CN104041532B - A kind of efficient sterilizing increases production suspending agent and production method thereof and application - Google Patents
A kind of efficient sterilizing increases production suspending agent and production method thereof and application Download PDFInfo
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Abstract
A kind of efficient sterilizing volume increase suspending agent, in this efficient sterilizing volume increase suspending agent raw material, the weight portion of bulk drug is: rhizome of cyrtomium 4.0～6.0 parts, giant knotweed 3.0～5.0 parts, folium isatidis 2.0～4.0 parts, kuh-seng 2.0～4.0 parts, schizonepeta 3.0～5.0 parts, copper 1.0～3.0 parts, zinc 2.0～4.0 parts, boron 1.0～3.0 parts, magnesium 3.0～5.0 parts, manganese 2.0～4.0 parts, potassium 1.0～3.0 parts.Its advantage is: the efficient sterilizing volume increase suspending agent made by 1), use botanical material be main, chemical agent be auxiliary, Environmental compatibility is good, nontoxic, harmless, pollution-free, noresidue, high to person poultry safety's property, diseases prevention, volume increase effect can be kept lasting, the autoimmunity of crops can be improved simultaneously, crops are played good sterilization, antiviral, diseases prevention, cure the disease, the effect of high volume increase；2) low cost.
Description
Technical field
The present invention relates to a kind of bactericidal yield-increase agent and production method thereof and application, particularly a kind of efficient sterilizing volume increase suspending agent and production method thereof and application.
Background technology
At present, along with people's environmental consciousness and awareness of safety constantly strengthen, food security is more paid attention to by people, and green crop products pollution-free, non agricultural chemical residuum is favored by people, but the agricultural chemicals of current preventing and treating corps diseases is mostly chemical synthesis, toxicity is high, easily remain in ecological environment and on crops, both destroyed ecological environment, and again the food of people and animals had been caused pollution, will the health of serious threat people and animals, and there is no the effect of high volume increase yet.It is more than the deficiencies in the prior art.
Summary of the invention
It is an object of the invention to: a kind of efficient sterilizing volume increase suspending agent and production method thereof and application are provided, made efficient sterilizing volume increase suspending agent Environmental compatibility is good, nontoxic, harmless, pollution-free, noresidue, high to person poultry safety's property, diseases prevention, volume increase effect can be kept lasting, the immunity of crops can be improved simultaneously, crops are played diseases prevention, cure the disease, the effect of high volume increase.
The purpose of the present invention can be realized by following technical proposals:
A kind of efficient sterilizing volume increase suspending agent, it is characterised in that in its raw material, the weight portion of bulk drug is: rhizome of cyrtomium 4.0～6.0 parts, giant knotweed 3.0～5.0 parts, folium isatidis 2.0～4.0 parts, kuh-seng 2.0～4.0 parts, schizonepeta 3.0～5.0 parts, copper 1.0～3.0 parts, zinc 2.0～4.0 parts, boron 1.0～3.0 parts, magnesium 3.0～5.0 parts, manganese 2.0～4.0 parts, potassium 1.0～3.0 parts.
In its raw material of the present invention, the weight portion of bulk drug is: rhizome of cyrtomium 4.0 parts, giant knotweed 3.0 parts, folium isatidis 2.0 parts, kuh-seng 2.0 parts, schizonepeta 3.0 parts, copper 1.0 parts, 2.0 parts of zinc, boron 1.0 parts, 3.0 parts of magnesium, 2.0 parts of manganese, 1.0 parts of potassium.
In its raw material of the present invention, the weight portion of bulk drug is: rhizome of cyrtomium 5.25 parts, giant knotweed 4.20 parts, folium isatidis 3.60 parts, kuh-seng 2.80 parts, schizonepeta 3.40 parts, copper 1.2 parts, 1.70 parts of zinc, boron 1.5 parts, 3.80 parts of magnesium, 2.20 parts of manganese, 2.60 parts of potassium.
In its raw material of the present invention, the weight portion of bulk drug is: rhizome of cyrtomium 6.0 parts, giant knotweed 5.0 parts, folium isatidis 4.0 parts, kuh-seng 4.0 parts, schizonepeta 5.0 parts, copper 3.0 parts, 4.0 parts of zinc, boron 3.0 parts, 5.0 parts of magnesium, 4.0 parts of manganese, 3.0 parts of potassium.
