CN1124245C - Huangningsu biological medicinal fertilizer and productive technology thereof - Google Patents

Huangningsu biological medicinal fertilizer and productive technology thereof Download PDF

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Publication number
CN1124245C
CN1124245C CN99122544A CN99122544A CN1124245C CN 1124245 C CN1124245 C CN 1124245C CN 99122544 A CN99122544 A CN 99122544A CN 99122544 A CN99122544 A CN 99122544A CN 1124245 C CN1124245 C CN 1124245C
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China
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fertilizer
peat
huangningsu
test
acid
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CN99122544A
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CN1295993A (en
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刘德玉
胡湘韩
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DONGBEI DESIGN RESEARCH BRANCH CHINESE COMPREHENSIVE DEVELOPMENT RESEARCH INST
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DONGBEI DESIGN RESEARCH BRANCH CHINESE COMPREHENSIVE DEVELOPMENT RESEARCH INST
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Priority to CN99122544A priority Critical patent/CN1124245C/en
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    • CCHEMISTRY; METALLURGY
    • C05FERTILISERS; MANUFACTURE THEREOF
    • C05GMIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
    • C05G3/00Mixtures of one or more fertilisers with additives not having a specially fertilising activity
    • C05G3/60Biocides or preservatives, e.g. disinfectants, pesticides or herbicides; Pest repellants or attractants

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  • Life Sciences & Earth Sciences (AREA)
  • Pest Control & Pesticides (AREA)
  • Plant Pathology (AREA)
  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Fertilizers (AREA)

Abstract

The present invention relates to Huangningsu as a biological medicinal fertilizer and a production technique thereof. The biological medicinal fertilizer is formed by compounding 1 % of complete plant fertilizer and 5 % of Ningnan zymoid, wherein the complete plant fertilizer comprises 1.2 to 1.4% of peat coal xanthohumic acid, 1.1 to 1.4% of nitrogen, 1.0 to 1.2% of phosphorus pentoxide, 3.9 to 4.1% of potassium oxide and 0.7 to 0.9% of zinc. The production technique comprises the steps of pulverization and sieving, pulverizing raw materials to 40 meshes, leaching, shaking for precipitation, stirring for acid regulation, and centrifugal separation for obtaining the peat coal xanthohumic acid, and then, the complete plant fertilizer is proportionally compounded with the Ningnan zymoid after the components are mixed in order according to the proportion. The present invention combines the functions of medicines and fertilizers and promotes the high yield, favorable quality and high efficiency of crops.

