CN115721590B - Black-removing pouch powder and preparation process thereof - Google Patents
Black-removing pouch powder and preparation process thereof Download PDFInfo
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- CN115721590B CN115721590B CN202211563313.9A CN202211563313A CN115721590B CN 115721590 B CN115721590 B CN 115721590B CN 202211563313 A CN202211563313 A CN 202211563313A CN 115721590 B CN115721590 B CN 115721590B
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- 239000000843 powder Substances 0.000 title claims abstract description 69
- 238000002360 preparation method Methods 0.000 title claims description 11
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims abstract description 70
- 239000012071 phase Substances 0.000 claims abstract description 45
- 240000005546 Piper methysticum Species 0.000 claims abstract description 40
- 235000016787 Piper methysticum Nutrition 0.000 claims abstract description 40
- 235000011389 fruit/vegetable juice Nutrition 0.000 claims abstract description 39
- 239000000377 silicon dioxide Substances 0.000 claims abstract description 35
- 244000061456 Solanum tuberosum Species 0.000 claims abstract description 31
- 235000002595 Solanum tuberosum Nutrition 0.000 claims abstract description 31
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 28
- 235000007516 Chrysanthemum Nutrition 0.000 claims abstract description 25
- GWEVSGVZZGPLCZ-UHFFFAOYSA-N Titan oxide Chemical compound O=[Ti]=O GWEVSGVZZGPLCZ-UHFFFAOYSA-N 0.000 claims abstract description 12
- 239000008346 aqueous phase Substances 0.000 claims abstract description 11
- ANZUDYZHSVGBRF-UHFFFAOYSA-N 3-ethylnonane-1,2,3-triol Chemical compound CCCCCCC(O)(CC)C(O)CO ANZUDYZHSVGBRF-UHFFFAOYSA-N 0.000 claims abstract description 8
- 239000003974 emollient agent Substances 0.000 claims abstract description 8
- 239000003906 humectant Substances 0.000 claims abstract description 8
- QCDWFXQBSFUVSP-UHFFFAOYSA-N 2-phenoxyethanol Chemical compound OCCOC1=CC=CC=C1 QCDWFXQBSFUVSP-UHFFFAOYSA-N 0.000 claims abstract description 6
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- 229920006037 cross link polymer Polymers 0.000 claims abstract description 6
- MSRJTTSHWYDFIU-UHFFFAOYSA-N octyltriethoxysilane Chemical compound CCCCCCCC[Si](OCC)(OCC)OCC MSRJTTSHWYDFIU-UHFFFAOYSA-N 0.000 claims abstract description 6
- 229960003493 octyltriethoxysilane Drugs 0.000 claims abstract description 6
- 229960005323 phenoxyethanol Drugs 0.000 claims abstract description 6
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- 238000003756 stirring Methods 0.000 claims description 21
- 238000002156 mixing Methods 0.000 claims description 12
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- JLPULHDHAOZNQI-ZTIMHPMXSA-N 1-hexadecanoyl-2-(9Z,12Z-octadecadienoyl)-sn-glycero-3-phosphocholine Chemical compound CCCCCCCCCCCCCCCC(=O)OC[C@H](COP([O-])(=O)OCC[N+](C)(C)C)OC(=O)CCCCCCC\C=C/C\C=C/CCCCC JLPULHDHAOZNQI-ZTIMHPMXSA-N 0.000 claims description 7
- KWIUHFFTVRNATP-UHFFFAOYSA-N Betaine Natural products C[N+](C)(C)CC([O-])=O KWIUHFFTVRNATP-UHFFFAOYSA-N 0.000 claims description 7
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- SNPLKNRPJHDVJA-ZETCQYMHSA-N D-panthenol Chemical compound OCC(C)(C)[C@@H](O)C(=O)NCCCO SNPLKNRPJHDVJA-ZETCQYMHSA-N 0.000 claims description 7
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- KWIUHFFTVRNATP-UHFFFAOYSA-O N,N,N-trimethylglycinium Chemical compound C[N+](C)(C)CC(O)=O KWIUHFFTVRNATP-UHFFFAOYSA-O 0.000 claims description 7
- 229960003237 betaine Drugs 0.000 claims description 7
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- 235000020957 pantothenol Nutrition 0.000 claims description 7
- 229940083466 soybean lecithin Drugs 0.000 claims description 7
- DFPAKSUCGFBDDF-UHFFFAOYSA-N Nicotinamide Chemical compound NC(=O)C1=CC=CN=C1 DFPAKSUCGFBDDF-UHFFFAOYSA-N 0.000 claims description 6
- DNIAPMSPPWPWGF-UHFFFAOYSA-N Propylene glycol Chemical compound CC(O)CO DNIAPMSPPWPWGF-UHFFFAOYSA-N 0.000 claims description 6
