CN118475587A - 通过氢化硅烷化制备3-卤代丙基三卤代硅烷的方法 - Google Patents

通过氢化硅烷化制备3-卤代丙基三卤代硅烷的方法 Download PDF

Info

Publication number
CN118475587A
CN118475587A CN202280081384.7A CN202280081384A CN118475587A CN 118475587 A CN118475587 A CN 118475587A CN 202280081384 A CN202280081384 A CN 202280081384A CN 118475587 A CN118475587 A CN 118475587A
Authority
CN
China
Prior art keywords
silane
unsaturated compound
catalyst
reaction
trihalosilane
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN202280081384.7A
Other languages
English (en)
Chinese (zh)
Inventor
N·马里恩
H·默奇
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Evonik Operations GmbH
Original Assignee
Evonik Operations GmbH
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Evonik Operations GmbH filed Critical Evonik Operations GmbH
Publication of CN118475587A publication Critical patent/CN118475587A/zh
Pending legal-status Critical Current

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07FACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
    • C07F7/00Compounds containing elements of Groups 4 or 14 of the Periodic Table
    • C07F7/02Silicon compounds
    • C07F7/08Compounds having one or more C—Si linkages
    • C07F7/12Organo silicon halides
    • C07F7/14Preparation thereof from optionally substituted halogenated silanes and hydrocarbons hydrosilylation reactions
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J31/00Catalysts comprising hydrides, coordination complexes or organic compounds
    • B01J31/02Catalysts comprising hydrides, coordination complexes or organic compounds containing organic compounds or metal hydrides
    • B01J31/0234Nitrogen-, phosphorus-, arsenic- or antimony-containing compounds
    • B01J31/0235Nitrogen containing compounds
    • B01J31/0237Amines
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J31/00Catalysts comprising hydrides, coordination complexes or organic compounds
    • B01J31/02Catalysts comprising hydrides, coordination complexes or organic compounds containing organic compounds or metal hydrides
    • B01J31/0234Nitrogen-, phosphorus-, arsenic- or antimony-containing compounds
    • B01J31/0235Nitrogen containing compounds
    • B01J31/0245Nitrogen containing compounds being derivatives of carboxylic or carbonic acids
    • B01J31/0247Imides, amides or imidates (R-C=NR(OR))
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J31/00Catalysts comprising hydrides, coordination complexes or organic compounds
    • B01J31/16Catalysts comprising hydrides, coordination complexes or organic compounds containing coordination complexes
    • B01J31/1608Catalysts comprising hydrides, coordination complexes or organic compounds containing coordination complexes the ligands containing silicon
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J31/00Catalysts comprising hydrides, coordination complexes or organic compounds
    • B01J31/16Catalysts comprising hydrides, coordination complexes or organic compounds containing coordination complexes
    • B01J31/22Organic complexes
    • B01J31/2282Unsaturated compounds used as ligands
    • B01J31/2291Olefins
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08GMACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G77/00Macromolecular compounds obtained by reactions forming a linkage containing silicon with or without sulfur, nitrogen, oxygen or carbon in the main chain of the macromolecule
    • C08G77/04Polysiloxanes
    • C08G77/12Polysiloxanes containing silicon bound to hydrogen
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08GMACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G77/00Macromolecular compounds obtained by reactions forming a linkage containing silicon with or without sulfur, nitrogen, oxygen or carbon in the main chain of the macromolecule
    • C08G77/04Polysiloxanes
    • C08G77/20Polysiloxanes containing silicon bound to unsaturated aliphatic groups
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08LCOMPOSITIONS OF MACROMOLECULAR COMPOUNDS
    • C08L83/00Compositions of macromolecular compounds obtained by reactions forming in the main chain of the macromolecule a linkage containing silicon with or without sulfur, nitrogen, oxygen or carbon only; Compositions of derivatives of such polymers
    • C08L83/04Polysiloxanes
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2231/00Catalytic reactions performed with catalysts classified in B01J31/00
    • B01J2231/30Addition reactions at carbon centres, i.e. to either C-C or C-X multiple bonds
    • B01J2231/32Addition reactions to C=C or C-C triple bonds
    • B01J2231/323Hydrometalation, e.g. bor-, alumin-, silyl-, zirconation or analoguous reactions like carbometalation, hydrocarbation
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2531/00Additional information regarding catalytic systems classified in B01J31/00
    • B01J2531/02Compositional aspects of complexes used, e.g. polynuclearity
    • B01J2531/0202Polynuclearity
    • B01J2531/0205Bi- or polynuclear complexes, i.e. comprising two or more metal coordination centres, without metal-metal bonds, e.g. Cp(Lx)Zr-imidazole-Zr(Lx)Cp
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2531/00Additional information regarding catalytic systems classified in B01J31/00
    • B01J2531/80Complexes comprising metals of Group VIII as the central metal
    • B01J2531/82Metals of the platinum group
    • B01J2531/828Platinum

