CN116157937A - 制造微粒(氧)氢氧化物的方法和微粒(氧)氢氧化物及其用途 - Google Patents

制造微粒(氧)氢氧化物的方法和微粒(氧)氢氧化物及其用途 Download PDF

Info

Publication number
CN116157937A
CN116157937A CN202180060026.3A CN202180060026A CN116157937A CN 116157937 A CN116157937 A CN 116157937A CN 202180060026 A CN202180060026 A CN 202180060026A CN 116157937 A CN116157937 A CN 116157937A
Authority
CN
China
Prior art keywords
hydroxide
range
solution
oxy
particulate
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN202180060026.3A
Other languages
English (en)
Chinese (zh)
Inventor
B·J·H·伯格纳
R·B·伯克
L·K·B·加尔弗
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
BASF SE
Original Assignee
BASF SE
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by BASF SE filed Critical BASF SE
Publication of CN116157937A publication Critical patent/CN116157937A/zh
Pending legal-status Critical Current

Links

Images

Classifications

    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01GCOMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
    • C01G53/00Compounds of nickel
    • C01G53/80Compounds containing nickel, with or without oxygen or hydrogen, and containing one or more other elements
    • C01G53/82Compounds containing nickel, with or without oxygen or hydrogen, and containing two or more other elements
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01GCOMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
    • C01G53/00Compounds of nickel
    • C01G53/40Complex oxides containing nickel and at least one other metal element
    • C01G53/42Complex oxides containing nickel and at least one other metal element containing alkali metals, e.g. LiNiO2
    • C01G53/44Complex oxides containing nickel and at least one other metal element containing alkali metals, e.g. LiNiO2 containing manganese
    • HELECTRICITY
    • H01ELECTRIC ELEMENTS
    • H01MPROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M4/00Electrodes
    • H01M4/02Electrodes composed of, or comprising, active material
    • H01M4/36Selection of substances as active materials, active masses, active liquids
    • H01M4/48Selection of substances as active materials, active masses, active liquids of inorganic oxides or hydroxides
    • H01M4/50Selection of substances as active materials, active masses, active liquids of inorganic oxides or hydroxides of manganese
    • H01M4/505Selection of substances as active materials, active masses, active liquids of inorganic oxides or hydroxides of manganese of mixed oxides or hydroxides containing manganese for inserting or intercalating light metals, e.g. LiMn2O4 or LiMn2OxFy
    • HELECTRICITY
    • H01ELECTRIC ELEMENTS
    • H01MPROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M4/00Electrodes
    • H01M4/02Electrodes composed of, or comprising, active material
    • H01M4/36Selection of substances as active materials, active masses, active liquids
    • H01M4/48Selection of substances as active materials, active masses, active liquids of inorganic oxides or hydroxides
    • H01M4/52Selection of substances as active materials, active masses, active liquids of inorganic oxides or hydroxides of nickel, cobalt or iron
    • H01M4/525Selection of substances as active materials, active masses, active liquids of inorganic oxides or hydroxides of nickel, cobalt or iron of mixed oxides or hydroxides containing iron, cobalt or nickel for inserting or intercalating light metals, e.g. LiNiO2, LiCoO2 or LiCoOxFy
    • HELECTRICITY
    • H01ELECTRIC ELEMENTS
    • H01MPROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M4/00Electrodes
    • H01M4/02Electrodes composed of, or comprising, active material
    • H01M4/62Selection of inactive substances as ingredients for active masses, e.g. binders, fillers
    • H01M4/621Binders
    • H01M4/622Binders being polymers
    • H01M4/623Binders being polymers fluorinated polymers
    • HELECTRICITY
    • H01ELECTRIC ELEMENTS
    • H01MPROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M4/00Electrodes
    • H01M4/02Electrodes composed of, or comprising, active material
    • H01M4/62Selection of inactive substances as ingredients for active masses, e.g. binders, fillers
    • H01M4/624Electric conductive fillers
    • H01M4/625Carbon or graphite
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01PINDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2002/00Crystal-structural characteristics
    • C01P2002/50Solid solutions
    • C01P2002/52Solid solutions containing elements as dopants
    • C01P2002/54Solid solutions containing elements as dopants one element only
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01PINDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00Particle morphology
    • C01P2004/01Particle morphology depicted by an image
    • C01P2004/03Particle morphology depicted by an image obtained by SEM
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01PINDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00Particle morphology
    • C01P2004/50Agglomerated particles
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01PINDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00Particle morphology
    • C01P2004/51Particles with a specific particle size distribution
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01PINDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00Particle morphology
    • C01P2004/51Particles with a specific particle size distribution
    • C01P2004/53Particles with a specific particle size distribution bimodal size distribution
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01PINDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00Particle morphology
    • C01P2004/54Particles characterised by their aspect ratio, i.e. the ratio of sizes in the longest to the shortest dimension
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01PINDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00Particle morphology
    • C01P2004/60Particles characterised by their size
    • C01P2004/61Micrometer sized, i.e. from 1-100 micrometer
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01PINDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2006/00Physical properties of inorganic compounds
    • C01P2006/40Electric properties
    • HELECTRICITY
    • H01ELECTRIC ELEMENTS
    • H01MPROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M4/00Electrodes
    • H01M4/02Electrodes composed of, or comprising, active material
    • H01M2004/021Physical characteristics, e.g. porosity, surface area
    • HELECTRICITY
    • H01ELECTRIC ELEMENTS
    • H01MPROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M4/00Electrodes
    • H01M4/02Electrodes composed of, or comprising, active material
    • H01M2004/026Electrodes composed of, or comprising, active material characterised by the polarity
    • H01M2004/028Positive electrodes
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02EREDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
    • Y02E60/00Enabling technologies; Technologies with a potential or indirect contribution to GHG emissions mitigation
    • Y02E60/10Energy storage using batteries

