CN1896034A - Composite mixed foliage fertilizer and its preparation - Google Patents

Composite mixed foliage fertilizer and its preparation Download PDF

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Publication number
CN1896034A
CN1896034A CN 200610010017 CN200610010017A CN1896034A CN 1896034 A CN1896034 A CN 1896034A CN 200610010017 CN200610010017 CN 200610010017 CN 200610010017 A CN200610010017 A CN 200610010017A CN 1896034 A CN1896034 A CN 1896034A
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Prior art keywords
fertilizer
agent
composite mixed
accounts
water
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CN 200610010017
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高树林
张惠春
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HEILONGJIANG QIDA PESTICIDE DEVELOPMENT Co Ltd
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HEILONGJIANG QIDA PESTICIDE DEVELOPMENT Co Ltd
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Priority to CN 200610010017 priority Critical patent/CN1896034A/en
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Abstract

A composite mixed foliage fertilizer and its production are disclosed. The fertilizer consists of amino-acid dry powder, iron, zinc, fast-effective nitrogen, phosphor and potassium fertilizer, plant growth regulator sodium nitrate, leaf wetting agent, adsorbent, penetrating agent and synergistic agent. It has better fertilizer effect, solubility and biological activity and more product yield.

Description

A kind of composite mixed foliage fertilizer and preparation method thereof
Technical field
The present invention relates to a kind of composite mixed foliage fertilizer of foliage-spray.
Background technology
At present foliage fertilizer exist easily be fixed, leaching, utilization ratio be low, causes defectives such as soil compaction.And common amino acids foliage fertilizer, mostly be hydrolysis amino acid, its main raw material is that trace elements such as amino acid and iron, zinc, copper are formed, and the trace element majority is a free state, and its biologos is relatively poor, and amino acid and trace element are low because of the crop leaf absorption rate in this series products, effective ingredient is single, lacks the essential nitrogen of plant, phosphorus, potassium three big element and competent trace elements, can not bring into play its effect better, so effect of increasing production is not obvious, the value of having wasted raw material.
Summary of the invention
The object of the present invention is to provide and a kind ofly can satisfy the balanced nutritious needs of plant, improve utilization rate of fertilizer, improve composite mixed foliage fertilizer of crop yield and preparation method thereof.
Composite mixed foliage fertilizer of the present invention selects for use trace elements such as biochemical agricultural amino acid dry powder and iron, zinc to be main raw material and quick-acting nitrogen, phosphorus, potash fertilizer, and the plant-growth regulator sodium nitrophenolate, add distinctive blade face wetting agent, sorbent material, permeate agent and synergistic agent is composite forms.
Its effective ingredient weight ratio of a kind of composite mixed foliage fertilizer of the present invention is:
Amino acid accounts for 5-15%, and nitrogenous fertilizer (N) accounts for 5-30%, phosphate fertilizer (P 2O 5) account for 2-15%, potash fertilizer (K 2O) account for 1-6%, trace element accounts for 1-5%, and sodium nitrophenolate accounts for 0.1-2%, and wetting agent NNO accounts for 0.1-1%, and permeate agent accounts for 0.1-0.7%, and surplus is a water.
The sorbent material TP (also being spreader-sticker) that can add 0.1-1% in the described composite mixed foliage fertilizer of the present invention, the synergistic agent syn of 0.1-0.8% (also crying the agent of pulling together).
Described trace element comprises zinc, iron, copper, molybdenum.Described wetting agent NNO chemical constitution: naphthalene sulfonic acidformaldehyde condensation product, described permeate agent is a Nekal BX, chemical constitution: sodium butylnaphthalenesulfonate.(wetting agent, permeate agent and sorbent material are that the intercalation native Group Co.,Ltd in Zhejiang produces, and synergistic agent is produced by farming chemical plant, Jianyang City, Sichuan.)
