CN1287218C - 卤化银照相光敏材料 - Google Patents
卤化银照相光敏材料 Download PDFInfo
- Publication number
- CN1287218C CN1287218C CNB011384069A CN01138406A CN1287218C CN 1287218 C CN1287218 C CN 1287218C CN B011384069 A CNB011384069 A CN B011384069A CN 01138406 A CN01138406 A CN 01138406A CN 1287218 C CN1287218 C CN 1287218C
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- Prior art keywords
- emulsion
- particle
- silver halide
- silver
- add
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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- 229910052709 silver Inorganic materials 0.000 title claims abstract description 237
- 239000004332 silver Substances 0.000 title claims abstract description 237
- -1 Silver halide Chemical class 0.000 title claims abstract description 223
- 239000000463 material Substances 0.000 title claims abstract description 56
- 230000003287 optical effect Effects 0.000 title description 6
- 239000000839 emulsion Substances 0.000 claims abstract description 346
- 238000011161 development Methods 0.000 claims abstract description 99
- 230000005855 radiation Effects 0.000 claims abstract description 55
- 239000002245 particle Substances 0.000 claims description 307
- 238000000034 method Methods 0.000 claims description 196
- 230000018109 developmental process Effects 0.000 claims description 94
- 230000008569 process Effects 0.000 claims description 56
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 38
- 239000013078 crystal Substances 0.000 claims description 32
- XUAJZOHXBBRXOX-UHFFFAOYSA-M [Ag]Br.[I] Chemical compound [Ag]Br.[I] XUAJZOHXBBRXOX-UHFFFAOYSA-M 0.000 claims description 21
- QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 claims description 18
- ORQHYVQMBSCQBZ-UHFFFAOYSA-M [Cl].[Ag]Br.[I] Chemical compound [Cl].[Ag]Br.[I] ORQHYVQMBSCQBZ-UHFFFAOYSA-M 0.000 claims description 13
- CIWBSHSKHKDKBQ-JLAZNSOCSA-N Ascorbic acid Chemical compound OC[C@H](O)[C@H]1OC(=O)C(O)=C1O CIWBSHSKHKDKBQ-JLAZNSOCSA-N 0.000 claims description 12
- 229960005070 ascorbic acid Drugs 0.000 claims description 6
- 239000002211 L-ascorbic acid Substances 0.000 claims description 4
- 235000000069 L-ascorbic acid Nutrition 0.000 claims description 4
- 230000000977 initiatory effect Effects 0.000 abstract description 3
- 230000005251 gamma ray Effects 0.000 abstract 1
- IOLCXVTUBQKXJR-UHFFFAOYSA-M potassium bromide Chemical compound [K+].[Br-] IOLCXVTUBQKXJR-UHFFFAOYSA-M 0.000 description 174
- 239000010410 layer Substances 0.000 description 141
- 239000007864 aqueous solution Substances 0.000 description 138
- 239000000243 solution Substances 0.000 description 110
- 239000000975 dye Substances 0.000 description 68
- 230000001235 sensitizing effect Effects 0.000 description 61
- 238000006243 chemical reaction Methods 0.000 description 60
- BQCADISMDOOEFD-UHFFFAOYSA-N Silver Chemical compound [Ag] BQCADISMDOOEFD-UHFFFAOYSA-N 0.000 description 59
- 229920000159 gelatin Polymers 0.000 description 59
- 235000019322 gelatine Nutrition 0.000 description 59
- 239000008273 gelatin Substances 0.000 description 58
- 108010010803 Gelatin Proteins 0.000 description 56
- 241000276425 Xiphophorus maculatus Species 0.000 description 56
- 235000011852 gelatine desserts Nutrition 0.000 description 56
- 239000000126 substance Substances 0.000 description 56
- 235000013339 cereals Nutrition 0.000 description 54
- 230000035945 sensitivity Effects 0.000 description 52
- 150000001875 compounds Chemical class 0.000 description 50
- 206010070834 Sensitisation Diseases 0.000 description 48
- 230000008313 sensitization Effects 0.000 description 48
- 101710134784 Agnoprotein Proteins 0.000 description 46
- 238000002360 preparation method Methods 0.000 description 46
- 230000008961 swelling Effects 0.000 description 41
- 229910021612 Silver iodide Inorganic materials 0.000 description 29
- NLKNQRATVPKPDG-UHFFFAOYSA-M potassium iodide Chemical compound [K+].[I-] NLKNQRATVPKPDG-UHFFFAOYSA-M 0.000 description 29
- 235000019580 granularity Nutrition 0.000 description 25
- 239000000654 additive Substances 0.000 description 24
- 239000003446 ligand Substances 0.000 description 22
- 238000011010 flushing procedure Methods 0.000 description 21
- 150000002500 ions Chemical class 0.000 description 21
- 230000003595 spectral effect Effects 0.000 description 21
- 229910052751 metal Inorganic materials 0.000 description 20
- 239000002184 metal Substances 0.000 description 20
- 230000000996 additive effect Effects 0.000 description 19
- 239000011248 coating agent Substances 0.000 description 18
- 238000000576 coating method Methods 0.000 description 18
- 239000010419 fine particle Substances 0.000 description 18
- GGCZERPQGJTIQP-UHFFFAOYSA-N sodium;9,10-dioxoanthracene-2-sulfonic acid Chemical compound [Na+].C1=CC=C2C(=O)C3=CC(S(=O)(=O)O)=CC=C3C(=O)C2=C1 GGCZERPQGJTIQP-UHFFFAOYSA-N 0.000 description 16
- 238000003756 stirring Methods 0.000 description 15
- 239000008187 granular material Substances 0.000 description 14
- 229910052736 halogen Inorganic materials 0.000 description 14
- 239000007788 liquid Substances 0.000 description 14
- 150000002367 halogens Chemical class 0.000 description 13
- KWYUFKZDYYNOTN-UHFFFAOYSA-M Potassium hydroxide Chemical compound [OH-].[K+] KWYUFKZDYYNOTN-UHFFFAOYSA-M 0.000 description 12
- 230000000052 comparative effect Effects 0.000 description 12
- 230000000694 effects Effects 0.000 description 12
- 239000000047 product Substances 0.000 description 12
- SQGYOTSLMSWVJD-UHFFFAOYSA-N silver(1+) nitrate Chemical compound [Ag+].[O-]N(=O)=O SQGYOTSLMSWVJD-UHFFFAOYSA-N 0.000 description 12