Landscapes

  • Chemical & Material Sciences (AREA)
  • Inorganic Chemistry (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Electrochemistry (AREA)
  • General Chemical & Material Sciences (AREA)
  • Inorganic Compounds Of Heavy Metals (AREA)
  • Battery Electrode And Active Subsutance (AREA)
CN202180060026.3A 2020-10-13 2021-09-16 制造微粒(氧)氢氧化物的方法和微粒(氧)氢氧化物及其用途 Pending CN116157937A (zh)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
EP20201539 2020-10-13
EP20201539.2 2020-10-13
PCT/EP2021/075441 WO2022078702A1 (en) 2020-10-13 2021-09-16 Process for making a particulate (oxy)hydroxide, and particulate (oxy)hydroxide and its use

Publications (1)

Publication Number Publication Date
CN116157937A true CN116157937A (zh) 2023-05-23

Family

ID=72852464

Family Applications (1)

Application Number Title Priority Date Filing Date
CN202180060026.3A Pending CN116157937A (zh) 2020-10-13 2021-09-16 制造微粒(氧)氢氧化物的方法和微粒(氧)氢氧化物及其用途

Country Status (10)

Country Link
US (1) US12570545B2 (https=)
EP (1) EP4229008B1 (https=)
JP (1) JP7818586B2 (https=)
KR (1) KR20230085913A (https=)
CN (1) CN116157937A (https=)
CA (1) CA3194883A1 (https=)
ES (1) ES2988547T3 (https=)
FI (1) FI4229008T3 (https=)
PL (1) PL4229008T3 (https=)
WO (1) WO2022078702A1 (https=)

Families Citing this family (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN117003295B (zh) * 2022-04-29 2025-12-12 中伟新材料股份有限公司 一种三元正极材料及其前驱体、锂离子电池
US20260028242A1 (en) * 2022-08-15 2026-01-29 Basf Se Process for making an (oxy)hydroxide, and (oxy)hydroxide
EP4649057A1 (en) * 2023-01-11 2025-11-19 Basf Se Process for making a particulate (oxy)hydroxide or oxide, particulate (oxy)hydroxide or oxide and use
WO2025016808A1 (en) * 2023-07-14 2025-01-23 Basf Se Process for making precursors of cathode active materials, and precursors

