Toosendan, kosam seeds, viciousness, black false hellebore, Radix Alangii mixed 205 kilograms of vat liquors, and stirred 35 minutes in 15 minutes at every interval, stirs altogether three times;
(3) the high speed reactor temperature is in the time of 65 ℃, adds 300 kilograms of potassium primary phosphates, dipotassium hydrogen phosphate, chelated microelement (zinc, molybdenum, iron, manganese, copper, boron) filtrate, and stirred 35 minutes in 15 minutes at every interval, stirs altogether three times;
When (4) the high speed reactor temperature is reduced to 60 ℃, add 50 kilograms of emamectin-benzoate filtrates, stirred 35 minutes in 15 minutes at every interval, stirs altogether three times;
When (5) the high speed reactor temperature is reduced to 50 ℃, add emulsifying agent, sanitas, stablizer successively, add each and all stirred in 15 minutes and stirred altogether three times in 35 minutes at every interval;
(6) injecting ethanol then is one ton until solution, stirs 45 minutes, filter the back finished fluid.
The described emulsifying agent of this cell-activating agent for biological and medicinal fertilizer is a castor oil polyoxyethylene ether, and described sanitas is a potassium sorbate, and described stablizer is the ethyl cellulose that contracts; The preparation technology of described SODLUM FULVATE filtrate is (by a finished product per ton): SODLUM FULVATE takes by weighing 30 kilograms, puts into 0.5 ton of reactor, adds the ethanol 120 kg, and heating makes reactor temperature rise to 85 ℃, and keeps this temperature 3 hours, filters the back and extracts filtrate; Described kuh-seng, trypterygine, nux vomica, Fructus Toosendan, kosam seeds, vicious, black false hellebore, the preparation technology that Radix Alangii mixes vat liquor filtrate is (by a finished product per ton): with these eight kinds of Chinese medicinal materials raw material stoving, moisture is not more than 15%, all be crushed to the 40-50 order, take by weighing 20 kilograms of kuh-sengs respectively, 20 kilograms of trypterygines, 20 kilograms of nux vomicas, 30 kilograms of Fructus Toosendans, 30 kilograms of kosam seeds, vicious 30 kilograms, 30 kilograms of black false hellebores, 25 kilograms of Radix Alangiis are all dropped in 2 tons of extractors simultaneously, add 820 kilograms of ethanol, heating makes the temperature to 85 ℃ of extractor, and under this temperature, soaked 8 hours, lixiviate three times altogether therebetween, and be concentrated to add Chinese medicinal materials weight, filter then, extract vat liquor; The preparation technology of described emamectin-benzoate filtrate is (by a finished product per ton): emamectin-benzoate takes by weighing 1.5 kilograms, put into 0.25 ton of reactor, add 50 kilograms of ethanol, heating makes reactor temperature rise to 60 ℃, and keep this temperature, stirred 30 minutes, and filtered the back and extract filtrate; Described potassium primary phosphate, dipotassium hydrogen phosphate, chelated microelement (zinc, molybdenum, iron, manganese, copper, boron) filtrate preparation technology are (by finished product per ton): inject 200 kilograms of ethanol in 0.5 ton of reactor, heating makes reactor temperature rise to 60 ℃, take by weighing 70 kilograms of potassium primary phosphates respectively, 60 kilograms of dipotassium hydrogen phosphates, 60 kilograms of chelated microelements (zinc, molybdenum, iron, manganese, copper, boron), all all drop in the reactor simultaneously, stirred 30 minutes in 10 minutes at every interval, stir twice altogether, filter the back and extract filtrate.
Advantage of the present invention and positively effect are: the present invention can be widely used in farm crop, as paddy and wheat class food crop, linen-cotton class cash crop, and vegetables, fruits and vegetables, rudiment, root of hair, fertility, solid to plant all have excellent efficacies; Anti-disease and insect resistance to above-mentioned crop also has good effect.