- GEHJYWRUCIMESM-UHFFFAOYSA-L sodium sulfite Chemical compound [Na+].[Na+].[O-]S([O-])=O GEHJYWRUCIMESM-UHFFFAOYSA-L 0.000 description 12
- 239000002253 acid Substances 0.000 description 11
- 239000003795 chemical substances by application Substances 0.000 description 11
- 238000009826 distribution Methods 0.000 description 11
- 150000001455 metallic ions Chemical class 0.000 description 11
- 150000003839 salts Chemical class 0.000 description 11
- ZMZDMBWJUHKJPS-UHFFFAOYSA-N thiocyanic acid Chemical compound SC#N ZMZDMBWJUHKJPS-UHFFFAOYSA-N 0.000 description 11
- KDLHZDBZIXYQEI-UHFFFAOYSA-N Palladium Chemical compound [Pd] KDLHZDBZIXYQEI-UHFFFAOYSA-N 0.000 description 10
- 239000000203 mixture Substances 0.000 description 10
- JMANVNJQNLATNU-UHFFFAOYSA-N oxalonitrile Chemical compound N#CC#N JMANVNJQNLATNU-UHFFFAOYSA-N 0.000 description 10
- QGKMIGUHVLGJBR-UHFFFAOYSA-M (4z)-1-(3-methylbutyl)-4-[[1-(3-methylbutyl)quinolin-1-ium-4-yl]methylidene]quinoline;iodide Chemical compound [I-].C12=CC=CC=C2N(CCC(C)C)C=CC1=CC1=CC=[N+](CCC(C)C)C2=CC=CC=C12 QGKMIGUHVLGJBR-UHFFFAOYSA-M 0.000 description 9
- JKFYKCYQEWQPTM-UHFFFAOYSA-N 2-azaniumyl-2-(4-fluorophenyl)acetate Chemical compound OC(=O)C(N)C1=CC=C(F)C=C1 JKFYKCYQEWQPTM-UHFFFAOYSA-N 0.000 description 9
- CSCPPACGZOOCGX-UHFFFAOYSA-N Acetone Chemical compound CC(C)=O CSCPPACGZOOCGX-UHFFFAOYSA-N 0.000 description 9
- PNEYBMLMFCGWSK-UHFFFAOYSA-N Alumina Chemical compound [O-2].[O-2].[O-2].[Al+3].[Al+3] PNEYBMLMFCGWSK-UHFFFAOYSA-N 0.000 description 9
- 230000008901 benefit Effects 0.000 description 9
- 230000015572 biosynthetic process Effects 0.000 description 9
- 239000006185 dispersion Substances 0.000 description 9
- XMBWDFGMSWQBCA-UHFFFAOYSA-M iodide Chemical compound [I-] XMBWDFGMSWQBCA-UHFFFAOYSA-M 0.000 description 9
- 229940006461 iodide ion Drugs 0.000 description 9
- 238000006116 polymerization reaction Methods 0.000 description 9
- 229940045105 silver iodide Drugs 0.000 description 9
- FAPWRFPIFSIZLT-UHFFFAOYSA-M Sodium chloride Chemical compound [Na+].[Cl-] FAPWRFPIFSIZLT-UHFFFAOYSA-M 0.000 description 8
- 239000005864 Sulphur Substances 0.000 description 8
- 229910052799 carbon Inorganic materials 0.000 description 8
- 230000008859 change Effects 0.000 description 8
- 239000003153 chemical reaction reagent Substances 0.000 description 8
- 238000005304 joining Methods 0.000 description 8
- 239000012071 phase Substances 0.000 description 8
- XNGIFLGASWRNHJ-UHFFFAOYSA-N phthalic acid Chemical compound OC(=O)C1=CC=CC=C1C(O)=O XNGIFLGASWRNHJ-UHFFFAOYSA-N 0.000 description 8
- 229910001961 silver nitrate Inorganic materials 0.000 description 8
- 239000003381 stabilizer Substances 0.000 description 8
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 description 7
- NINIDFKCEFEMDL-UHFFFAOYSA-N Sulfur Chemical compound [S] NINIDFKCEFEMDL-UHFFFAOYSA-N 0.000 description 7
- 239000000084 colloidal system Substances 0.000 description 7
- 230000006866 deterioration Effects 0.000 description 7
- 239000000986 disperse dye Substances 0.000 description 7
- ZNNZYHKDIALBAK-UHFFFAOYSA-M potassium thiocyanate Chemical compound [K+].[S-]C#N ZNNZYHKDIALBAK-UHFFFAOYSA-M 0.000 description 7
- 229910052711 selenium Inorganic materials 0.000 description 7
- 239000011669 selenium Substances 0.000 description 7
- 239000011734 sodium Substances 0.000 description 7
- QAOWNCQODCNURD-UHFFFAOYSA-N sulfuric acid Substances OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 description 7
- RYYXDZDBXNUPOG-UHFFFAOYSA-N 4,5,6,7-tetrahydro-1,3-benzothiazole-2,6-diamine;dihydrochloride Chemical compound Cl.Cl.C1C(N)CCC2=C1SC(N)=N2 RYYXDZDBXNUPOG-UHFFFAOYSA-N 0.000 description 6
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 description 6
- 241000209094 Oryza Species 0.000 description 6
- 235000007164 Oryza sativa Nutrition 0.000 description 6
- BUGBHKTXTAQXES-UHFFFAOYSA-N Selenium Chemical compound [Se] BUGBHKTXTAQXES-UHFFFAOYSA-N 0.000 description 6
- PMZURENOXWZQFD-UHFFFAOYSA-L Sodium Sulfate Chemical compound [Na+].[Na+].[O-]S([O-])(=O)=O PMZURENOXWZQFD-UHFFFAOYSA-L 0.000 description 6
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 6
- XYXNTHIYBIDHGM-UHFFFAOYSA-N ammonium thiosulfate Chemical compound [NH4+].[NH4+].[O-]S([O-])(=O)=S XYXNTHIYBIDHGM-UHFFFAOYSA-N 0.000 description 6
- 150000002148 esters Chemical class 0.000 description 6
- 150000004820 halides Chemical class 0.000 description 6
- 238000004519 manufacturing process Methods 0.000 description 6
- 235000009566 rice Nutrition 0.000 description 6
- 235000010265 sodium sulphite Nutrition 0.000 description 6
- 239000002904 solvent Substances 0.000 description 6
- ZCYVEMRRCGMTRW-UHFFFAOYSA-N 7553-56-2 Chemical compound [I] ZCYVEMRRCGMTRW-UHFFFAOYSA-N 0.000 description 5
- 101100501966 Caenorhabditis elegans exc-6 gene Proteins 0.000 description 5
- 235000008733 Citrus aurantifolia Nutrition 0.000 description 5
- GUTLYIVDDKVIGB-OUBTZVSYSA-N Cobalt-60 Chemical compound [60Co] GUTLYIVDDKVIGB-OUBTZVSYSA-N 0.000 description 5
- 235000011941 Tilia x europaea Nutrition 0.000 description 5
- 239000003513 alkali Substances 0.000 description 5
- 230000005540 biological transmission Effects 0.000 description 5
- 150000004696 coordination complex Chemical class 0.000 description 5
- 125000004093 cyano group Chemical group *C#N 0.000 description 5
- FDWREHZXQUYJFJ-UHFFFAOYSA-M gold monochloride Chemical compound [Cl-].[Au+] FDWREHZXQUYJFJ-UHFFFAOYSA-M 0.000 description 5
- 230000006872 improvement Effects 0.000 description 5
- 229910052740 iodine Inorganic materials 0.000 description 5