Description

Huangningsu biological medicinal fertilizer and production technique
The invention belongs to a kind of biological medicine fertilizer and production technique.
Existing composite fertilizer, majority has only fertilizer efficiency, no drug effect.At present existing existing drug effects have the medicine of fertilizer efficiency fertile in biochemical fulvic acid medicine fertilizer again, and it is that biochemical fulvic acid is concentrated, and with the resultant of organic pesticide Belmark, monocrotophos, methyl alcohol mixed liquor hybrid reaction, it wherein has chemical pesticide again.
The purpose of this invention is to provide a kind of existing drug effect, fertilizer efficiency is arranged again, and do not have chemical pesticide, is pollution-free, non-harmful Huangningsu biological medicinal fertilizer and the production technique that is re-dubbed by biological pesticide and the full fertilizer of plant.
Technical scheme of the present invention:
The present invention is by Ningnanmycin and composite the forming of the full rich water solution of plant.
The full rich water solution of plant comprises peat xanthohumic acid, nitrogen, Vanadium Pentoxide in FLAKES, potassium oxide, zinc and water.
The shared weight percent of above-mentioned each component is:
Peat xanthohumic acid 1.2-1.4%
Nitrogen 1.1-1.4%
Vanadium Pentoxide in FLAKES 1.0-1.2%
Potassium oxide 3.9-4.1%
Zinc 0.7-0.9%
All the other are water
The full fertilizer of plant is that plant is fertile entirely: Ningnanmycin=1: 5 with the Ningnanmycin compound proportion.
The production technique of Huangningsu biological medicinal fertilizer is:
One, produces plant fertilizer entirely
1, at first peat is carried out air-dry, pulverizing, sieve, make raw material pulverizing reach 40 purpose granularities;
2, lixiviate.Peat is put into the vat liquor lixiviate, the per 20 gram peat of extractive substance and vat liquor ratio, with 100 milliliters of vat liquors, vat liquor adds water by trisodium phosphate hydro-oxidation potassium (or sodium hydroxide) and is mixed and forms, back pH value about 13 is mixed, maintain the temperature between 15-25 ℃, extraction time is chosen at 14-24 hour according to the different material type.The result of lixiviate can obtain the reel chain Sodium salts humic acids;
3, concussion precipitation.Place stirrer to stir vat liquor, make its reciprocation cycle vibrations 5-10 minute, temperature remains between 15-25 ℃, makes vat liquor and extractive substance thorough mixing, puts into settling tank then and carries out 24 hours precipitations;
4, stir acid adjustment.Mixed liquid fully reacting in settling tank is reentered in the stirrer and stirs.Carry out acid adjustment after stirring and handle, make it that decomposition and separation take place, through 12 hours precipitations, can finish approximately;
5, centrifugation.With the mixed solution after the acid adjustment precipitation process, the whizzer of putting into rotating speed and be 4000 rev/mins carries out solid-liquid separation, separates a collection of in 1-5 minute.The isolated liquid of supercentrifuge mainly is the peat xanthohumic acid;
6, the full fertilizer of preparation plant is got in following prescription and ratio: N1.1-1.4%, P 2O 51.0-1.2%, K 2O3.9-4.1%, Zn0.7-0.9% mix each component successively, pour in the peat xanthohumic acid that makes, and pH value 6.8-7.2 is regulated in the group back.The shared weight percent of xanthohumic acid is 1.2-1.4%, and it is fertile entirely promptly to obtain plant;
7, the preparation of Huangningsu biological medicinal fertilizer.Full fertilizer of plant and Ningnanmycin are carried out compound.The ratio of preparation is that plant is fertile entirely: Ningnanmycin=1: 5.Promptly obtain Huangningsu biological medicinal fertilizer after they are stirred.
The present invention is that the less xanthohumic acid of the biological pesticide Ningnanmycin that is generated by the biotechnology fermentation technique and the high reactivity, the molecular weight that are main material production is that the complete fertile compound of plant of main material production cooperates to come with peat.It can improve the crop immunological competence.Strengthen the plant metabolism function, promote thymus nucleic acid in the cell, Yeast Nucleic Acid and proteinic synthesizing, improve the activity of multiple lytic enzyme, promote the soil nutrient composition to decompose favourable crop growth.It can prevent and treat tobacco mosaic disease, can also prevent the Powdery Mildew of vegetables, wheat, melon and fruit, flowers; Secondly, plant is had the activation physiologically active, root of hair encourages, and is disease-resistant drought-enduring, promotes precocity, and anti-flowers and fruits come off, and improve the effect of crop quality.Increase yield significantly, to people and animals, environmental nonpollution, applied widely.Because its basic raw material is peat (producing xanthohumic acid uses), corn, peanut cake, starch, glucose (producing Ningnanmycin uses), cost is low, and raw material is extensive, has high economic benefit.
Be a part of test effect data below
Huangningsu biological medicinal fertilizer prevention effect cartogram
Table 1
Test site The crop title Investigation strain number Sickness rate % Prevention effect Remarks
Shuangyashan City clay fertilizer station Tomato 40 32.5 7.5 Virus disease
Road Outside Area, Harbin City agricultural technique spread station 144 16.0 84.9 Virus disease
Harbin City's Taiping District agricultural technique spread station 15 7 93 Virus disease