Embodiments of the invention are (below be weight proportion, by finished product per ton):
One, this cell-activating agent for biological and medicinal fertilizer includes following material, and its title and content range are as follows:
Emamectin-benzoate 0.15-0.25%
Potassium primary phosphate 7-9%
Dipotassium hydrogen phosphate 6-7%
Xanthohumic acid is received 3-4%
Chelated microelement (zinc, molybdenum, iron, manganese, copper, boron) 6-8%
Kuh-seng 2-3%
Trypterygine 2-3.5%
Nux vomica 1-2.5%
Fructus Toosendan 3-4%
Kosam seeds 3-4.5%
Vicious 3-4%
Black false hellebore 3-4.5%
Radix Alangii 2.5-3.5%
Emulsifying agent 2.5-3.5%
Sanitas 0.2-0.6%
Stablizer 0.4-0.6%
Other add ethanol to 100%.
Wherein, the chemical content of described emamectin-benzoate is:
EB?B
1a≥90％ EB?B
1b≤10％
Molecular formula is: EBB
1aC
49H
75NO
13C
7H
6O
2
EBB
1bC
48H
73NO
13·C
7H
6O
2
Described emulsifying agent is commercially available castor oil polyoxyethylene ether, and described sanitas is a potassium sorbate, and described stablizer is the ethyl cellulose that contracts.
Two, the content of each material of most preferred embodiment of the present invention is:
1. emamectin-benzoate 0.2%
2. potassium primary phosphate 7%
3. dipotassium hydrogen phosphate 8%
4. xanthohumic acid receives 3%
5. chelated microelement
(zinc, molybdenum, iron, manganese, copper, boron) 6%
6. kuh-seng 2.5%
7. trypterygine 2%
8. nux vomica 2%
9. Fructus Toosendan 3%
10. kosam seeds 4.5%
11. vicious 3%
12. black false hellebore 4%
13. Radix Alangii 3%
14. emulsifying agent 3%
15. sanitas 0.4%
16. stablizer 0.5%
17. ethanol 47.9%.
Three, feedstock production
(1) preparation technology of described SODLUM FULVATE filtrate is: SODLUM FULVATE takes by weighing 30 kilograms, puts into 0.5 ton of reactor, adds the ethanol 120 kg, heating makes reactor temperature rise to 85 ℃, and kept this temperature 3 hours, and filter the back and extract filtrate, in adding lid container, deposit stand-by.
(2) preparation technology of kuh-seng, trypterygine, nux vomica, Fructus Toosendan, kosam seeds, viciousness, black false hellebore, Radix Alangii mixing vat liquor is:
With these eight kinds of Chinese medicinal materials raw material stoving, moisture is not more than 15%, is respectively machined to the 40-50 order, take by weighing 20 kilograms of kuh-sengs then respectively, 20 kilograms of trypterygines, 20 kilograms of nux vomicas, 30 kilograms of Fructus Toosendans, 30 kilograms of kosam seeds, vicious 30 kilograms, 30 kilograms of black false hellebores, 25 kilograms of Radix Alangiis, all drop in 2 tons of extractors simultaneously, add 820 kilograms of ethanol, soaked at normal temperatures 3-5 days, heating makes the temperature to 85 ℃ of extractor then, and under this temperature, soaked 8 hours, altogether lixiviate three times therebetween, evaporation concentration to add Chinese medicinal materials weight, filter with 100 order strainers then, extract vat liquor, seal up for safekeeping stand-by.
(3) emamectin-benzoate takes by weighing 1.5 kilograms, puts into 0.25 ton of reactor, adds 50 kilograms of ethanol, and heating makes reactor temperature rise to 60 ℃, and keeps under this temperature conditions and stirred 30 minutes, filters the back and extracts filtrate, seals up for safekeeping stand-by.