- 239000004571 lime Substances 0.000 description 5
- 229910052763 palladium Inorganic materials 0.000 description 5
- 150000002941 palladium compounds Chemical class 0.000 description 5
- 239000000843 powder Substances 0.000 description 5
- 238000012545 processing Methods 0.000 description 5
- 230000001105 regulatory effect Effects 0.000 description 5
- 239000012266 salt solution Substances 0.000 description 5
- ADZWSOLPGZMUMY-UHFFFAOYSA-M silver bromide Chemical compound [Ag]Br ADZWSOLPGZMUMY-UHFFFAOYSA-M 0.000 description 5
- AKHNMLFCWUSKQB-UHFFFAOYSA-L sodium thiosulfate Chemical compound [Na+].[Na+].[O-]S([O-])(=O)=S AKHNMLFCWUSKQB-UHFFFAOYSA-L 0.000 description 5
- 235000019345 sodium thiosulphate Nutrition 0.000 description 5
- AZQWKYJCGOJGHM-UHFFFAOYSA-N 1,4-benzoquinone Chemical compound O=C1C=CC(=O)C=C1 AZQWKYJCGOJGHM-UHFFFAOYSA-N 0.000 description 4
- RVXJIYJPQXRIEM-UHFFFAOYSA-N 1-$l^{1}-selanyl-n,n-dimethylmethanimidamide Chemical compound CN(C)C([Se])=N RVXJIYJPQXRIEM-UHFFFAOYSA-N 0.000 description 4
- KDCGOANMDULRCW-UHFFFAOYSA-N 7H-purine Chemical compound N1=CNC2=NC=NC2=C1 KDCGOANMDULRCW-UHFFFAOYSA-N 0.000 description 4
- QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 description 4
- VEXZGXHMUGYJMC-UHFFFAOYSA-M Chloride anion Chemical compound [Cl-] VEXZGXHMUGYJMC-UHFFFAOYSA-M 0.000 description 4
- WSFSSNUMVMOOMR-UHFFFAOYSA-N Formaldehyde Chemical group O=C WSFSSNUMVMOOMR-UHFFFAOYSA-N 0.000 description 4
- UQSXHKLRYXJYBZ-UHFFFAOYSA-N Iron oxide Chemical compound [Fe]=O UQSXHKLRYXJYBZ-UHFFFAOYSA-N 0.000 description 4
- 241000446313 Lamella Species 0.000 description 4
- GLUUGHFHXGJENI-UHFFFAOYSA-N Piperazine Chemical compound C1CNCCN1 GLUUGHFHXGJENI-UHFFFAOYSA-N 0.000 description 4
- 239000004372 Polyvinyl alcohol Substances 0.000 description 4
- JUJWROOIHBZHMG-UHFFFAOYSA-N Pyridine Chemical compound C1=CC=NC=C1 JUJWROOIHBZHMG-UHFFFAOYSA-N 0.000 description 4
- FOIXSVOLVBLSDH-UHFFFAOYSA-N Silver ion Chemical compound [Ag+] FOIXSVOLVBLSDH-UHFFFAOYSA-N 0.000 description 4
- MCMNRKCIXSYSNV-UHFFFAOYSA-N Zirconium dioxide Chemical compound O=[Zr]=O MCMNRKCIXSYSNV-UHFFFAOYSA-N 0.000 description 4
- 238000010521 absorption reaction Methods 0.000 description 4
- 239000002671 adjuvant Substances 0.000 description 4
- QGZKDVFQNNGYKY-UHFFFAOYSA-O ammonium group Chemical group [NH4+] QGZKDVFQNNGYKY-UHFFFAOYSA-O 0.000 description 4
- 235000011114 ammonium hydroxide Nutrition 0.000 description 4
- 238000004061 bleaching Methods 0.000 description 4
- 239000007844 bleaching agent Substances 0.000 description 4
- 239000007767 bonding agent Substances 0.000 description 4
- 238000004364 calculation method Methods 0.000 description 4
- 229920001429 chelating resin Polymers 0.000 description 4
- 230000001143 conditioned effect Effects 0.000 description 4
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- 238000005516 engineering process Methods 0.000 description 4
- 239000011630 iodine Substances 0.000 description 4
- 239000006224 matting agent Substances 0.000 description 4
- 238000002156 mixing Methods 0.000 description 4
- 229910000510 noble metal Inorganic materials 0.000 description 4
- 239000007800 oxidant agent Substances 0.000 description 4
- 229910052760 oxygen Inorganic materials 0.000 description 4
- BASFCYQUMIYNBI-UHFFFAOYSA-N platinum Chemical compound [Pt] BASFCYQUMIYNBI-UHFFFAOYSA-N 0.000 description 4
- 229920002451 polyvinyl alcohol Polymers 0.000 description 4
- 125000002924 primary amino group Chemical group [H]N([H])* 0.000 description 4
- 238000011160 research Methods 0.000 description 4
- 239000011780 sodium chloride Substances 0.000 description 4
- 239000007962 solid dispersion Substances 0.000 description 4
- 229910052714 tellurium Inorganic materials 0.000 description 4
- 239000006097 ultraviolet radiation absorber Substances 0.000 description 4
- PAWQVTBBRAZDMG-UHFFFAOYSA-N 2-(3-bromo-2-fluorophenyl)acetic acid Chemical compound OC(=O)CC1=CC=CC(Br)=C1F PAWQVTBBRAZDMG-UHFFFAOYSA-N 0.000 description 3
- AXDJCCTWPBKUKL-UHFFFAOYSA-N 4-[(4-aminophenyl)-(4-imino-3-methylcyclohexa-2,5-dien-1-ylidene)methyl]aniline;hydron;chloride Chemical compound Cl.C1=CC(=N)C(C)=CC1=C(C=1C=CC(N)=CC=1)C1=CC=C(N)C=C1 AXDJCCTWPBKUKL-UHFFFAOYSA-N 0.000 description 3
- OYPRJOBELJOOCE-UHFFFAOYSA-N Calcium Chemical compound [Ca] OYPRJOBELJOOCE-UHFFFAOYSA-N 0.000 description 3
- 102000004190 Enzymes Human genes 0.000 description 3
- 108090000790 Enzymes Proteins 0.000 description 3
- 239000001828 Gelatine Substances 0.000 description 3
- 101000964479 Homo sapiens Zinc finger and BTB domain-containing protein 18 Proteins 0.000 description 3
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 description 3
- ZLMJMSJWJFRBEC-UHFFFAOYSA-N Potassium Chemical compound [K] ZLMJMSJWJFRBEC-UHFFFAOYSA-N 0.000 description 3
- 229910021607 Silver chloride Inorganic materials 0.000 description 3
- ZMZDMBWJUHKJPS-UHFFFAOYSA-M Thiocyanate anion Chemical compound [S-]C#N ZMZDMBWJUHKJPS-UHFFFAOYSA-M 0.000 description 3
- 235000010724 Wisteria floribunda Nutrition 0.000 description 3
- 102100040762 Zinc finger and BTB domain-containing protein 18 Human genes 0.000 description 3
- 229910052946 acanthite Inorganic materials 0.000 description 3
- 150000007513 acids Chemical class 0.000 description 3
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 3
- 239000012752 auxiliary agent Substances 0.000 description 3
- 238000000498 ball milling Methods 0.000 description 3
- 239000011324 bead Substances 0.000 description 3
- GDTBXPJZTBHREO-UHFFFAOYSA-N bromine Chemical compound BrBr GDTBXPJZTBHREO-UHFFFAOYSA-N 0.000 description 3