- ROTFCACGLKOUGI-JYJNAYRXSA-N (2s)-2-[[(2s)-2-[[(2s)-2-(3-acetamidopropanoylamino)-3-(1h-imidazol-5-yl)propanoyl]amino]-3-hydroxypropanoyl]amino]-3-(1h-imidazol-5-yl)propanoic acid Chemical compound C([C@H](NC(=O)CCNC(=O)C)C(=O)N[C@@H](CO)C(=O)N[C@@H](CC=1NC=NC=1)C(O)=O)C1=CN=CN1 ROTFCACGLKOUGI-JYJNAYRXSA-N 0.000 claims description 4
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 claims description 4
- DFPAKSUCGFBDDF-ZQBYOMGUSA-N [14c]-nicotinamide Chemical compound N[14C](=O)C1=CC=CN=C1 DFPAKSUCGFBDDF-ZQBYOMGUSA-N 0.000 claims description 4
- 238000005070 sampling Methods 0.000 claims description 4
- 125000000218 acetic acid group Chemical group C(C)(=O)* 0.000 claims description 3
- 229940099112 cornstarch Drugs 0.000 claims description 3
- 239000011570 nicotinamide Substances 0.000 claims description 3
- 229960003966 nicotinamide Drugs 0.000 claims description 3
- 235000005152 nicotinamide Nutrition 0.000 claims description 3
- -1 octyl glycol Chemical compound 0.000 claims description 3
- 239000004205 dimethyl polysiloxane Substances 0.000 claims description 2
- 235000011187 glycerol Nutrition 0.000 claims description 2
- 229920006007 hydrogenated polyisobutylene Polymers 0.000 claims description 2
- 229920000435 poly(dimethylsiloxane) Polymers 0.000 claims description 2
- 210000003462 vein Anatomy 0.000 claims description 2
- 241000723353 Chrysanthemum Species 0.000 claims 3
- 238000013329 compounding Methods 0.000 claims 1
- LYCAIKOWRPUZTN-UHFFFAOYSA-N ethylene glycol Natural products OCCO LYCAIKOWRPUZTN-UHFFFAOYSA-N 0.000 claims 1
- WGCNASOHLSPBMP-UHFFFAOYSA-N hydroxyacetaldehyde Natural products OCC=O WGCNASOHLSPBMP-UHFFFAOYSA-N 0.000 claims 1
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- 210000004243 sweat Anatomy 0.000 description 2
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- PUPZLCDOIYMWBV-UHFFFAOYSA-N (+/-)-1,3-Butanediol Chemical compound CC(O)CCO PUPZLCDOIYMWBV-UHFFFAOYSA-N 0.000 description 1
- 241001237160 Kallima inachus Species 0.000 description 1
- 206010070834 Sensitisation Diseases 0.000 description 1
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- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 1
- 208000010668 atopic eczema Diseases 0.000 description 1
- 239000008280 blood Substances 0.000 description 1
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- 210000000744 eyelid Anatomy 0.000 description 1
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Classifications
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02A—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE
- Y02A50/00—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE in human health protection, e.g. against extreme weather
- Y02A50/30—Against vector-borne diseases, e.g. mosquito-borne, fly-borne, tick-borne or waterborne diseases whose impact is exacerbated by climate change
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02W—CLIMATE CHANGE MITIGATION TECHNOLOGIES RELATED TO WASTEWATER TREATMENT OR WASTE MANAGEMENT
- Y02W90/00—Enabling technologies or technologies with a potential or indirect contribution to greenhouse gas [GHG] emissions mitigation
- Y02W90/10—Bio-packaging, e.g. packing containers made from renewable resources or bio-plastics
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- Cosmetics (AREA)
Abstract
The application relates to the field of cosmetics, and particularly discloses blacking eye bag removing powder which comprises the following components in percentage by mass: an oil phase: 20-50% of humectant; 0.5-1% of phenoxyethanol; 0.05-0.1% of ethylhexyl glycerol; 2-10% of an emollient; aqueous phase: 20-45% of water; 0.4-5% of mountain burley leaf extract; 0.5-5% of kava leaf/root/stem extract; 0.6-5% of a Baimai root seed extract; 1-3% of chrysanthemum potato root juice; powder phase: 1-10% of titanium dioxide; 1-8% of silica; 1-10% of methyl methacrylate cross-linked polymer; CI 77499 0-1%; 0.01-0.05% of triethoxy octyl silane; CI 77492 0-2%; CI 77491 0-1%. The application has the effects of removing the black pouch and improving the pouch for a long time and preventing recurrence.