Possibly together with the antifreezing agent ethanol of 3% percentage by weight, the thickener xanthans of 0.3% percentage by weight, the wetting dispersing agent alkylnaphthalene hydrochlorate of 5% percentage by weight, the defoamer n-octyl alcohol of 0.1% percentage by weight, the preservative acetaldehyde solution of 0.2% percentage by weight, the PH conditioning agent acetic acid of 0.1% percentage by weight in its raw material of the present invention；The concentration expressed in percentage by volume of described antifreezing agent ethanol is 99%, and the concentration expressed in percentage by volume of described defoamer n-octyl alcohol is 99%, and the mass percentage concentration of described preservative acetaldehyde solution is 40%, and the mass percentage concentration of described PH conditioning agent acetic acid is 99%.
The production method of a kind of efficient sterilizing volume increase suspending agent, it is characterised in that comprise the following steps that:
(1) the antifreezing agent ethanol of bulk drug and 3% percentage by weight is taken according to above-mentioned weight portion, the thickener xanthans of 0.3% percentage by weight, the wetting dispersing agent alkylnaphthalene hydrochlorate of 5% percentage by weight, the defoamer n-octyl alcohol of 0.1% percentage by weight, the preservative acetaldehyde solution of 0.2% percentage by weight, the PH conditioning agent acetic acid of 0.1% percentage by weight, and water, load in the reactor of band high-shear impeller, and make the content of the water in loading reactor reach the 58.5% of efficient sterilizing to be produced volume increase suspending agent product weight, stirring is pulverized, mixing, until during mixture uniformly viscous fluid, stop stirring；
(2) material pulverized through step (1) stirring being passed through sand mill, then logical cooling water carries out sand milling ultramicro grinding, and < 3um i.e. obtains efficient sterilizing volume increase suspending agent to be crushed to material terminal particle diameter；
(3) detection: in the efficient sterilizing volume increase suspending agent obtained from step (2), extraction sample, at normal temperatures with the detection sample particle diameter distribution of Malvern laser fineness gage, and by sample particle diameter distribution calculate sample normal temperature suspensibility be 96.3%, sample is store 14 days through TC cooling 7 days, 54 DEG C of heat, sample is without the knot end, and syneresis rate is 0.5%.
A kind of application of efficient sterilizing volume increase suspending agent, it is characterised in that: for preventing and treating the following disease of wheat, corn, paddy rice, cotton, peanut, fresh kidney beans, capsicum, watermelon, grape crops: charcoal subcutaneous ulcer, scab, epidemic disease, target spot, downy mildew；Further, for preventing and treating the virosis of solanaceous crops.
The invention have the advantage that 1) made by efficient sterilizing volume increase suspending agent, use botanical material be main, chemical agent be auxiliary, Environmental compatibility is good, nontoxic, harmless, pollution-free, noresidue, high to person poultry safety's property, diseases prevention, volume increase effect can be kept lasting, the autoimmunity of crops can be improved simultaneously, crops are played good sterilization, antiviral, diseases prevention, cure the disease, the effect of high volume increase；2) low cost.
Detailed description of the invention
Efficient sterilizing of the present invention volume increase suspending agent, in its raw material, the weight portion of bulk drug is: rhizome of cyrtomium 4.0～6.0 parts, giant knotweed 3.0～5.0 parts, folium isatidis 2.0～4.0 parts, kuh-seng 2.0～4.0 parts, schizonepeta 3.0～5.0 parts, copper 1.0～3.0 parts, zinc 2.0～4.0 parts, boron 1.0～3.0 parts, magnesium 3.0～5.0 parts, manganese 2.0～4.0 parts, potassium 1.0～3.0 parts.Possibly together with the antifreezing agent ethanol of 3% percentage by weight, the thickener xanthans of 0.3% percentage by weight, the wetting dispersing agent alkylnaphthalene hydrochlorate of 5% percentage by weight, the defoamer n-octyl alcohol of 0.1% percentage by weight, the preservative acetaldehyde solution of 0.2% percentage by weight, the PH conditioning agent acetic acid of 0.1% percentage by weight in its raw material；The concentration expressed in percentage by volume of described antifreezing agent ethanol is 99%, and the concentration expressed in percentage by volume of described defoamer n-octyl alcohol is 99%, and the mass percentage concentration of described preservative acetaldehyde solution is 40%, and the mass percentage concentration of described PH conditioning agent acetic acid is 99%.