- 239000011575 calcium Substances 0.000 description 3
- 229910052791 calcium Inorganic materials 0.000 description 3
- 239000001913 cellulose Substances 0.000 description 3
- 229920002678 cellulose Polymers 0.000 description 3
- 239000007795 chemical reaction product Substances 0.000 description 3
- 239000002131 composite material Substances 0.000 description 3
- 102000038379 digestive enzymes Human genes 0.000 description 3
- 108091007734 digestive enzymes Proteins 0.000 description 3
- HMGMGVYGCBAGMQ-UHFFFAOYSA-L disodium 1,3,5-triazinane-2,4,6-trione dichloride Chemical compound [Cl-].[Cl-].N1C(=O)NC(=O)NC1=O.[Na+].[Na+] HMGMGVYGCBAGMQ-UHFFFAOYSA-L 0.000 description 3
- 238000010893 electron trap Methods 0.000 description 3
- 125000005843 halogen group Chemical group 0.000 description 3
- 125000004435 hydrogen atom Chemical group [H]* 0.000 description 3
- KONZICNQWURKQP-UHFFFAOYSA-N hydroxy-oxo-phenoxy-sulfanylidene-$l^{6}-sulfane Chemical compound OS(=O)(=S)OC1=CC=CC=C1 KONZICNQWURKQP-UHFFFAOYSA-N 0.000 description 3
- 229910052741 iridium Inorganic materials 0.000 description 3
- GKOZUEZYRPOHIO-UHFFFAOYSA-N iridium atom Chemical compound [Ir] GKOZUEZYRPOHIO-UHFFFAOYSA-N 0.000 description 3
- 239000004816 latex Substances 0.000 description 3
- 229920000126 latex Polymers 0.000 description 3
- DZVCFNFOPIZQKX-LTHRDKTGSA-M merocyanine Chemical compound [Na+].O=C1N(CCCC)C(=O)N(CCCC)C(=O)C1=C\C=C\C=C/1N(CCCS([O-])(=O)=O)C2=CC=CC=C2O\1 DZVCFNFOPIZQKX-LTHRDKTGSA-M 0.000 description 3
- 230000004048 modification Effects 0.000 description 3
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- 239000001301 oxygen Substances 0.000 description 3
- 229920000120 polyethyl acrylate Polymers 0.000 description 3
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- 229910052700 potassium Inorganic materials 0.000 description 3
- 239000011591 potassium Substances 0.000 description 3
- 230000001681 protective effect Effects 0.000 description 3
- 230000002285 radioactive effect Effects 0.000 description 3
- HKZLPVFGJNLROG-UHFFFAOYSA-M silver monochloride Chemical compound [Cl-].[Ag+] HKZLPVFGJNLROG-UHFFFAOYSA-M 0.000 description 3
- 229940056910 silver sulfide Drugs 0.000 description 3
- XUARKZBEFFVFRG-UHFFFAOYSA-N silver sulfide Chemical compound [S-2].[Ag+].[Ag+] XUARKZBEFFVFRG-UHFFFAOYSA-N 0.000 description 3
- 229910052708 sodium Inorganic materials 0.000 description 3
- 229910052938 sodium sulfate Inorganic materials 0.000 description 3
- 235000011152 sodium sulphate Nutrition 0.000 description 3
- KDYFGRWQOYBRFD-UHFFFAOYSA-N succinic acid Chemical compound OC(=O)CCC(O)=O KDYFGRWQOYBRFD-UHFFFAOYSA-N 0.000 description 3
- PORWMNRCUJJQNO-UHFFFAOYSA-N tellurium atom Chemical compound [Te] PORWMNRCUJJQNO-UHFFFAOYSA-N 0.000 description 3
- YUYCVXFAYWRXLS-UHFFFAOYSA-N trimethoxysilane Chemical compound CO[SiH](OC)OC YUYCVXFAYWRXLS-UHFFFAOYSA-N 0.000 description 3
- TXUICONDJPYNPY-UHFFFAOYSA-N (1,10,13-trimethyl-3-oxo-4,5,6,7,8,9,11,12,14,15,16,17-dodecahydrocyclopenta[a]phenanthren-17-yl) heptanoate Chemical compound C1CC2CC(=O)C=C(C)C2(C)C2C1C1CCC(OC(=O)CCCCCC)C1(C)CC2 TXUICONDJPYNPY-UHFFFAOYSA-N 0.000 description 2
- NWUYHJFMYQTDRP-UHFFFAOYSA-N 1,2-bis(ethenyl)benzene;1-ethenyl-2-ethylbenzene;styrene Chemical compound C=CC1=CC=CC=C1.CCC1=CC=CC=C1C=C.C=CC1=CC=CC=C1C=C NWUYHJFMYQTDRP-UHFFFAOYSA-N 0.000 description 2
- NSPMIYGKQJPBQR-UHFFFAOYSA-N 4H-1,2,4-triazole Chemical compound C=1N=CNN=1 NSPMIYGKQJPBQR-UHFFFAOYSA-N 0.000 description 2
- PAYRUJLWNCNPSJ-UHFFFAOYSA-N Aniline Chemical compound NC1=CC=CC=C1 PAYRUJLWNCNPSJ-UHFFFAOYSA-N 0.000 description 2
- QKAKHBUMCMDTAX-UHFFFAOYSA-N C1C=CC2=CC=CC=C12.N1C=CC=CC=C1 Chemical class C1C=CC2=CC=CC=C12.N1C=CC=CC=C1 QKAKHBUMCMDTAX-UHFFFAOYSA-N 0.000 description 2
- 101100501963 Caenorhabditis elegans exc-4 gene Proteins 0.000 description 2
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 2
- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 description 2
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 2
- OAKJQQAXSVQMHS-UHFFFAOYSA-N Hydrazine Chemical compound NN OAKJQQAXSVQMHS-UHFFFAOYSA-N 0.000 description 2
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- VOLCSSLIOHKGDN-UHFFFAOYSA-N [Se](O)(O)(=O)=O.N#CC#N Chemical compound [Se](O)(O)(=O)=O.N#CC#N VOLCSSLIOHKGDN-UHFFFAOYSA-N 0.000 description 1
- DHKHKXVYLBGOIT-UHFFFAOYSA-N acetaldehyde Diethyl Acetal Natural products CCOC(C)OCC DHKHKXVYLBGOIT-UHFFFAOYSA-N 0.000 description 1
- 150000001242 acetic acid derivatives Chemical class 0.000 description 1
- 125000002777 acetyl group Chemical class [H]C([H])([H])C(*)=O 0.000 description 1
- 150000008065 acid anhydrides Chemical class 0.000 description 1
- 238000013019 agitation Methods 0.000 description 1
- 125000000217 alkyl group Chemical group 0.000 description 1
- 150000001412 amines Chemical class 0.000 description 1
- SOIFLUNRINLCBN-UHFFFAOYSA-N ammonium thiocyanate Chemical compound [NH4+].[S-]C#N SOIFLUNRINLCBN-UHFFFAOYSA-N 0.000 description 1
- 125000002029 aromatic hydrocarbon group Chemical group 0.000 description 1
- 125000000852 azido group Chemical group *N=[N+]=[N-] 0.000 description 1
- 230000006399 behavior Effects 0.000 description 1
- 150000001556 benzimidazoles Chemical class 0.000 description 1
- 150000004054 benzoquinones Chemical group 0.000 description 1
- 229960004217 benzyl alcohol Drugs 0.000 description 1
- 230000003115 biocidal effect Effects 0.000 description 1
- 238000009835 boiling Methods 0.000 description 1