Its preparation method: raw material amino acid, nitrogenous fertilizer, phosphate fertilizer, potash fertilizer and trace element pulverizing are dissolved it with a small amount of solvent water; With less water sodium nitrophenolate is dissolved in addition, after the two mixes, add suitable quantity of water dissolved blade face wetting agent, sorbent material, permeate agent and synergistic agent, after mixing, stir with the excess water dilution, pH value is 2-6, promptly makes.
The invention has the advantages that:
1, main raw material of the present invention is the complete water-soluble biochemical amino acid powder and the concentrated solution of trace elements such as iron, zinc, and because of its good water solubility, the biological activity height is so fertilizer efficiency can be fully played.
2, the present invention adds proportioning scientific and reasonable quick-acting nitrogen, phosphorus, potassium, can in time supply the needs of plant-growth to a large amount of essential elements apace, promotes the absorption of plant to little fertilizer, realizes that plant obtains the demand of equilibrium, full nutrition.
3, the present invention contains the plant-growth regulator sodium nitrophenolate, and it is a kind of powerful cell-activating agent, with can rapid permeability after the plant contact in plant materials, promote the protoplasma of cell to flow, improve fine work power.Can accelerate rooting rate, breaking dormancy promotes to grow, and prevents fallen flowers fruits, improves product quality, improves crop yield, improves the anti-poisoning of crop, disease-resistant, pest-resistant, drought resisting, waterlogging-resistant, cold-resistant, anti-resistance ability such as saline and alkaline, resistant to lodging.
4, the present invention also adds auxiliary agent wetting agent, permeate agent, sorbent material and synergistic agent, and effective ingredient is fully absorbed by crop leaf, and strengthens fertilizer efficiency.The blade face wetting agent can reduce the surface tension of water, makes it to be easy to moistening arranging exhibits on plant surface, improves fertilizer efficiency; Sorbent material can make foliage fertilizer see through the protective membrane of plant surface, and nutritive ingredient is conducted to plant, and damaged blade is had repairing effect, can stimulate leaf regeneration, and has the disease of inhibition to take place; Synergistic agent can play solublization, has reduced product and has produced the crystalline possibility, thereby protected and increase the composite reactive of each effective ingredient, brings into play each nutrition to greatest extent and is realized effect of increasing production by plant absorbing.
Embodiment
Preferred amino acid 10%, nitrogenous fertilizer 15%, phosphate fertilizer 5%, potash fertilizer 3%, trace element 2.5%, sodium nitrophenolate 0.4%, wetting agent 0.2%, permeate agent 0.5%, sorbent material 0.15%, synergistic agent 0.5%, surplus is a water.Trace element comprises zinc, iron, copper, molybdenum, and weight ratio is 1%, 0.8%, 0.3%, 0.4%.With raw material pulverizing 200 orders that sieve, with a small amount of solvent water it is dissolved then; With less water sodium nitrophenolate is dissolved in addition, after the two mixes, add suitable quantity of water dissolved blade face wetting agent, sorbent material, permeate agent and synergistic agent, after mixing,, stirred 10-15 minute with the excess water dilution, pH value is 3, through can after the assay was approved, packing.The present invention is applicable to the food crop based on soybean, all kinds of vegetable crop and cash crop.The present invention's 500 grams are converted water 300-400 kilogram, spray 15 mu of ground.
Composite mixed foliage fertilizer of the present invention two places field test:
One, test objective
In order to verify the effect of increasing production of volume increase composite mixed foliage fertilizer on soybean crops of Heilongjiang Qida Pesticide Development Co., Ltd.'s development and production, for the big area popularization provides foundation.Company in 2005 entrusts that Heilongjiang Province's clay fertilizer stands in Hailun City, agricultural technology extension department in Hailin City has carried out this test.Now test-results is gathered as follows.
Two, test materials and method