The production method of efficient sterilizing of the present invention volume increase suspending agent, comprises the following steps that:
(1) the antifreezing agent ethanol of bulk drug and 3% percentage by weight is taken according to above-mentioned weight portion, the thickener xanthans of 0.3% percentage by weight, the wetting dispersing agent alkylnaphthalene hydrochlorate of 5% percentage by weight, the defoamer n-octyl alcohol of 0.1% percentage by weight, the preservative acetaldehyde solution of 0.2% percentage by weight, the PH conditioning agent acetic acid of 0.1% percentage by weight, and water, load in the reactor of band high-shear impeller, and make the content of the water in loading reactor reach the 58.5% of efficient sterilizing to be produced volume increase suspending agent product weight, stirring is pulverized, mixing, until during mixture uniformly viscous fluid, stop stirring；
(2) material pulverized through step (1) stirring being passed through sand mill, then logical cooling water carries out sand milling ultramicro grinding, and < 3um i.e. obtains efficient sterilizing volume increase suspending agent to be crushed to material terminal particle diameter；
(3) detection: in the efficient sterilizing volume increase suspending agent obtained from step (2), extraction sample, at normal temperatures with the detection sample particle diameter distribution of Malvern laser fineness gage, and by sample particle diameter distribution calculate sample normal temperature suspensibility be 96.3%, sample is store 14 days through TC cooling 7 days, 54 DEG C of heat, sample is without the knot end, and syneresis rate is 0.5%.
In the of the present invention efficient sterilizing volume increase suspending agent raw material several embodiments of raw material medicines in portions by weight are presented herein below:
Embodiment 1:
In its raw material, the weight portion of bulk drug is: rhizome of cyrtomium 4.0 parts, giant knotweed 3.0 parts, folium isatidis 2.0 parts, kuh-seng 2.0 parts, schizonepeta 3.0 parts, copper 1.0 parts, 2.0 parts of zinc, boron 1.0 parts, 3.0 parts of magnesium, 2.0 parts of manganese, 1.0 parts of potassium.
Embodiment 2:
In its raw material, the weight portion of bulk drug is: rhizome of cyrtomium 5.25 parts, giant knotweed 4.20 parts, folium isatidis 3.60 parts, kuh-seng 2.80 parts, schizonepeta 3.40 parts, copper 1.2 parts, 1.70 parts of zinc, boron 1.5 parts, 3.80 parts of magnesium, 2.20 parts of manganese, 2.60 parts of potassium.
Embodiment 3:
In its raw material, the weight portion of bulk drug is: rhizome of cyrtomium 6.0 parts, giant knotweed 5.0 parts, folium isatidis 4.0 parts, kuh-seng 4.0 parts, schizonepeta 5.0 parts, copper 3.0 parts, 4.0 parts of zinc, boron 3.0 parts, 5.0 parts of magnesium, 4.0 parts of manganese, 3.0 parts of potassium.
Efficient sterilizing of the present invention volume increase suspending agent can be used for effectively preventing and treating contingent more than 85% fungal diseases of crops such as wheat, corn, paddy rice, cotton, peanut, fresh kidney beans, capsicum, watermelon, grape, as, charcoal subcutaneous ulcer, scab, epidemic disease, target spot, downy mildew etc..It addition, efficient sterilizing of the present invention volume increase suspending agent can be additionally used in the virosis effectively preventing and treating the solanaceous crops such as tobacco, tomato, capsicum.There is sterilization, expelling parasite, antiviral, supplement crops desired nutritional material, improve crops autoimmunity, diseases prevention, cure the disease, promote crops reproductive growth, make effect of crops height volume increase.Nontoxic, harmless, person poultry safety.
The application process of efficient sterilizing of the present invention volume increase suspending agent is: general when crops length to 60～70 centimeter, or uses before florescence, and during use, every 25～30 milliliters of bactericidal yield-increase suspending agents are watered 30 jin, even spraying.