(4) in 0.5 ton of reactor, inject 200 kilograms of ethanol, heating makes reactor temperature rise to 60 ℃, take by weighing 70 kilograms of potassium primary phosphates respectively, 60 kilograms of dipotassium hydrogen phosphates, 60 kilograms of chelated microelements (zinc, molybdenum, iron, manganese, copper, boron) add in the reactor, stirred 30 minutes in 10 minutes at every interval, stir twice altogether, filter the back and extract filtrate, seal up for safekeeping stand-by.
Four, preparation technology
(1) inject 100 kilograms of ethanol in one ton of high speed reactor, behind the heat temperature raising to 85 ℃, add 100 kilograms of SODLUM FULVATE filtrates, stirred 35 minutes in 15 minutes at every interval, stirs altogether three times.
(2) after the high speed temperature of reaction kettle is reduced to 80 ℃, adding kuh-seng, trypterygine, nux vomica, Fructus Toosendan, kosam seeds, viciousness, black false hellebore, Radix Alangii mix 205 kilograms of vat liquors, and stirred 35 minutes in 15 minutes at every interval, stirs altogether three times.
(3) the high speed reactor temperature is in the time of 65 ℃, adds 300 kilograms of potassium primary phosphates, dipotassium hydrogen phosphate, chelated microelement (zinc, molybdenum, iron, manganese, copper, boron) filtrate, and stirred 35 minutes in 15 minutes at every interval, stirs altogether three times.
(4) when the high speed reactor temperature is reduced to 60 ℃, add 50 kilograms of emamectin-benzoate filtrates, stirred 35 minutes in 15 minutes at every interval, stirs altogether three times.
When (5) the high speed reactor temperature is reduced to 50 ℃, add emulsifying agent, sanitas, stablizer successively, add each and all stirred 35 minutes in 15 minutes, stir altogether three times at every interval by proportioning.
(6) injecting ethanol then is one ton until solution, stirs 45 minutes, filter the back finished fluid.
Claims (7)
1. cell-activating agent for biological and medicinal fertilizer is characterized in that:
Its weight proportion is:
Emamectin-benzoate 0.15-0.25%
Potassium primary phosphate 7-9%
Dipotassium hydrogen phosphate 6-7%
Xanthohumic acid is received 3-4%
Chelated microelement (zinc, molybdenum, iron, manganese, copper, boron) 6-8%
Kuh-seng 2-3%
Trypterygine 2-3.5%
Nux vomica 1-2.5%
Fructus Toosendan 3-4%
Kosam seeds 3-4.5%
Vicious 3-4%
Black false hellebore 3-4.5%
Radix Alangii 2.5-3.5%
Emulsifying agent 2.5-3.5%
Sanitas 0.2-0.6%
Stablizer 0.4-0.6%
Other add ethanol to 100%.
2. preparation technology who realizes the described cell-activating agent for biological and medicinal fertilizer of claim 1 is characterized in that: preparation technology is (by finished product per ton):
(1) inject 100 kilograms of ethanol in one ton of high speed reactor, behind the heat temperature raising to 85 ℃, add 100 kilograms of SODLUM FULVATE filtrates, stirred 35 minutes in 15 minutes at every interval, stirs altogether three times;
(2) after the high speed temperature of reaction kettle was reduced to 80 ℃, adding kuh-seng, trypterygine, nux vomica, Fructus Toosendan, kosam seeds, viciousness, black false hellebore, Radix Alangii mixed 205 kilograms of vat liquors, and stirred 35 minutes in 15 minutes at every interval, stirs altogether three times;
(3) the high speed reactor temperature is in the time of 65 ℃, adds 300 kilograms of potassium primary phosphates, dipotassium hydrogen phosphate, chelated microelement (zinc, molybdenum, iron, manganese, copper, boron) filtrate, and stirred 35 minutes in 15 minutes at every interval, stirs altogether three times;
When (4) the high speed reactor temperature is reduced to 60 ℃, add 50 kilograms of emamectin-benzoate filtrates, stirred 35 minutes in 15 minutes at every interval, stirs altogether three times;
When (5) the high speed reactor temperature is reduced to 50 ℃, add emulsifying agent, sanitas, stablizer successively, add each and all stirred in 15 minutes and stirred altogether three times in 35 minutes at every interval;
(6) injecting ethanol then is one ton until solution, stirs 45 minutes, filter the back finished fluid.