1, test materials: the efficient composite mixed foliage fertilizer of Heilongjiang Qida Pesticide Development Co., Ltd.'s development and production.
2, for studying thing: soybean
3, test design and method
Three processing of test design, randomized blocks is adopted in three repetitions.Each sub-district specification is 6 row districts, long 10 meters of row, and each sub-district area is 40m2.
Handle 1: spray efficient composite mixed foliage fertilizer on the conventional fertilizer application basis, per hectare is converted 300 kilograms in water with 500 grams, sprays once at the soybean initial bloom stage, sprays once every 7 days again.
Handle 2: conventional fertilizer application sprays the equivalent clear water 1 same period with handling.
Handle 3: conventional fertilizer application, blank.
Conventional fertilizer application, promptly 10 kilograms/mu+vitriolate of tartar of 2 kilograms/mu+diammonium phosphate of urea is 3 kilograms/mu
Three, basic condition experimental field
1, the Hailun City township that works in peace and contentment works in peace and contentment in the high quality soybean balance fertilizing demonstration area, village, and physical features is smooth, the fertility uniformity
Essential nutrient contents is an organic matter 3.3%, alkali-hydrolyzable nitrogen 160ppm, rapid available phosphorus 32ppm, quick-acting nitrogen 185ppm
2, star village, Hailin City Xin An town Guo Wen opens in the tame contracted field.Middle fertility, quality are middle earth
Organic content 2.76%, full nitrogenous fertilizer 0.154%, available phosphorus 19.8mg/kg, available potassium 121mg/kg
Four, test result analysis
1, to the influence of soybean growth period
Table 1 soybean growth period questionnaire
This efficient composite mixed foliage fertilizer of table 1 explanation can better satisfy the soybean growth needs, accelerates the soybean growing process, has the effect that promotes the soybean premature ripening.
2, soybean is given birth to the influence of proterties
Table 2 soybean fertility proterties questionnaire
Figure A20061001001700061
As can be seen from Table 2, soybean sprays the volume increase composite mixed foliage fertilizer, and the florescence plant height contrasts high 6.3cm, many 6 of root nodule.
3, to the influence of soybean yields
Table 3 soybean is surveyed and produces and the species test table
Figure A20061001001700062
As can be seen from Table 3, soybean sprays the foliage fertilizer plant height and contrasts high 6.4cm, many 7.4 of strain grain number, and many 0.5 grams of 100-grain weight, 29.1 kilograms of mu volume increase, stimulation ratio is 16.8%.
4, interpretation of result
Variation DF SS MS The F value F 0.05 F 0.01
The Hailin The Helen The Hailin The Helen The Hailin The Helen
Between repetition 2 7.19 16.3 3.59 8.16 —— —— 6.94 18.00
Between processing 2 4.26 235.22 2.13 117.61 14.01 14.63
Error 4 0.61 32.17 0.152 8.04
Sum 8 12.06 283.72
The F value is all greater than F between processing 0.05=6.94, but between handling the F value less than F 0.01=18.00, reach conspicuous level, illustrate and handle increase yield significantly.
Five, conclusion
By surveying family species test and variance analysis, on output, comparison is handled according to 20.8 kilograms of volume increase per mu in two places, and stimulation ratio per mu is 12.55%, and stimulation ratio is 16.8% at most.It is remarkable that ANOVA showed significant is handled differences, and the foliage fertilizer effect of increasing production is obvious.
Composite mixed foliage fertilizer prescription field screening test of the present invention:
One, test objective
This formulating of recipe purpose is the Chinese northern traditional fertilization mode of reform, use base fertilizer in routine, and only spray under single amino acid or the not obvious present situation of little fertile effect of increasing production on the blade face at early growth period, take into full account the growth rhythm of plant physiology demand, nutritional needs, select that multiple nutrient is composite to go out a kind of novel product for use, and giving full play to the advantage that it increases production and improves productivity, the spy does this prescription screening design.And several prescriptions by field test examination design are to the influence of breeding time, biological character and the output of soybean, thereby filter out best prescription.