Family Cites Families (19)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP3192374B2 (ja) 1996-07-01 2001-07-23 正同化学工業株式会社 水酸化ニッケルの製造方法
US6660432B2 (en) 2000-09-14 2003-12-09 Ilion Technology Corporation Lithiated oxide materials and methods of manufacture
DE102007049108A1 (de) 2007-10-12 2009-04-16 H.C. Starck Gmbh Pulverförmige Verbindungen, Verfahren zu deren Herstellung sowie deren Verwendung in Batterien
CN103282310B (zh) 2011-01-10 2015-04-29 巴斯夫欧洲公司 制备过渡金属氢氧化物的方法
CN104114494B (zh) 2012-02-08 2016-09-28 巴斯夫欧洲公司 制备可包含氢氧化物的混合碳酸盐的方法
JP2013180917A (ja) 2012-03-01 2013-09-12 Nippon Chem Ind Co Ltd ニッケル含有水酸化物及びその製造方法
TWI636613B (zh) * 2013-07-18 2018-09-21 日商東曹股份有限公司 鎳-錳系複合氧氫氧化物及其製造方法、以及其用途
JP6357928B2 (ja) 2013-07-18 2018-07-18 東ソー株式会社 ニッケル−マンガン系複合オキシ水酸化物及びその製造方法、並びにその用途
CN104157873A (zh) 2014-08-04 2014-11-19 北京万源工业有限公司 一种利用聚合反应制备改性磷酸铁锂的方法
CN104157872A (zh) 2014-08-26 2014-11-19 宁波金和新材料股份有限公司 低成本高容量倍率型镍锰前驱体及其制备方法、正极材料
JP6265117B2 (ja) 2014-12-22 2018-01-24 住友金属鉱山株式会社 ニッケルコバルトマンガン複合水酸化物とその製造方法
JP6665634B2 (ja) 2016-03-30 2020-03-13 東ソー株式会社 ニッケル−マンガン複合オキシ水酸化物の製造方法
US11476460B2 (en) 2016-07-29 2022-10-18 Sumitomo Metal Mining Co., Ltd. Nickel manganese composite hydroxide and method for producing same, positive electrode active material for nonaqueous electrolyte secondary battery and method for producing same, and nonaqueous electrolyte secondary battery
JP7215169B2 (ja) 2016-07-29 2023-01-31 住友金属鉱山株式会社 ニッケルマンガン複合水酸化物とその製造方法、非水系電解質二次電池用正極活物質とその製造方法、および非水系電解質二次電池
KR102521605B1 (ko) 2018-03-02 2023-04-12 유미코아 재충전가능 리튬 이온 배터리용 양극 물질
WO2020094482A1 (en) * 2018-11-09 2020-05-14 Basf Se Process for making a nickel composite hydroxide
WO2021080374A1 (ko) 2019-10-23 2021-04-29 주식회사 엘지화학 양극 활물질 전구체의 제조 방법 및 양극 활물질 전구체
CN112777647B (zh) 2019-11-04 2023-04-07 巴斯夫杉杉电池材料有限公司 一种窄粒径分布高镍氢氧化物及其制备方法
WO2021154021A1 (ko) 2020-01-29 2021-08-05 주식회사 엘지화학 이차전지용 양극 활물질 전구체, 양극 활물질 및 이를 포함하는 리튬 이차전지

Also Published As

Publication number Publication date
US20230406722A1 (en) 2023-12-21
ES2988547T3 (es) 2024-11-21
US12570545B2 (en) 2026-03-10
JP7818586B2 (ja) 2026-02-20
EP4229008B1 (en) 2024-07-24
PL4229008T3 (pl) 2024-11-25
CA3194883A1 (en) 2022-04-21
KR20230085913A (ko) 2023-06-14
WO2022078702A1 (en) 2022-04-21
FI4229008T3 (fi) 2024-10-25
JP2023550011A (ja) 2023-11-30
EP4229008A1 (en) 2023-08-23

Similar Documents

Publication Publication Date Title
JP7818586B2 (ja) 粒子状(オキシ)水酸化物の製造方法、粒子状(オキシ)水酸化物及びその使用方法
EP4263435B1 (en) Process for making an electrode active material, and electrode active material
JP7638966B2 (ja) 粒子状物質、その製造方法及び使用方法
EP4149889B1 (en) Process for making a particulate (oxy)hydroxide, and electrode active material made therefrom
US12401034B2 (en) Multi-step process for making cathode active materials, and cathode active materials
JP2025510202A (ja) ドープされたカソード活物質の製造方法
JP2023547996A (ja) ドープされたカソード活物質の製造方法
EP4095102A1 (en) Process for making a particulate electrode active material, and electrode active material
US20260028242A1 (en) Process for making an (oxy)hydroxide, and (oxy)hydroxide
EP4281415B1 (en) Process for making a particulate (oxy)hydroxide
EP4649057A1 (en) Process for making a particulate (oxy)hydroxide or oxide, particulate (oxy)hydroxide or oxide and use
WO2025078192A1 (en) Method of making a precursor for a cathode active material
CN121443558A (zh) 用于制造阴极活性材料及其前体的方法
WO2026008399A1 (en) Process for making a particulate (oxy)hydroxide or oxide, particulate (oxy)hydroxide and use
JP2026513924A (ja) リチウムイオン電池用カソード活物質、およびその製造方法
JP2024502936A (ja) 電極活物質の製造方法

Legal Events

Date Code Title Description
PB01 Publication
PB01 Publication
SE01 Entry into force of request for substantive examination
SE01 Entry into force of request for substantive examination