- RJTANRZEWTUVMA-UHFFFAOYSA-N boron;n-methylmethanamine Chemical compound [B].CNC RJTANRZEWTUVMA-UHFFFAOYSA-N 0.000 description 1
- 244000309464 bull Species 0.000 description 1
- JHIWVOJDXOSYLW-UHFFFAOYSA-N butyl 2,2-difluorocyclopropane-1-carboxylate Chemical compound CCCCOC(=O)C1CC1(F)F JHIWVOJDXOSYLW-UHFFFAOYSA-N 0.000 description 1
- 229910052793 cadmium Inorganic materials 0.000 description 1
- BDOSMKKIYDKNTQ-UHFFFAOYSA-N cadmium atom Chemical compound [Cd] BDOSMKKIYDKNTQ-UHFFFAOYSA-N 0.000 description 1
- 125000002915 carbonyl group Chemical group [*:2]C([*:1])=O 0.000 description 1
- JJWKPURADFRFRB-UHFFFAOYSA-N carbonyl sulfide Chemical compound O=C=S JJWKPURADFRFRB-UHFFFAOYSA-N 0.000 description 1
- 239000001768 carboxy methyl cellulose Substances 0.000 description 1
- 235000010948 carboxy methyl cellulose Nutrition 0.000 description 1
- 239000008112 carboxymethyl-cellulose Substances 0.000 description 1
- 235000010980 cellulose Nutrition 0.000 description 1
- 229920002301 cellulose acetate Polymers 0.000 description 1
- 150000001786 chalcogen compounds Chemical class 0.000 description 1
- ZCDOYSPFYFSLEW-UHFFFAOYSA-N chromate(2-) Chemical compound [O-][Cr]([O-])(=O)=O ZCDOYSPFYFSLEW-UHFFFAOYSA-N 0.000 description 1
- 229910052804 chromium Inorganic materials 0.000 description 1
- 238000000975 co-precipitation Methods 0.000 description 1
- 229920001436 collagen Polymers 0.000 description 1
- 230000006835 compression Effects 0.000 description 1
- 238000007906 compression Methods 0.000 description 1
- 239000000470 constituent Substances 0.000 description 1
- 238000010276 construction Methods 0.000 description 1
- 230000001276 controlling effect Effects 0.000 description 1
- 238000012937 correction Methods 0.000 description 1
- 230000008878 coupling Effects 0.000 description 1
- 238000010168 coupling process Methods 0.000 description 1
- 238000005859 coupling reaction Methods 0.000 description 1
- 150000001913 cyanates Chemical class 0.000 description 1
- LKUCSBHCLHXINO-UHFFFAOYSA-N cyanatoselanyl cyanate Chemical compound N#CO[Se]OC#N LKUCSBHCLHXINO-UHFFFAOYSA-N 0.000 description 1
- UBFWAFZODRGFIF-UHFFFAOYSA-N cyanic acid;selenium Chemical compound [Se].OC#N UBFWAFZODRGFIF-UHFFFAOYSA-N 0.000 description 1
- 125000004122 cyclic group Chemical group 0.000 description 1
- 230000009849 deactivation Effects 0.000 description 1
- 239000007857 degradation product Substances 0.000 description 1
- 238000002242 deionisation method Methods 0.000 description 1
- 238000000151 deposition Methods 0.000 description 1
- 230000008021 deposition Effects 0.000 description 1
- 238000010612 desalination reaction Methods 0.000 description 1
- 238000013461 design Methods 0.000 description 1
- 238000001514 detection method Methods 0.000 description 1
- 229920005994 diacetyl cellulose Polymers 0.000 description 1
- 238000000502 dialysis Methods 0.000 description 1
- 229960004132 diethyl ether Drugs 0.000 description 1
- HPNMFZURTQLUMO-UHFFFAOYSA-N diethylamine Chemical compound CCNCC HPNMFZURTQLUMO-UHFFFAOYSA-N 0.000 description 1
- 238000007599 discharging Methods 0.000 description 1
- OKBPCTLSPGDQBO-UHFFFAOYSA-L disodium;dichloride Chemical compound [Na+].[Na+].[Cl-].[Cl-] OKBPCTLSPGDQBO-UHFFFAOYSA-L 0.000 description 1
- 238000001035 drying Methods 0.000 description 1
- 238000000635 electron micrograph Methods 0.000 description 1
- 238000004945 emulsification Methods 0.000 description 1
- 230000007515 enzymatic degradation Effects 0.000 description 1
- 125000001495 ethyl group Chemical group [H]C([H])([H])C([H])([H])* 0.000 description 1
- 238000011156 evaluation Methods 0.000 description 1
- 238000001704 evaporation Methods 0.000 description 1
- 230000008020 evaporation Effects 0.000 description 1
- 238000002474 experimental method Methods 0.000 description 1
- 230000002349 favourable effect Effects 0.000 description 1
- 238000011049 filling Methods 0.000 description 1
- 238000001914 filtration Methods 0.000 description 1
- 239000012530 fluid Substances 0.000 description 1
- 230000000855 fungicidal effect Effects 0.000 description 1
- 230000004927 fusion Effects 0.000 description 1
- 229910052733 gallium Inorganic materials 0.000 description 1
- 150000002344 gold compounds Chemical class 0.000 description 1
- JUWSSMXCCAMYGX-UHFFFAOYSA-N gold platinum Chemical compound [Pt].[Au] JUWSSMXCCAMYGX-UHFFFAOYSA-N 0.000 description 1
- 229920000578 graft copolymer Polymers 0.000 description 1
- 238000013007 heat curing Methods 0.000 description 1
- 125000004051 hexyl group Chemical group [H]C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])* 0.000 description 1
- 229920001519 homopolymer Polymers 0.000 description 1
- 150000002430 hydrocarbons Chemical group 0.000 description 1
- XMBWDFGMSWQBCA-UHFFFAOYSA-N hydrogen iodide Chemical compound I XMBWDFGMSWQBCA-UHFFFAOYSA-N 0.000 description 1
- 230000007062 hydrolysis Effects 0.000 description 1
- 238000006460 hydrolysis reaction Methods 0.000 description 1
- 229920001477 hydrophilic polymer Polymers 0.000 description 1
- 235000019447 hydroxyethyl cellulose Nutrition 0.000 description 1
- 229910000378 hydroxylammonium sulfate Inorganic materials 0.000 description 1
- 229910052738 indium Inorganic materials 0.000 description 1
- APFVFJFRJDLVQX-UHFFFAOYSA-N indium atom Chemical compound [In] APFVFJFRJDLVQX-UHFFFAOYSA-N 0.000 description 1
- 150000002475 indoles Chemical class 0.000 description 1
- 239000004615 ingredient Substances 0.000 description 1
- 239000003112 inhibitor Substances 0.000 description 1
- 239000011229 interlayer Substances 0.000 description 1