Harbin City's Xiangfang District agricultural technique spread station 30 35 27.0 Virus disease
The Daqing agricultural technique spread station 19 81 Virus disease
The rich rural area of Shuangcheng City 10 3.3 83.3 Blight
Harbin City's Nangang District agricultural technique spread station Capsicum 446 12.29 100 Virus disease
Road Outside Area, Harbin City agricultural technique spread station 168 16.6 83.4 Virus disease
Harbin City's Nangang District agricultural technique spread station Fresh kidney beans 30 70 Anthrax
Heilongjiang Province gardening institute 6.2 93.8 Anthrax
Harbin City's Taiping District agricultural technique spread station Cucumber 15 7 93 Oidium
The Daqing agricultural technique spread station 10 90 Oidium
The concentric township of Shuangcheng City Muskmelon 10 3.3 66.6 Powdery Mildew
The concentric township of Shuangcheng City Watermelon 10 3.3 83.8 Powdery Mildew
Kiamusze City's Vegetable Research Institute Chinese cabbage 23.3 7.33 Oidium
Hainan Province stabilizes the county 1.8 72 Oidium
Special product institute of the Chinese Academy of Agricultural Sciences (Jilin Zuo Jia) Radix Panacis Quinquefolii 740 1.6 86.31 Damping-off
740 17.5 35.0 Black spot
740 5.4 71.42 Stem rot
Huangningsu biological medicinal fertilizer test output questionnaire
Table 2
Test site Crop species Per mu yield kilogram/mu Stimulation ratio % Remarks Test site Crop species Per mu yield kilogram/mu Stimulation ratio % Remarks
Harbin City's Nangang District Capsicum 5904 18.0 Test The Power Area of Harbin City Cucumber 7.5 Test
Fresh kidney beans 1627 29.6 Test Harbin City's Taiping District Tomato 5656 12.0 Test
Celery 8662 22.0 Test Cucumber 5772 11.0 Test
The naked oats dish 3500 25.0 Demonstration Harbin City's cottage area Tomato 6507.6 6.6 Test
The Road Inside Area, Harbin City Tomato 6782 32.0 Test The Road Outside Area, Harbin City Tomato 7250 11.9 Test
Romaine lettuce 1791 65.9 Test The Power Area of Harbin City Capsicum 4898 12.6 Test
Cucumber 6222 17.0 Test Harbin City's Xiangfang District Tomato 3558.4 10.2 Test
Fresh kidney beans 3458 12.4 Demonstration Heilongjiang Province's Jixi City Tomato 4920 16.4 Test
Heilongjiang Province Bin County Tobacco 178.3 12.1 Test Heilongjiang Province's Shuangcheng City Muskmelon 3251.1 12.4 Demonstration
Muskmelon 1512.8 17.4 Test Muskmelon 3388.4 17.1 Test
Cucumber 11138. 8 10.6 Demonstration Watermelon 2277.7 13.0 Demonstration
Tomato 12839. 8 15.5 Demonstration Watermelon 2368.9 17.5 Test
Shuangyashan City Tomato 6125 9.3 Test The Kiamusze City Tomato 4989.9 8.8 Test
The Mudanjiang City Romaine lettuce 3953.5 47.1 Test Wild cabbage 3120.8 9.4 Test
Tomato 1914.7 4 13.6 Test The Daqing Tomato 3596.4 11.0 Test
Suihua City Chinese cabbage 7704 9.5 Test Cucumber 6107.0 15.0 Test
Hainan Province stabilizes the county Chinese cabbage 2945.8 5.5 Test Kiamusze City vegetables institute Autumn cabbage 8130.5 10.3 Test
Sponge gourd 3354 3.2 Test Heilongjiang Province gardening institute Fresh kidney beans 1320 20.0 Test
Zhejiang Province's Anji County Tomato 4690.9 1.4 Test The Baiquan County, Heilongjiang Province Soybean 131.6 5.5
Mudanjiang aggie Caraway 26.9 Test Paddy rice
Rape 21.9 Test Corn
Spinach 23.5 Test The Gai Zhou of Liaoning Province Grape
The Xiong Yue of Liaoning Province Apple 9.5 31.9 Test The Bayan County, Heilongjiang Province county Soybean 148.9 10.1 Test
Wafangdian, Liaoning Province Apple 45.0 14.2 Test The Qiqihaer City Tomato Test
Embodiment:
1, get peat, at first to peat carry out air-dry, pulverize, sieve, make raw material pulverizing reach 40 purpose granularities; With the lixiviate in vat liquor of the peat after sieving, vat liquor is that per 44.6 gram trisodium phosphates and 4 gram potassium hydroxide (or sodium hydroxide) are mixed, and adds water to 1 kilogram again, and pH value is reached about 13.The extractive substance liquid proportional is per 20 gram peat, need be with 100 milliliters of vat liquor, and leaching process will maintain the temperature between 15-25 ℃, and extraction time is chosen at 14-24 hour according to the different material type; The result of lixiviate can obtain the reel chain Sodium salts humic acids.Place stirrer to stir vat liquor, make its reciprocation cycle vibrations 5-10 minute, temperature remains between 15-25 ℃, make vat liquor and extractive substance thorough mixing, put into settling tank then and carry out 24 hours precipitations, the mixed solution that in settling tank, fully reacted, be reentered in the stirrer and stir.Strengthen acid (sulfuric acid, hydrochloric acid, nitric acid etc. all can) acid adjustment after stirring and handle, make it that decomposition and separation take place, through 12 hours precipitations, can finish approximately; With the mixed solution after the acid adjustment precipitation process, the whizzer of putting into rotating speed and be 4000 rev/mins carries out solid-liquid separation, separates a collection of in 1-5 minute.The isolated liquid of supercentrifuge mainly is xanthohumic acid;
Nitrogen, Vanadium Pentoxide in FLAKES, potassium oxide, zinc are joined successively in the xanthohumic acid of above-mentioned preparation, the proportioning of each component (weight percent) is xanthohumic acid 1.3%, nitrogen 1.2%, Vanadium Pentoxide in FLAKES 1.1%, potassium oxide 4.0%, zinc 0.8%, water 91.6%.The pH value of the complete fertile solution of plant that preparation obtains is 6.8-7.2.
The complete fertile 33 milliliters of Ningnanmycins with 167 milliliter of 2% concentration of plant that prepare are mixed, stir, just can obtain 200 milliliters of liquid Huangningsu biological medicinal fertilizers, its total effective ingredient is 3%.