Two, test materials and method
1, for examination fertilizer: foliage fertilizer formulation series---our company provides.
2, for studying thing: soybean, the farming 14 of pacifying
3, test method: randomized blocks is adopted in this test.If 5 processing, 3 repetitions, random alignment, 4 row districts are established in each sub-district, long 21 meters of row, the sub-district area is 84m 2
4, test is handled:
Handle 1---amino acid 6%, little fertile 1.0%, nitrogen content 5%, phosphorus content 2%, potassium content 1%, sodium nitrophenolate 0.4%, wetting agent 0.2%, sorbent material 0.15%, permeate agent 0.3%, synergistic agent are 0.5%
Handle 2---amino acid 8%, little fertile 1.8%, nitrogen content 10%, phosphorus content 3%, potassium content 2%, sodium nitrophenolate 0.4%, wetting agent 0.2%, sorbent material 0.15%, permeate agent 0.3%, synergistic agent are 0.5%
Handle 3---amino acid/11 0%, little fertile 2.5%, nitrogen content 15%, phosphorus content 5%, potassium content 3%, sodium nitrophenolate 0.4%, wetting agent 0.2%, sorbent material 0.15%, permeate agent 0.3%, synergistic agent are 0.5% and handle 4---the spray clear water
Handle 5---blank
More than handle 1~5 and all use equivalent base fertilizer
Three, test basic condition
This test is implemented in institute of Suihua City Heilongjiang Qida Pesticide Development Co., Ltd. experimental field.Soil type is a chernozem, middle fertility, organic content 2.54%, fast nitrogen 146.12ppm, fast phosphorus 54.2ppm, fast potassium 198.2ppm, pH value 6.8.Physical features is smooth, and fertility is even, May 2 mechanical making ridge, May 3 sowing.Base fertilizer mu is executed urea 2kg, diammonium phosphate 10kg, Repone K 3kg.Spray for the first time in soybean early flowering season June 28, July 12 sprayed for the second time.
Four, test results and analysis
1, to the influence of soybean growth period:
Table 1 soybean growth period plan
As can be seen from Table 1: handle 1~3 and handled 4 advance flowering period 2~3 days, handled 5 advance flowering period 4 days; Fruiting period, handled 4 and shifts to an earlier date 3 days, handles 5 and shifts to an earlier date 4 days; Ripening stage handles 4 and shifts to an earlier date 2 days, handles 5 and shifts to an earlier date 4 days; It is not obvious to handle 1,2,3 differences.
2, to the influence of soybean biological proterties
Table 2 soybean fertility proterties investigation (investigation on July 25)
As can be seen from Table 2: spray processing 1,2,3 plant heights and all be higher than control treatment 4,5, wherein, exceed 4.5cm, exceed 6.4cm than handling 5 than handling 4 to handle 3 for the highest; The number of blade also to handle 3 for the highest, is handled 1 and is had more 1.5, has more 0.9 than handling 2, exceeds 2.7cm than handling 4, exceeds 2.9cm than handling 5; All leaf looks that sprays foliage fertilizer all show as deep green, and contrast then is a light green.
3, to the influence of soybean yields
Table 3 soybean field is surveyed and is produced and indoor species test table
Figure A20061001001700082
Table 4 cell production (kg/8m 2)
Table 5 analysis of variance
Variation Mi Yuan Degree of freedom (dt) Sum of squares (ss) Variance (s 2) The F value F 0.05 F 0.01
Between processing 4 12.28 3.07 22.65 4.5 9.2
Between repetition (between district's group) 2 0.074 0.037 —— —— ——
Error 6 0.813 0.1355 —— —— ——
Total variation 12 13.167 —— —— —— ——
The F test result shows: F value>F 0.05And F 0.01, reach utmost point conspicuous level between processing, illustrate and handle increase yield significantly.
Five, conclusion (of pressure testing)
Produce species test and variance analysis by surveying, on output, handle 3 comparisons according to mu volume increase 25.91kg, stimulation ratio reaches 11.80%, and it is remarkable that ANOVA showed significant is handled differences, and the foliage fertilizer effect of increasing production is obvious.Given this conclusion filters out and handles 3 (be that aminoacids content is 10%, little fertile content is 2.5%, nitrogen (N) content 15%, phosphorus (P 2O 5) 5%, potassium (K 2O) 3%, sodium nitrophenolate 0.4%, blade face wetting agent 0.2%, sorbent material 0.15%, permeate agent 0.3%, synergistic agent 0.5%.) be optimum formula.