- 150000004694 iodide salts Chemical class 0.000 description 1
- 150000002503 iridium Chemical class 0.000 description 1
- 229910052742 iron Inorganic materials 0.000 description 1
- RBTARNINKXHZNM-UHFFFAOYSA-K iron trichloride Chemical class Cl[Fe](Cl)Cl RBTARNINKXHZNM-UHFFFAOYSA-K 0.000 description 1
- 125000001518 isoselenocyanato group Chemical group *N=C=[Se] 0.000 description 1
- 125000000239 isotellurocyanato group Chemical group *N=C=[Te] 0.000 description 1
- 238000004898 kneading Methods 0.000 description 1
- 230000002045 lasting effect Effects 0.000 description 1
- 238000012886 linear function Methods 0.000 description 1
- 239000007791 liquid phase Substances 0.000 description 1
- 239000006166 lysate Substances 0.000 description 1
- VZCYOOQTPOCHFL-UPHRSURJSA-N maleic acid Chemical compound OC(=O)\C=C/C(O)=O VZCYOOQTPOCHFL-UPHRSURJSA-N 0.000 description 1
- 239000011976 maleic acid Substances 0.000 description 1
- 230000035800 maturation Effects 0.000 description 1
- 150000002739 metals Chemical class 0.000 description 1
- OETHQSJEHLVLGH-UHFFFAOYSA-N metformin hydrochloride Chemical compound Cl.CN(C)C(=N)N=C(N)N OETHQSJEHLVLGH-UHFFFAOYSA-N 0.000 description 1
- 125000001434 methanylylidene group Chemical group [H]C#[*] 0.000 description 1
- 229930182817 methionine Natural products 0.000 description 1
- 125000002496 methyl group Chemical group [H]C([H])([H])* 0.000 description 1
- 235000019426 modified starch Nutrition 0.000 description 1
- 239000003607 modifier Substances 0.000 description 1
- 150000004682 monohydrates Chemical class 0.000 description 1
- UEGLSOSLURUDIU-UHFFFAOYSA-N n,n-diethyl-1-$l^{1}-selanylmethanimidamide Chemical compound CCN(CC)C([Se])=N UEGLSOSLURUDIU-UHFFFAOYSA-N 0.000 description 1
- KYTZHLUVELPASH-UHFFFAOYSA-N naphthalene-1,2-dicarboxylic acid Chemical compound C1=CC=CC2=C(C(O)=O)C(C(=O)O)=CC=C21 KYTZHLUVELPASH-UHFFFAOYSA-N 0.000 description 1
- KIUJQVAFYAWQDX-UHFFFAOYSA-N naphthalene;1,3-oxazole Chemical class C1=COC=N1.C1=CC=CC2=CC=CC=C21 KIUJQVAFYAWQDX-UHFFFAOYSA-N 0.000 description 1
- 230000007935 neutral effect Effects 0.000 description 1
- 229910017604 nitric acid Inorganic materials 0.000 description 1
- 229910052757 nitrogen Inorganic materials 0.000 description 1
- 238000005457 optimization Methods 0.000 description 1
- 235000019248 orcein Nutrition 0.000 description 1
- 150000007524 organic acids Chemical class 0.000 description 1
- 150000001451 organic peroxides Chemical class 0.000 description 1
- 229910052762 osmium Inorganic materials 0.000 description 1
- SYQBFIAQOQZEGI-UHFFFAOYSA-N osmium atom Chemical compound [Os] SYQBFIAQOQZEGI-UHFFFAOYSA-N 0.000 description 1
- 150000002916 oxazoles Chemical class 0.000 description 1
- WMHSAFDEIXKKMV-UHFFFAOYSA-N oxoantimony;oxotin Chemical group [Sn]=O.[Sb]=O WMHSAFDEIXKKMV-UHFFFAOYSA-N 0.000 description 1
- 238000005192 partition Methods 0.000 description 1
- 230000002093 peripheral effect Effects 0.000 description 1
- 150000002978 peroxides Chemical class 0.000 description 1
- 229940044654 phenolsulfonic acid Drugs 0.000 description 1
- NBIIXXVUZAFLBC-UHFFFAOYSA-K phosphate Chemical compound [O-]P([O-])([O-])=O NBIIXXVUZAFLBC-UHFFFAOYSA-K 0.000 description 1
- 229910052698 phosphorus Inorganic materials 0.000 description 1
- 238000007747 plating Methods 0.000 description 1
- 150000003057 platinum Chemical class 0.000 description 1
- 229920002006 poly(N-vinylimidazole) polymer Polymers 0.000 description 1
- 229920002401 polyacrylamide Polymers 0.000 description 1
- 239000004584 polyacrylic acid Substances 0.000 description 1
- 229920000768 polyamine Polymers 0.000 description 1
- 238000006068 polycondensation reaction Methods 0.000 description 1
- FJVZDOGVDJCCCR-UHFFFAOYSA-M potassium periodate Chemical compound [K+].[O-]I(=O)(=O)=O FJVZDOGVDJCCCR-UHFFFAOYSA-M 0.000 description 1
- 239000012286 potassium permanganate Substances 0.000 description 1
- 229940116357 potassium thiocyanate Drugs 0.000 description 1
- 239000010970 precious metal Substances 0.000 description 1
- 238000004321 preservation Methods 0.000 description 1
- 238000007639 printing Methods 0.000 description 1
- 102000004169 proteins and genes Human genes 0.000 description 1
- 108090000623 proteins and genes Proteins 0.000 description 1
- 238000010926 purge Methods 0.000 description 1
- 150000003222 pyridines Chemical class 0.000 description 1
- HBCQSNAFLVXVAY-UHFFFAOYSA-N pyrimidine-2-thiol Chemical compound SC1=NC=CC=N1 HBCQSNAFLVXVAY-UHFFFAOYSA-N 0.000 description 1
- 150000003233 pyrroles Chemical class 0.000 description 1
- 238000012887 quadratic function Methods 0.000 description 1
- 239000011541 reaction mixture Substances 0.000 description 1
- 230000009467 reduction Effects 0.000 description 1
- 230000008929 regeneration Effects 0.000 description 1
- 238000011069 regeneration method Methods 0.000 description 1
- 230000002441 reversible effect Effects 0.000 description 1
- 229910052702 rhenium Inorganic materials 0.000 description 1
- WUAPFZMCVAUBPE-UHFFFAOYSA-N rhenium atom Chemical compound [Re] WUAPFZMCVAUBPE-UHFFFAOYSA-N 0.000 description 1
- 150000003283 rhodium Chemical class 0.000 description 1
- 229910052703 rhodium Inorganic materials 0.000 description 1
- MHOVAHRLVXNVSD-UHFFFAOYSA-N rhodium atom Chemical compound [Rh] MHOVAHRLVXNVSD-UHFFFAOYSA-N 0.000 description 1
- 229910052701 rubidium Inorganic materials 0.000 description 1
- IGLNJRXAVVLDKE-UHFFFAOYSA-N rubidium atom Chemical compound [Rb] IGLNJRXAVVLDKE-UHFFFAOYSA-N 0.000 description 1
- 150000003303 ruthenium Chemical class 0.000 description 1
- 238000001073 sample cooling Methods 0.000 description 1