Description
Technical Field
The application relates to the field of cosmetics, in particular to blacking eye pouch powder and a preparation process thereof.
Background
Dark circles are caused by night stay, large mood fluctuation, eye fatigue and aging, and the blood flow velocity of blood vessels of the skin of eyes is too slow to form stagnation; insufficient oxygen supply to tissues and excessive accumulation of metabolic wastes in blood vessels, which causes ocular pigmentation. The pouch refers to the sagging and bloated skin of the lower eyelid, and is in the shape of a pouch. The existence of the dark circles and the eye bags easily causes the figure image to lack primordial qi and spirit, especially the eye bags, is a facial problem which is difficult to mask by the cosmetic technology, seriously affects the personal image, and is a difficult problem which puzzles masses, especially female siblings for many years.
At present, the pouch removing cosmetics on the market often have the defects of unobvious pouch removing effect, easy recurrence, high sensitization and the like. Thus, there is still room for improvement.
Disclosure of Invention
In order to ensure that the cosmetics have the effect of remarkably removing the black eye bags, and also have the effect of improving the black eye circles and the eye bags for a long time and are not easy to relapse, the application provides the black eye bag removing powder and the preparation process thereof.
In a first aspect, the present application provides a blacking pouch powder and a preparation process thereof, which adopts the following technical scheme:
the blacking eye pouch powder comprises the following components in percentage by mass:
an oil phase: 20-50% of humectant; 0.5-1% of phenoxyethanol; 0.05-0.1% of ethylhexyl glycerol; 2-10% of an emollient;
aqueous phase: 20-45% of water; 0.4-5% of mountain burley leaf extract; 0.5-5% of kava leaf/root/stem extract; 0.6-5% of a Baimai root seed extract; 1-3% of chrysanthemum potato root juice;
powder phase: 1-10% of titanium dioxide; 1-8% of silica; 1-10% of methyl methacrylate cross-linked polymer; CI 77499 0-1%; 0.01-0.05% of triethoxy octyl silane; CI 77492 0-2%; CI 77491 0-1%;
the total mass percentage is 100%.
By adopting the technical scheme, the mountain burley leaf extract can continuously release multiple heat energy in fat cells, so that the driving and burning of fat are accelerated, and the problems of dark eye circles and eye bags caused by unsmooth blood at the eye bags, continuous shrinkage of capillary vessels and the like are solved. However, the inventor found that the extract of the mountain sheath blight leaves has a certain stimulus to the skin during the actual research and development process, so that the skin is easy to be allergic. Therefore, a great deal of researches show that the addition of the kava leaf/root/stem extract, the Baimai root seed extract and the chrysanthemum potato root juice in cooperation with the mountain bureau leaf extract is beneficial to alleviating the skin irritation caused by the mountain bureau leaf extract, and simultaneously, the addition of the silica in the powder phase utilizes the special structure of the silica to wrap the mountain bureau leaf extract, the kava leaf/root/stem extract, the Baimai root seed extract and the chrysanthemum potato root juice in the water phase, so that the mountain bureau leaf extract has no irritation to the skin, can also effectively moisten the skin, relieve and repair the skin, avoid skin dryness, improve the cell repair capability, reduce the depth of tiny wrinkles on the skin surface and have a better wrinkle removing effect.