The proterties of efficient sterilizing of the present invention volume increase suspending agent is pasty state, and pH value is 5～6.It is sterilized, drives after being ill, and high effect of increasing production is extremely notable, respond well to the virus disease control of solanaceous crops, can be verified by following field test.
(1) efficient sterilizing of the present invention volume increase suspending agent application effect test on cotton
One, test field and trial crops situation:
Test site launches demonstration test in so-and-so field of Xinjiang Pu Huixiang tri-group king.In test field, (spraying the field of efficient sterilizing of the present invention volume increase suspending agent) with choosing demonstration is 20 mu, and comparatively (field of local peasant household Routine Management) is 8 mu.Test field soil is loam ground.This test, test field plant cotton, kind is rich No. 8 of peace.
Two, testing program and method:
This test time is 2013.Field management and process of the test be: test field (with including demonstration and comparatively), all use pressurization drip irrigation technique, superior sowing cultivation technique, stubble-cleaning winter irrigation after autumn, the spring turns over basal dressing phosphoric acid diamines 40 kgs/acre, potassium sulfate 26 kgs/acre, 10 kgs/acre of urea；After spring turns over fertilising, on April 3rd, 2013, April 5 was sowed, and a film sows 4 row wholely, and theory goes out strain number 12700～13000 plants/acre, actual cut strain number 10800～11690 plants/acre, investigation fixed point strain number 10800 plants/acre.April 15 seeding stage～April 20, intertill 2 times, change control 2 times, May 25 buddingged, and June 23 bloomed, and July 3～7 days pinch, August 20 blow-of-cottons.Daily use chemicals control in June 18, every mu with mepiquat chloride 1.5 grams；Daily use chemicals control in July 18, every mu with mepiquat chloride 7 grams.Filled water for the first time on June 16；Filled second time water on June 23, and mu executes 5 kilograms of urea；Filled third time water on July 4, and mu executes 8 kilograms of urea, boron fertilizer 1 kg/acre, 2 kgs/acre of zinc sulfate；July 12 filled the 4th water, and mu executes 10 kilograms of urea；July 18 filled the 5th water, and mu executes 10 kilograms of urea；July 25 filled the 6th water, and mu executes 11 kilograms of urea；August 2 filled the 7th water, and mu executes 10 kilograms of urea；August 10 filled the 8th water, and mu executes 8 kilograms of urea；August 16 filled the 9th water, and mu executes 8 kilograms of urea；August 21 filled the tenth water.Respectively at June 18, June 27, July 9, using efficient sterilizing of the present invention in three times demonstration ground and increase production suspending agent, be all that every 25～30 milliliters of bactericidal yield-increase suspending agents are watered 30 jin every time when using, even spraying, every mu with bactericidal yield-increase suspending agent 40 milliliters；The most do not use efficient sterilizing of the present invention volume increase suspending agent.The guarantor investigating cotton after July 12 and 12 days at twice spends, protects bell effect.Peach situation before investigation on July 16 volt.August 16 investigated bell weight with September 6.Detection on August 26 yield.
Three, result of the test:
Result of the test is shown in Table 1, table 2, table 3 and table 4.
Table 1. is spent in protecting of investigation on July 12 cotton, the situation of guarantor's bell effect
Table 2. is peach situation before investigation on July 16 volt
Table 3. is in the situation of August 16 and September 6 days investigation bell weight
Table 4. detected output condition August 26
From in table 1, efficient sterilizing of the present invention volume increase suspending agent is obvious to the root system effect of cotton, can accelerate cotton plant and be produced conversion by nourishing and growing to reproduction, it is achieved early buddings, prematurity, early pinch, and protects flower, to protect bell effective, increases caping peach effect especially prominent.From in table 2, investigation to Fu Qiantao, after demonstration ground cotton sprays efficient sterilizing of the present invention volume increase suspending agent, demonstration ground cotton cane rugosity is than the comparatively many 0.05cm of cotton cane rugosity, the most 0.96 of the single-strain bell-forming ratio in demonstration ground, the most 1.46 of the individual plant children's bell ratio in demonstration ground.From in table 3, after demonstration ground cotton sprays efficient sterilizing of the present invention volume increase suspending agent, demonstration ground is compared with comparatively, the thick many 0.087cm of cane, many 0.91 of single-strain bell-forming, individual plant comes off few 1.4, tie 9828, bell, the many 0.32g of Single boll weight, every mu of volume increase unginned cotton 86.2kg for every mu more.From in table 4, spraying the demonstration ground of efficient sterilizing of the present invention volume increase suspending agent, compared with comparatively, many 2.2 of cotton boll per plant quantity, Single boll weight reduces 0.4g, and detects yield every mu and increased production 92.16kg.Visible, after spraying efficient sterilizing of the present invention volume increase suspending agent, effect of increasing production is the most notable.