- 150000003346 selenoethers Chemical class 0.000 description 1
- IYKVLICPFCEZOF-UHFFFAOYSA-N selenourea Chemical compound NC(N)=[Se] IYKVLICPFCEZOF-UHFFFAOYSA-N 0.000 description 1
- 238000007493 shaping process Methods 0.000 description 1
- 229910000077 silane Inorganic materials 0.000 description 1
- 150000003378 silver Chemical class 0.000 description 1
- LKZMBDSASOBTPN-UHFFFAOYSA-L silver carbonate Substances [Ag].[O-]C([O-])=O LKZMBDSASOBTPN-UHFFFAOYSA-L 0.000 description 1
- 229910001958 silver carbonate Inorganic materials 0.000 description 1
- FJOLTQXXWSRAIX-UHFFFAOYSA-K silver phosphate Chemical compound [Ag+].[Ag+].[Ag+].[O-]P([O-])([O-])=O FJOLTQXXWSRAIX-UHFFFAOYSA-K 0.000 description 1
- RHUVFRWZKMEWNS-UHFFFAOYSA-M silver thiocyanate Chemical compound [Ag+].[S-]C#N RHUVFRWZKMEWNS-UHFFFAOYSA-M 0.000 description 1
- 235000010344 sodium nitrate Nutrition 0.000 description 1
- 239000004317 sodium nitrate Substances 0.000 description 1
- SDKPSXWGRWWLKR-UHFFFAOYSA-M sodium;9,10-dioxoanthracene-1-sulfonate Chemical compound [Na+].O=C1C2=CC=CC=C2C(=O)C2=C1C=CC=C2S(=O)(=O)[O-] SDKPSXWGRWWLKR-UHFFFAOYSA-M 0.000 description 1
- 239000006104 solid solution Substances 0.000 description 1
- 230000003068 static effect Effects 0.000 description 1
- 125000005504 styryl group Chemical group 0.000 description 1
- BDHFUVZGWQCTTF-UHFFFAOYSA-M sulfonate Chemical compound [O-]S(=O)=O BDHFUVZGWQCTTF-UHFFFAOYSA-M 0.000 description 1
- 229910052717 sulfur Inorganic materials 0.000 description 1
- 239000011593 sulfur Substances 0.000 description 1
- UTYXJYFJPBYDKY-UHFFFAOYSA-N tetrapotassium;iron(2+);hexacyanide;trihydrate Chemical compound O.O.O.[K+].[K+].[K+].[K+].[Fe+2].N#[C-].N#[C-].N#[C-].N#[C-].N#[C-].N#[C-] UTYXJYFJPBYDKY-UHFFFAOYSA-N 0.000 description 1
- 125000003831 tetrazolyl group Chemical group 0.000 description 1
- 229910052716 thallium Inorganic materials 0.000 description 1
- BKVIYDNLLOSFOA-UHFFFAOYSA-N thallium Chemical compound [Tl] BKVIYDNLLOSFOA-UHFFFAOYSA-N 0.000 description 1
- 238000007669 thermal treatment Methods 0.000 description 1
- 150000003557 thiazoles Chemical class 0.000 description 1
- CBDKQYKMCICBOF-UHFFFAOYSA-N thiazoline Chemical compound C1CN=CS1 CBDKQYKMCICBOF-UHFFFAOYSA-N 0.000 description 1
- 125000002813 thiocarbonyl group Chemical group *C(*)=S 0.000 description 1
- 238000006365 thiocyanation reaction Methods 0.000 description 1
- 150000003568 thioethers Chemical class 0.000 description 1
- 125000005323 thioketone group Chemical group 0.000 description 1
- VZCYOOQTPOCHFL-UHFFFAOYSA-N trans-butenedioic acid Natural products OC(=O)C=CC(O)=O VZCYOOQTPOCHFL-UHFFFAOYSA-N 0.000 description 1
- 238000012546 transfer Methods 0.000 description 1
- 230000001131 transforming effect Effects 0.000 description 1
- 229910052723 transition metal Inorganic materials 0.000 description 1
- 150000003624 transition metals Chemical class 0.000 description 1
- JOFWLTCLBGQGBO-UHFFFAOYSA-N triazolam Chemical compound C12=CC(Cl)=CC=C2N2C(C)=NN=C2CN=C1C1=CC=CC=C1Cl JOFWLTCLBGQGBO-UHFFFAOYSA-N 0.000 description 1
- 229960003386 triazolam Drugs 0.000 description 1
- XFNJVJPLKCPIBV-UHFFFAOYSA-N trimethylenediamine Chemical class NCCCN XFNJVJPLKCPIBV-UHFFFAOYSA-N 0.000 description 1
- 229910052720 vanadium Inorganic materials 0.000 description 1
- GPPXJZIENCGNKB-UHFFFAOYSA-N vanadium Chemical compound [V]#[V] GPPXJZIENCGNKB-UHFFFAOYSA-N 0.000 description 1
- 230000000007 visual effect Effects 0.000 description 1
- 239000002699 waste material Substances 0.000 description 1
Classifications
-
- G—PHYSICS
- G03—PHOTOGRAPHY; CINEMATOGRAPHY; ANALOGOUS TECHNIQUES USING WAVES OTHER THAN OPTICAL WAVES; ELECTROGRAPHY; HOLOGRAPHY
- G03C—PHOTOSENSITIVE MATERIALS FOR PHOTOGRAPHIC PURPOSES; PHOTOGRAPHIC PROCESSES, e.g. CINE, X-RAY, COLOUR, STEREO-PHOTOGRAPHIC PROCESSES; AUXILIARY PROCESSES IN PHOTOGRAPHY
- G03C7/00—Multicolour photographic processes or agents therefor; Regeneration of such processing agents; Photosensitive materials for multicolour processes
- G03C7/30—Colour processes using colour-coupling substances; Materials therefor; Preparing or processing such materials
- G03C7/3022—Materials with specific emulsion characteristics, e.g. thickness of the layers, silver content, shape of AgX grains
-
- G—PHYSICS
- G03—PHOTOGRAPHY; CINEMATOGRAPHY; ANALOGOUS TECHNIQUES USING WAVES OTHER THAN OPTICAL WAVES; ELECTROGRAPHY; HOLOGRAPHY
- G03C—PHOTOSENSITIVE MATERIALS FOR PHOTOGRAPHIC PURPOSES; PHOTOGRAPHIC PROCESSES, e.g. CINE, X-RAY, COLOUR, STEREO-PHOTOGRAPHIC PROCESSES; AUXILIARY PROCESSES IN PHOTOGRAPHY
- G03C1/00—Photosensitive materials
- G03C1/005—Silver halide emulsions; Preparation thereof; Physical treatment thereof; Incorporation of additives therein
- G03C1/0051—Tabular grain emulsions
- G03C2001/0055—Aspect ratio of tabular grains in general; High aspect ratio; Intermediate aspect ratio; Low aspect ratio
-
- G—PHYSICS
- G03—PHOTOGRAPHY; CINEMATOGRAPHY; ANALOGOUS TECHNIQUES USING WAVES OTHER THAN OPTICAL WAVES; ELECTROGRAPHY; HOLOGRAPHY
- G03C—PHOTOSENSITIVE MATERIALS FOR PHOTOGRAPHIC PURPOSES; PHOTOGRAPHIC PROCESSES, e.g. CINE, X-RAY, COLOUR, STEREO-PHOTOGRAPHIC PROCESSES; AUXILIARY PROCESSES IN PHOTOGRAPHY
- G03C2200/00—Details
- G03C2200/03—111 crystal face
Landscapes
- Physics & Mathematics (AREA)
- General Physics & Mathematics (AREA)
- Silver Salt Photography Or Processing Solution Therefor (AREA)
- Non-Silver Salt Photosensitive Materials And Non-Silver Salt Photography (AREA)
Abstract
Description
步骤 | 处理时间 | 处理温度 |
彩色显影 | 1分钟 | 38℃ |
停显(stop) | 30秒 | 20℃ |