3. cell-activating agent for biological and medicinal fertilizer according to claim 1 and 2 and preparation technology thereof is characterized in that, described emulsifying agent is a castor oil polyoxyethylene ether, and described sanitas is a potassium sorbate, and described stablizer is the ethyl cellulose that contracts.
4. cell-activating agent for biological and medicinal fertilizer according to claim 1 and 2 and preparation technology thereof, it is characterized in that: the preparation technology of described SODLUM FULVATE filtrate is (by finished product per ton): SODLUM FULVATE takes by weighing 30 kilograms, put into 0.5 ton of reactor, add the ethanol 120 kg, heating makes reactor temperature rise to 85 ℃, and kept this temperature 3 hours, filter the back and extract filtrate.
5. cell-activating agent for biological and medicinal fertilizer according to claim 1 and 2 and preparation technology thereof, it is characterized in that: described kuh-seng, trypterygine, nux vomica, Fructus Toosendan, kosam seeds, vicious, black false hellebore, the preparation technology that Radix Alangii mixes vat liquor filtrate is (by a finished product per ton): with these eight kinds of Chinese medicinal materials raw material stoving, moisture is not more than 15%, all be crushed to the 40-50 order, take by weighing 20 kilograms of kuh-sengs respectively, 20 kilograms of trypterygines, 20 kilograms of nux vomicas, 30 kilograms of Fructus Toosendans, 30 kilograms of kosam seeds, vicious 30 kilograms, 30 kilograms of black false hellebores, 25 kilograms of Radix Alangiis, all drop in 2 tons of extractors simultaneously, add 820 kilograms of ethanol, heating makes the temperature to 85 ℃ of extractor, and soaks 8 hours under this temperature, be total to lixiviate three times therebetween, and be concentrated to add Chinese medicinal materials weight, filter then, extract vat liquor.
6. cell-activating agent for biological and medicinal fertilizer according to claim 1 and 2 and preparation technology thereof, it is characterized in that: the preparation technology of described emamectin-benzoate filtrate is (by finished product per ton): emamectin-benzoate takes by weighing 1.5 kilograms, put into 0.25 village reactor, add 50 kilograms of ethanol, heating makes reactor temperature rise to 60 ℃, and keep this temperature, and stirred 30 minutes, filter the back and extract filtrate.
7. cell-activating agent for biological and medicinal fertilizer according to claim 1 and 2 and preparation technology thereof, it is characterized in that: described potassium primary phosphate, dipotassium hydrogen phosphate, chelated microelement (zinc, molybdenum, iron, manganese, copper, boron) filtrate preparation technology is (by a finished product per ton): inject 200 kilograms of ethanol in 0.5 ton of reactor, heating makes reactor temperature rise to 60 ℃, take by weighing 70 kilograms of potassium primary phosphates respectively, 60 kilograms of dipotassium hydrogen phosphates, chelated microelement (zinc, molybdenum, iron, manganese, copper, boron) 60 kilograms, all all drop in the reactor simultaneously, stirred 30 minutes in 10 minutes at every interval, stir twice altogether, filter the back and extract filtrate.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CNB001032887A CN1139558C (en) | 2000-03-23 | 2000-03-23 | Cell-activating agent for biological and medicinal fertilizer and its preparing process |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CNB001032887A CN1139558C (en) | 2000-03-23 | 2000-03-23 | Cell-activating agent for biological and medicinal fertilizer and its preparing process |
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|---|---|
| CN1315309A true CN1315309A (en) | 2001-10-03 |