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Inorganic Chemistry (AREA)
  • Health & Medical Sciences (AREA)
  • Medicinal Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
CN202280081384.7A 2021-12-08 2022-11-28 通过氢化硅烷化制备3-卤代丙基三卤代硅烷的方法 Pending CN118475587A (zh)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
EP21213073.6A EP4194462B1 (en) 2021-12-08 2021-12-08 Method of making 3-halopropyltrihalosilanes by hydrosilylation
EP21213073.6 2021-12-08
PCT/EP2022/083399 WO2023104560A1 (en) 2021-12-08 2022-11-28 Method of making 3-halopropyltrihalosilanes by hydrosilylation

Publications (1)

Publication Number Publication Date
CN118475587A true CN118475587A (zh) 2024-08-09

Family

ID=78824776

Family Applications (1)

Application Number Title Priority Date Filing Date
CN202280081384.7A Pending CN118475587A (zh) 2021-12-08 2022-11-28 通过氢化硅烷化制备3-卤代丙基三卤代硅烷的方法

Country Status (6)

Country Link
US (1) US20250034179A1 (https=)
EP (1) EP4194462B1 (https=)
JP (1) JP2024542891A (https=)
CN (1) CN118475587A (https=)
ES (1) ES3057127T3 (https=)
WO (1) WO2023104560A1 (https=)

Families Citing this family (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP4112674A1 (de) 2021-06-30 2023-01-04 Evonik Operations GmbH Verfahren zur herstellung hochreiner hydrosilylierungsprodukte

Family Cites Families (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE1156073B (de) 1962-06-29 1963-10-24 Goldschmidt Ag Th Verfahren zur Herstellung von siliciumhaltigen Kohlenwasserstoffverbindungen
US3925434A (en) 1975-01-22 1975-12-09 Union Carbide Corp The reaction of chlorosilanes with unsaturated organic compounds
DE3000768A1 (de) 1980-01-10 1981-07-16 Wacker-Chemie GmbH, 8000 München Verfahren zum anlagern von si-gebundenem wasserstoff an aliphatische mehrfachbindung
DE10243180A1 (de) 2001-10-10 2003-04-24 Degussa Verfahren zur Hydrosilylierung ungesättigter aliphatischer Verbindungen
CN102127104B (zh) * 2010-12-04 2013-07-31 郭学阳 一种γ-氯丙基三氯硅烷的生产方法
CN108069996B (zh) 2016-11-18 2020-03-06 荆州市江汉精细化工有限公司 生产氯丙基三氯硅烷的方法
CN113444122A (zh) * 2020-03-24 2021-09-28 新特能源股份有限公司 一种γ-氯丙基三氯硅烷的连续生产工艺与装置

Also Published As

Publication number Publication date
EP4194462A1 (en) 2023-06-14
US20250034179A1 (en) 2025-01-30
WO2023104560A1 (en) 2023-06-15
ES3057127T3 (en) 2026-02-26
EP4194462B1 (en) 2025-10-15
JP2024542891A (ja) 2024-11-18

Similar Documents

Publication Publication Date Title
JPH03197484A (ja) 水素シロキサンの製造方法
JPH10130278A (ja) フルオロアルキル基含有有機ケイ素化合物及びこれから成る織物用助剤、表面加工剤及び建築物保護剤並びにこれらを含有する相応する組成物
JP5360736B2 (ja) Si−Si結合を有する化合物の製造方法
JPH0353317B2 (https=)
EP3186262B1 (en) Fluorosilicon nitrile compounds
US10329313B2 (en) Organosilicon compounds having (meth)acrylate groups and a process for preparation thereof
CN118475587A (zh) 通过氢化硅烷化制备3-卤代丙基三卤代硅烷的方法
EP1241171B1 (en) Preparation of branched siloxanes
US4469881A (en) [2-(p-t-Butylphenyl)ethyl]silanes and method of making the same
CN1298725C (zh) 制备苯基有机硅中间体的方法
JPH05239073A (ja) けい素化合物の塩素化方法
JP4216354B2 (ja) ヒドロシリル化方法
US6521774B2 (en) Organosilicon compounds
JP6598406B2 (ja) イリジウム錯体等を用いたアリル化合物のヒドロシリル化によるシリル化合物の製造方法
US20030233005A1 (en) Preparation of organosilicon intermediate and their derivatives in a novel grignard process
EP3684777A1 (en) Process for the production of organohydridochlorosilanes
JP7488265B2 (ja) 官能性有機シラノール化合物を調製する方法
JPS63107943A (ja) 芳香族イミドのシリル化法および生成したシリルイミド
KR20050057614A (ko) 백금 비함유 순수 구리 함유 촉매를 사용한 하이드로실릴화방법
JP7350253B2 (ja) ビスハロアルキルシロキサン化合物及びその製造方法、並びに、両末端官能性のシロキサン化合物の製造方法
KR100469945B1 (ko) 비닐클로로실란의제조방법
JPH01113395A (ja) アルキルハロシラン中のオレフィン含有量の低減方法
JP3445322B2 (ja) 長鎖n−アルキル基含有シランの製造方法
JP4279066B2 (ja) 環状シロキサン化合物及びその製造方法
JPH0210837B2 (https=)

Legal Events

Date Code Title Description
PB01 Publication
PB01 Publication
SE01 Entry into force of request for substantive examination
SE01 Entry into force of request for substantive examination