(2) prevention effect of tomato, capsicum, tobacco solanaceous crops virosis is tested by efficient sterilizing of the present invention volume increase suspending agent
This test time is 2011.Test site is in Yunnan Province's Kaiyuan City, Jianshui County, and the local height above sea level 1420 meters of test, long-term rainfall about 880mm, experimental field block length phase plantation solanaceous crops, cultivation management condition is preferable, and solanaceous crops virosis occurs seriously over the years.The generation of solanaceous crops virosis had been shown in this test the most already.During test, after solanaceous crops transplants into 7 days, first meeting virosis begins with spray-on process and carries out dispenser (spraying efficient sterilizing of the present invention volume increase suspending agent) when occurring, dispenser 3 times altogether, tomato spraying time is on June 24th, 2011, July 1, July 8；Capsicum spraying time is on June 25th, 2011, July 2, July 9；Tobacco spraying time is on June 26th, 2011, July 3, July 10；Dispenser dosage is, 40 milliliters every mu, dilutes 750～1000 times of uses, the amount of spraying with plant fully medicine and do not drip and be advisable；The preventing and treating of other disease is not carried out during test.Observe during test and draw, efficient sterilizing of the present invention volume increase suspending agent does not produce poisoning phenomenon to crop, not affecting quality and the yield of crop, being not only other pest and disease damage to solanaceous crops virosis, to crop generation also has obvious prevention effect, on non-target organism without impact.After dispenser 3 times 10 days as stated above, detection sprayed the effect after efficient sterilizing of the present invention volume increase suspending agent, show that the average prevention effect to tomato virus disease is 83.54%～94.51%；Average prevention effect to tobacco virus is 82.44%～91.89%；Average prevention effect to pepper virus disease is 80.24%～92.34%.Visible, efficient sterilizing of the present invention volume increase suspending agent has good prevention effect to three kinds of solanaceous crops virosis.
Claims (7)
1. an efficient sterilizing volume increase suspending agent, it is characterised in that in its raw material, the weight portion of bulk drug is: rhizome of cyrtomium 4.0～6.0 parts, giant knotweed 3.0～5.0 parts, folium isatidis 2.0～4.0 parts, kuh-seng 2.0～4.0 parts, schizonepeta 3.0～5.0 parts, copper 1.0～3.0 parts, zinc 2.0～4.0 parts, boron 1.0～3.0 parts, magnesium 3.0～5.0 parts, manganese 2.0～4.0 parts, potassium 1.0～3.0 parts.
A kind of efficient sterilizing volume increase suspending agent the most according to claim 1, it is characterised in that in its raw material, the weight portion of bulk drug is: rhizome of cyrtomium 4.0 parts, giant knotweed 3.0 parts, folium isatidis 2.0 parts, kuh-seng 2.0 parts, schizonepeta 3.0 parts, copper 1.0 parts, 2.0 parts of zinc, boron 1.0 parts, 3.0 parts of magnesium, 2.0 parts of manganese, 1.0 parts of potassium.
A kind of efficient sterilizing volume increase suspending agent the most according to claim 1, it is characterised in that in its raw material, the weight portion of bulk drug is: rhizome of cyrtomium 5.25 parts, giant knotweed 4.20 parts, folium isatidis 3.60 parts, kuh-seng 2.80 parts, schizonepeta 3.40 parts, copper 1.2 parts, 1.70 parts of zinc, boron 1.5 parts, 3.80 parts of magnesium, 2.20 parts of manganese, 2.60 parts of potassium.