| CN1139558C CN1139558C (en) | 2004-02-25 |
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| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CNB001032887A Expired - Lifetime CN1139558C (en) | 2000-03-23 | 2000-03-23 | Cell-activating agent for biological and medicinal fertilizer and its preparing process |
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|---|---|
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Cited By (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN100350844C (en) * | 2006-07-26 | 2007-11-28 | 浙江林学院 | Bacteriostatic organic-inorganic composite fertilizer and its production process |
| CN101223892B (en) * | 2008-01-25 | 2011-04-20 | 辛贵有 | Toosendanin-containing compound pesticide and preparing method thereof |
| CN102503698A (en) * | 2011-11-10 | 2012-06-20 | 中国农业科学院农业资源与农业区划研究所 | Chelated trace element fertilizer-medicament mixture |
| CN103254014A (en) * | 2013-05-28 | 2013-08-21 | 余志高 | Production process of multi-nutrition revitalizing potassium base fertilizer |
| CN103755486A (en) * | 2013-12-25 | 2014-04-30 | 枣庄市沃丰化工有限公司 | Compound traditional Chinese medicine liquid foliar fertilizer and production method thereof |
| CN104041532A (en) * | 2014-05-05 | 2014-09-17 | 邯郸市建华植物农药厂 | Efficient sterilization yield-increasing suspending agent and production method and application thereof |
| CN107056418A (en) * | 2017-02-16 | 2017-08-18 | 梁慰爱 | A kind of mulch base manure and preparation method thereof |
| US9980479B2 (en) | 2004-06-07 | 2018-05-29 | Syngenta Crop Protection, Llc | Method of reducing nematode damage |
Families Citing this family (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN100423645C (en) * | 2005-07-05 | 2008-10-08 | 吴新忠 | Foliage fertilizer capable of make rabbit, mouse (poultry) keep away while smelling and animal expelling agent |
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2000
- 2000-03-23 CN CNB001032887A patent/CN1139558C/en not_active Expired - Lifetime
Cited By (11)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US9980479B2 (en) | 2004-06-07 | 2018-05-29 | Syngenta Crop Protection, Llc | Method of reducing nematode damage |
| CN100350844C (en) * | 2006-07-26 | 2007-11-28 | 浙江林学院 | Bacteriostatic organic-inorganic composite fertilizer and its production process |
| CN101223892B (en) * | 2008-01-25 | 2011-04-20 | 辛贵有 | Toosendanin-containing compound pesticide and preparing method thereof |
| CN102503698A (en) * | 2011-11-10 | 2012-06-20 | 中国农业科学院农业资源与农业区划研究所 | Chelated trace element fertilizer-medicament mixture |
| CN102503698B (en) * | 2011-11-10 | 2013-11-13 | 中国农业科学院农业资源与农业区划研究所 | Chelated trace element fertilizer-medicament mixture |
| CN103254014A (en) * | 2013-05-28 | 2013-08-21 | 余志高 | Production process of multi-nutrition revitalizing potassium base fertilizer |
| CN103755486A (en) * | 2013-12-25 | 2014-04-30 | 枣庄市沃丰化工有限公司 | Compound traditional Chinese medicine liquid foliar fertilizer and production method thereof |
| CN103755486B (en) * | 2013-12-25 | 2016-02-03 | 枣庄市沃丰化工有限公司 | A kind of Compound traditional Chinese medicine liquid foliar fertilizer and preparation method thereof |
| CN104041532A (en) * | 2014-05-05 | 2014-09-17 | 邯郸市建华植物农药厂 | Efficient sterilization yield-increasing suspending agent and production method and application thereof |
| CN104041532B (en) * | 2014-05-05 | 2016-08-24 | 邯郸市建华植物农药厂 | A kind of efficient sterilizing increases production suspending agent and production method thereof and application |
| CN107056418A (en) * | 2017-02-16 | 2017-08-18 | 梁慰爱 | A kind of mulch base manure and preparation method thereof |
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| Publication number | Publication date |
|---|---|
| CN1139558C (en) | 2004-02-25 |
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