Claims (5)

1, a kind of composite mixed foliage fertilizer is characterized in that: its effective ingredient weight ratio is:
Amino acid accounts for 5-15%, and nitrogenous fertilizer (N) accounts for 5-30%, phosphate fertilizer (P 2O 5) account for 2-15%, potash fertilizer (K 2O) account for 1-6%, trace element accounts for 1-5%, and sodium nitrophenolate accounts for 0.1-2%, and wetting agent NNO accounts for 0.1-1%, and permeate agent accounts for 0.1-0.7%, and surplus is a water.
2, a kind of composite mixed foliage fertilizer as claimed in claim 1 is characterized in that: add the sorbent material TP of 0.1-1% and the synergistic agent syn of 0.1-0.8%.
3, a kind of composite mixed foliage fertilizer as claimed in claim 1 or 2 is characterized in that: amino acid/11 0%, nitrogenous fertilizer 15%, phosphate fertilizer 5%, potash fertilizer 3%, trace element 2.5%, sodium nitrophenolate 0.4%, wetting agent 0.2%, permeate agent 0.3%, sorbent material 0.15%, synergistic agent 0.5%, surplus is a water.
4, as claim 1 or 3 described a kind of composite mixed foliage fertilizers, it is characterized in that: described trace element comprises zinc, iron, copper, molybdenum.
5, a kind of preparation method of composite mixed foliage fertilizer as claimed in claim 1 or 2 is characterized in that:
Raw material amino acid, nitrogenous fertilizer, phosphate fertilizer, potash fertilizer and trace element pulverizing are dissolved it with a small amount of solvent water; With less water sodium nitrophenolate is dissolved in addition, after the two mixes, add suitable quantity of water dissolved blade face wetting agent, sorbent material, permeate agent and synergistic agent, after mixing, stirring pH value with the excess water dilution is 2-6, promptly makes.
CN 200610010017 2006-05-01 2006-05-01 Composite mixed foliage fertilizer and its preparation Pending CN1896034A (en)

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Cited By (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101973820A (en) * 2010-09-26 2011-02-16 王春雨 Foliar fertilizer and production method thereof
CN102584407A (en) * 2012-03-19 2012-07-18 广西壮族自治区林业科学研究院 Special fertilizer for leaf surfaces at oil-tea camellia seedling stage and preparing method thereof
CN101768021B (en) * 2008-12-31 2014-02-05 罗波 Organic material composting promoter and preparation method and application thereof
CN107141098A (en) * 2017-06-01 2017-09-08 平南县颖绿龙眼种植专业合作社 A kind of foliar fertilizer for improving Longan Output
CN114907158A (en) * 2022-06-26 2022-08-16 陇西县农业技术推广中心 Preparation method and use method of leaf fertilizer for planting traditional Chinese medicinal materials

Cited By (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101768021B (en) * 2008-12-31 2014-02-05 罗波 Organic material composting promoter and preparation method and application thereof
CN101973820A (en) * 2010-09-26 2011-02-16 王春雨 Foliar fertilizer and production method thereof
CN102584407A (en) * 2012-03-19 2012-07-18 广西壮族自治区林业科学研究院 Special fertilizer for leaf surfaces at oil-tea camellia seedling stage and preparing method thereof
CN107141098A (en) * 2017-06-01 2017-09-08 平南县颖绿龙眼种植专业合作社 A kind of foliar fertilizer for improving Longan Output
CN114907158A (en) * 2022-06-26 2022-08-16 陇西县农业技术推广中心 Preparation method and use method of leaf fertilizer for planting traditional Chinese medicinal materials

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