Claims (2)

1, a kind of Huangningsu biological medicinal fertilizer is characterized in that it is to be formed with Ningnanmycin is composite by the full fertilizer of plant, and the full fertilizer of plant comprises peat xanthohumic acid, nitrogen, Vanadium Pentoxide in FLAKES, potassium oxide, zinc and water.Their weight percent is:
Peat xanthohumic acid 1.2-1.4%
Nitrogen 1.1-1.4%
Vanadium Pentoxide in FLAKES 1.0-1.2%
Potassium oxide 3.9-4.1%
Zinc 0.7-0.9%
All the other are water
The complete fertile composite weight ratio with Ningnanmycin of plant is 1: 5.
2, a kind of production technique of Huangningsu biological medicinal fertilizer, it is finished successively according to the following steps:
(1) peat is carried out air-dry, pulverizing, sieve, make raw material pulverizing reach 40 purpose granularities;
(2) lixiviate in vat liquor, extractive substance liquid proportional are per 20 gram peat, need be with 100 milliliters of vat liquors, vat liquor is that trisodium phosphate hydro-oxidation potassium (or sodium hydroxide) adds water again and is mixed, the pH value about 13 of solution after being mixed, extraction temperature remains between 15-25 ℃, extraction time 14-24 hour;
(3) place stirrer to stir vat liquor, make its reciprocation cycle vibrations 5-10 minute, temperature makes vat liquor and extractive substance thorough mixing between keeping 15-25 ℃, puts into settling tank then and carries out 24 hours precipitations;
(4), be reentered in the stirrer and stir the mixed solution that in settling tank, fully reacted.Carry out acid adjustment after stirring and handle, make it that decomposition and separation take place, through 12 hours precipitations, can finish approximately;
(5) with the mixed solution after the acid adjustment precipitation process, the whizzer of putting into rotating speed and be 4000 rev/mins carries out solid-liquid separation, separates a collection ofly in 1-5 minute, and the isolated liquid of supercentrifuge mainly is the peat xanthohumic acid;
(6) by prescription (weight percent): xanthohumic acid 1.2-1.4%, nitrogen 1.1-1.4%, Vanadium Pentoxide in FLAKES 1.0-1.2%, potassium oxide 3.9-4.1%, zinc 0.7-0.9%, above-mentioned each component is added water mix successively, the solution pH value that makes preparation is 6.8-7.2;
(7) full fertilizer of the above-mentioned plant that obtains and Ningnanmycin are carried out the compound preparation, the ratio of preparation is 1: 5, can obtain Huangningsu biological medicinal fertilizer.
CN99122544A 1999-11-16 1999-11-16 Huangningsu biological medicinal fertilizer and productive technology thereof Expired - Fee Related CN1124245C (en)

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* Cited by examiner, † Cited by third party
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KR101034047B1 (en) * 2008-11-20 2011-05-11 조권호 Method to manufacture plant growth regulator using peat moss
CN104671965A (en) * 2013-12-03 2015-06-03 东港市丰穗肥业有限公司 Nutritional soil for raising seedlings of sweet melons in greenhouse and application of nutritional soil
CN105152774A (en) * 2015-09-01 2015-12-16 安徽省安庆市金太阳生物科技有限责任公司 Novel paddy rice reviving tillering granular fertilizer and preparation method thereof
CN105272694A (en) * 2015-10-08 2016-01-27 定远县蒋集镇丰润蔬菜种植专业合作社 Leek fertilizer prepared from modified peat and preparation method thereof
CN105237191A (en) * 2015-10-08 2016-01-13 定远县蒋集镇丰润蔬菜种植专业合作社 Environment-friendly fertilizer for potato planting and preparation method thereof
CN105237299A (en) * 2015-10-08 2016-01-13 定远县蒋集镇丰润蔬菜种植专业合作社 Green and environment-friendly paddy rice nitrogen fertilizer and preparation method thereof
CN105237190A (en) * 2015-10-08 2016-01-13 定远县蒋集镇丰润蔬菜种植专业合作社 Insect pest resistant sustain-released fertilizer for peanut planting and preparation method thereof
CN105237196A (en) * 2015-10-08 2016-01-13 定远县蒋集镇丰润蔬菜种植专业合作社 Cucumber fertilizer prepared from modified peat and preparation method thereof

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