A kind of efficient sterilizing volume increase suspending agent the most according to claim 1, it is characterised in that in its raw material, the weight portion of bulk drug is: rhizome of cyrtomium 6.0 parts, giant knotweed 5.0 parts, folium isatidis 4.0 parts, kuh-seng 4.0 parts, schizonepeta 5.0 parts, copper 3.0 parts, 4.0 parts of zinc, boron 3.0 parts, 5.0 parts of magnesium, 4.0 parts of manganese, 3.0 parts of potassium.
5. increase production suspending agent according to a kind of efficient sterilizing described in claim 1-4 any one, it is characterised in that: possibly together with the antifreezing agent ethanol of 3% percentage by weight, the thickener xanthans of 0.3% percentage by weight, the wetting dispersing agent alkylnaphthalene hydrochlorate of 5% percentage by weight, the defoamer n-octyl alcohol of 0.1% percentage by weight, the preservative acetaldehyde solution of 0.2% percentage by weight, the PH conditioning agent acetic acid of 0.1% percentage by weight in its raw material；The concentration expressed in percentage by volume of described antifreezing agent ethanol is 99%, and the concentration expressed in percentage by volume of described defoamer n-octyl alcohol is 99%, and the mass percentage concentration of described preservative acetaldehyde solution is 40%, and the mass percentage concentration of described PH conditioning agent acetic acid is 99%.
6. the production method of a kind of efficient sterilizing volume increase suspending agent as described in claim 1-4 any one, it is characterised in that comprise the following steps that:
(1) the antifreezing agent ethanol of bulk drug and 3% percentage by weight is taken according to above-mentioned weight portion, the thickener xanthans of 0.3% percentage by weight, the wetting dispersing agent alkylnaphthalene hydrochlorate of 5% percentage by weight, the defoamer n-octyl alcohol of 0.1% percentage by weight, the preservative acetaldehyde solution of 0.2% percentage by weight, the PH conditioning agent acetic acid of 0.1% percentage by weight, and water, load in the reactor of band high-shear impeller, and make the content of the water in loading reactor reach the 58.5% of efficient sterilizing to be produced volume increase suspending agent product weight, stirring is pulverized, mixing, until during mixture uniformly viscous fluid, stop stirring；
(2) material pulverized through step (1) stirring being passed through sand mill, then logical cooling water carries out sand milling ultramicro grinding, and < 3um i.e. obtains efficient sterilizing volume increase suspending agent to be crushed to material terminal particle diameter；
(3) detection: in the efficient sterilizing volume increase suspending agent obtained from step (2), extraction sample, at normal temperatures with the detection sample particle diameter distribution of Malvern laser fineness gage, and by sample particle diameter distribution calculate sample normal temperature suspensibility be 96.3%, sample is store 14 days through TC cooling 7 days, 54 DEG C of heat, sample is without the knot end, and syneresis rate is 0.5%.
7. the application of a kind of efficient sterilizing volume increase suspending agent as described in claim 1-4 any one, it is characterised in that: for preventing and treating the following disease of wheat, corn, paddy rice, cotton, peanut, fresh kidney beans, capsicum, watermelon, grape crops: charcoal subcutaneous ulcer, scab, epidemic disease, target spot, downy mildew；Further, for preventing and treating the virosis of solanaceous crops.
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| CN105875640A (en) * | 2016-05-14 | 2016-08-24 | 广东中迅农科股份有限公司 | Suspending agent containing trace element and preparation method thereof |
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| JP3639456B2 (en) * | 1999-04-28 | 2005-04-20 | 池田食研株式会社 | Plant growth promoter and fertilizer using the plant growth promoter |
| CN1623402A (en) * | 2004-10-21 | 2005-06-08 | 刘起麟 | Preparation of antifalse pesticide and its use method |
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| CN1082817A (en) * | 1993-08-25 | 1994-03-02 | 薛永宏 | Chinese herbal medicine insecticide and leach extraction method thereof |
| CN1129065A (en) * | 1995-02-16 | 1996-08-21 | 韩允志 | Preparation method for synergistic compound urea mixture made from traditional Chinese herbs |
| JP3639456B2 (en) * | 1999-04-28 | 2005-04-20 | 池田食研株式会社 | Plant growth promoter and fertilizer using the plant growth promoter |
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| CN1623402A (en) * | 2004-10-21 | 2005-06-08 | 刘起麟 | Preparation of antifalse pesticide and its use method |
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