对-N-甲氨基苯酚磺酸酯 | 2.5克 |
L-抗坏血酸 | 10.0克 |
偏硼酸钠四水合物 | 3.5克 |
KBr | 1.0克 |
水 | 1升 |
乳剂 | 片状颗粒的平均ESD(Dsp)(微米) | 纵横比(AR) | 占据总颗粒50%或更多的颗粒的形状 | 位于颗粒内部的断层线 | Ir的加入量(摩尔/摩尔银) | Rh的加入量(摩尔/摩尔银) | 用溶解刀片高速搅拌 |
1-A | 0.92 | 4.1 | Dsp≥0.8微米且AR≥2 | 无 | 0 | 0 | 未进行 |
1-B | 0.92 | 4.1 | Dsp≥0.8微米且AR≥2 | 有 | 2×10-7 | 6.4×10-8 | 进行 |
1-C | 0.92 | 9.3 | Dsp≥0.8微米且AR≥8 | 无 | 0 | 0 | 未进行 |
1-D | 0.92 | 9.3 | Dsp≥0.8微米且AR≥8 | 有 | 2×10-7 | 6.4×10-8 | 进行 |
1-E | 0.92 | 15.4 | Dsp≥0.8微米且AR≥13 | 无 | 0 | 0 | 未进行 |
1-F | 0.92 | 15.4 | Dsp≥0.8微米且AR≥13 | 有 | 2×10-7 | 6.4×10-8 | 进行 |
1-G | 0.92 | 23.4 | Dsp≥0.8微米且AR≥20 | 无 | 0 | 0 | 未进行 |
1-H | 0.92 | 23.4 | Dsp≥0.8微米且AR≥20 | 有 | 2×10-7 | 6.4×10-8 | 进行 |
1-I | 1.49 | 4.3 | Dsp≥1.0微米且AR≥2 | 无 | 0 | 0 | 未进行 |
1-J | 1.49 | 4.3 | Dsp≥1.0微米且AR≥2 | 有 | 2×10-7 | 6.4×10-8 | 进行 |
1-K | 1.49 | 9.1 | Dsp≥1.0微米且AR≥8 | 无 | 0 | 0 | 未进行 |
1-L | 1.49 | 9.1 | Dsp≥1.0微米且AR≥8 | 有 | 2×10-7 | 6.4×10-8 | 进行 |
1-M | 1.49 | 13.1 | Dsp≥1.0微米且AR≥13 | 无 | 0 | 0 | 未进行 |
1-N | 1.49 | 13.1 | Dsp≥1.0微米且AR≥13 | 有 | 2×10-7 | 6.4×10-8 | 进行 |
1-O | 1.49 | 26.6 | Dsp≥1.0微米且AR≥20 | 无 | 0 | 0 | 未进行 |
1-P | 1.49 | 26.6 | Dsp≥1.0微米且AR≥20 | 有 | 0 | 0 | 未进行 |
1-Q | 1.49 | 26.6 | Dsp≥1.0微米且AR≥20 | 有 | 2×10-7 | 0 | 未进行 |
1-R | 1.49 | 26.6 | Dsp≥1.0微米且AR≥20 | 有 | 2×10-7 | 6.4×10-8 | 未进行 |
1-S | 1.49 | 26.6 | Dsp≥1.0微米且AR≥20 | 有 | 2×10-7 | 6.4×10-8 | 进行 |
试样 | 乳剂 | 每个颗粒具有两个或多个显影起始点的卤化银颗粒的数目/每个颗粒具有一个或多个显影起始点的卤化银颗粒的数目(%) | A | B | AB | 照射时的RMS颗粒度 | 标记 |
相对感度 | 由辐射造成的灰雾增加值 | ||||||
101 | 1-A | 49 | 100 | 100 | 1.00 | 100 | 对比例 |
102 | 1-B | 34 | 102 | 95 | 1.07 | 98 | 本发明 |
103 | 1-C | 54 | 120 | 126 | 0.95 | 102 | 对比例 |
104 | 1-D | 32 | 123 | 115 | 1.07 | 93 | 本发明 |
105 | 1-E | 56 | 141 | 151 | 0.93 | 105 | 对比例 |
106 | 1-F | 31 | 145 | 132 | 1.10 | 91 | 本发明 |
107 | 1-G | 61 | 174 | 191 | 0.91 | 107 | 对比例 |
108 | 1-H | 30 | 174 | 158 | 1.10 | 87 | 本发明 |
109 | 1-J | 57 | 155 | 174 | 0.89 | 179 | 对比例 |
110 | 1-J | 33 | 158 | 141 | 1.12 | 151 | 本发明 |
111 | 1-K | 66 | 209 | 234 | 0.89 | 190 | 对比例 |
112 | 1-L | 29 | 214 | 186 | 1.15 | 141 | 本发明 |
113 | 1-M | 68 | 251 | 288 | 0.87 | 204 | 对比例 |
114 | 1-N | 27 | 257 | 224 | 1.15 | 134 | 本发明 |
115 | 1-O | 70 | 372 | 437 | 0.85 | 214 | 对比例 |
116 | 1-P | 44 | 372 | 355 | 1.05 | 167 | 本发明 |
117 | 1-Q | 39 | 380 | 339 | 1.12 | 151 | 本发明 |
118 | 1-R | 32 | 372 | 316 | 1.18 | 138 | 本发明 |
119 | 1-S | 23 | 380 | 302 | 1.26 | 126 | 本发明 |
乳剂 | ECC(微米)COV(%) | Th(微米)COV(%) | 长宽比COV(%) | 平板度 | 双晶面距离COV(%) | 具有(111)主面的片状颗粒占投影总面积的比率(%) | 侧面中的(100)晶面的比率(%) | 碘化银含量(mol%)COV(%) | 氯化银含量(mol%) | 表面碘化银含量(mol%) | |
A | 1.9823 | 0.19828 | 1035 | 51 | 0.01432 | 92 | 23 | 1517 | 0 | 4.3 | |
B | 1.3025 | 0.10827 | 1238 | 111 | 0.01330 | 93 | 22 | 1116 | 0 | 3.6 | |
C | 1.0027 | 0.08326 | 1237 | 145 | 0.01230 | 93 | 18 | 48 | 1 | 1.8 | |
D | 0.7531 | 0.07518 | 1029 | 133 | 0.01027 | 91 | 33 | 48 | 2 | 1.9 | |
E | 1.5426 | 0.0718 | 2033 | 260 | 0.01326 | 99 | 23 | 8.48 | 0 | 6.2 | |
F | 1.0818 | 0.07215 | 1519 | 208 | 0.00822 | 97 | 23 | 65 | 0 | 2.0 | |
G | 0.4416 | 0.22013 | 29 | 9 | 0.01318 | 90 | 38 | 36 | 2 | 1.0 | |
H | 0.3317 | 0.16513 | 212 | 12 | 0.01318 | 88 | 42 | 36 | 2 | 1.0 | |
I | 2.2531 | 0.10719 | 2134 | 197 | 0.01333 | 99 | 20 | 7.27 | 0 | 2.4 | |
J | 2.3820 | 0.13820 | 1723 | 125 | 0.01319 | 98 | 23 | 56 | 1 | 1.6 | |
K | 1.8318 | 0.12220 | 1522 | 123 | 0.01219 | 98 | 23 | 56 | 1 | 1.8 | |
L | 0.8417 | 0.12018 | 719 | 58 | 0.01316 | 99 | 25 | 37 | 0 | 2.7 | |
M | 0.4417 | 0.22013 | 212 | 9 | 0.01318 | 88 | 42 | 26 | 2 | 1.0 | |
N | 0.3317 | 0.16513 | 212 | 12 | 0.01318 | 88 | 46 | 16 | 2 | 0.5 | |
O | 0.07- | 0.070- | 1- | - | -- | - | - | 1- | 0 | - | |
P | 0.07- | 0.070- | 1- | - | - | - | - | 0.9- | 0 | - |
试样 | 乳剂 | 具有两个或多个显影起始点的颗粒数目/具有一个或多个显影起始点的颗粒数目(%) | A | B | A/B | 辐射时的RMS颗粒度 | 标记 |
相对感度 | 由辐射造成的灰雾增加值 | ||||||
201 | 1-E | 57 | 100 | 100 | 1.00 | 100 | 对比例 |
202 | 1-F | 32 | 102 | 89 | 1.15 | 85 | 本发明 |
203 | 1-G | 63 | 123 | 129 | 0.95 | 105 | 对比例 |
204 | 1-H | 33 | 123 | 107 | 1.15 | 79 | 本发明 |
205 | 1-M | 69 | 178 | 195 | 0.91 | 199 | 对比例 |
206 | 1-N | 28 | 182 | 148 | 1.23 | 122 | 本发明 |
207 | 1-O | 71 | 263 | 295 | 0.89 | 214 | 对比例 |
208 | 1-P | 45 | 269 | 229 | 1.17 | 162 | 本发明 |
209 | 1-Q | 41 | 263 | 219 | 1.20 | 138 | 本发明 |
210 | 1-R | 35 | 263 | 200 | 1.32 | 126 | 本发明 |
211 | 1-S | 25 | 269 | 191 | 1.41 | 116 | 本发明 |
Claims (6)
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JP2000294852A JP2002107863A (ja) | 2000-09-27 | 2000-09-27 | ハロゲン化銀写真感光材料 |
JP2000294852 | 2000-09-27 |
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Publication Number | Publication Date |
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CN1346073A CN1346073A (zh) | 2002-04-24 |
CN1287218C true CN1287218C (zh) | 2006-11-29 |
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CNB011384069A Expired - Fee Related CN1287218C (zh) | 2000-09-27 | 2001-09-27 | 卤化银照相光敏材料 |
Country Status (3)
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US (1) | US6524783B2 (zh) |
JP (1) | JP2002107863A (zh) |
CN (1) | CN1287218C (zh) |
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GB9611272D0 (en) | 1996-05-30 | 1996-07-31 | Kodak Ltd | Colour negative photographic silver halide materials |
GB9828152D0 (en) | 1998-12-22 | 1999-02-17 | Eastman Kodak Co | Reduction of the sensitivity of photograhic emulsions to ionising radiation |
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JP2002107863A (ja) | 2002-04-10 |
US6524783B2 (en) | 2003-02-25 |
CN1346073A (zh) | 2002-04-24 |
US20020076665A1 (en) | 2002-06-20 |
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