Therefore, the mountain withered leaf extract, the kava pepper leaf/root/stem extract, the lotus seed extract and the chrysanthemum potato root juice are matched with each other, and the mountain withered leaf extract, the kava pepper leaf/root/stem extract, the lotus seed extract and the chrysanthemum potato root juice are wrapped by the synergistic silica, so that the black eye bag removing powder has water feel when being smeared on eyes, is fresh and cool when being used, immediately fills up wrinkles, has a very natural covering and filling effect, has the effect of obviously removing black eye bags, and simultaneously has the effect of improving black eye rings and the eye bags for a long time and preventing relapse, thereby achieving the effects of good wrinkle resistance and firm eye skin.
Preferably, the blacking eye pouch powder comprises the following components in percentage by mass:
an oil phase: 30-40% of humectant; 0.6 to 0.7 percent of phenoxyethanol; 0.06-0.08% of ethylhexyl glycerol; 5-7% of an emollient;
aqueous phase: 22-35% of water; 2-4% of a mountain burley leaf extract; kava leaf/root/stem extract 1-3%; 2-4% of a Baimai root seed extract; 1-2% of chrysanthemum potato root juice;
powder phase: 4-6% of titanium dioxide; 3-5% of silica; 6-8% of methyl methacrylate cross-linked polymer; CI 77499 0.07-0.1%; 0.01-0.02% of triethoxy octyl silane; CI 77492 1-2%; CI 77491 is 0.2-0.4%;
the total mass percentage is 100%.
Preferably, the mass ratio of the mountain burley leaf extract, the kava leaf/root/stem extract, the Baimai root seed extract, the chrysanthemum potato root juice and the silica is 3:2:3:1:4.
by adopting the technical scheme, the mountain sheath blight leaf extract, the kava leaf/root/stem extract, the Baimai root seed extract and the Ju potato root juice are matched with the silica in a specific proportion, so that the silica better wraps the mountain sheath blight leaf extract, the kava leaf/root/stem extract, the Baimai root seed extract and the Ju potato root juice, and the situation of wrap failure is difficult to occur, thereby enabling the blacking eye bag removing powder to achieve the purposes of better removing the eye bags and increasing the skin elasticity.
Preferably, the skin conditioning agent further comprises a plurality of corn starch, soybean lecithin, panthenol, maltodextrin, nicotinamide, butylene glycol, acetyl tetrapeptide-5, betaine.
Preferably, the skin conditioning agent further comprises the following components in percentage by mass:
corn starch 0.2-1%;
0.2-1% of soybean lecithin;
1-2% of panthenol;
maltodextrin 0.5-1%;
1-2% of nicotinamide;
0.1-0.5% of butanediol;
acetyl tetrapeptide-5.08-0.1%;
betaine 0.5-2%.
By adopting the technical scheme, corn starch, soybean lecithin, panthenol, maltodextrin, nicotinamide, butanediol, acetyl tetrapeptide-5 and betaine are mutually matched, so that the effects of improving wrinkles at corners of eyes, improving skin elasticity, improving eye bags and weakening dark circles are facilitated, meanwhile, the skin tightening effect can be achieved, and the skin aging resistance and the cell life prolonging effect are achieved on human skin.
Preferably, the humectant is a compound of glycerin, propylene glycol and butanediol.
By adopting the technical scheme, the blacking pouch removing powder has better effects of moisturizing and supplementing water.
Preferably, the emollient comprises a combination of octylglycol, ethylhexyl glycerol, hydrogenated polyisobutene, polydimethylsiloxane.
Through adopting above-mentioned technical scheme for remove black pouch powder and have the effect of better getting rid of pouch to eye skin, and, can form one deck even protection film that has waterproof nature after the coating skin, do not have greasy sense, be favorable to improving people's comfort.
In a second aspect, the present application provides a preparation process of blacking eye pouch powder, which adopts the following technical scheme:
a preparation process of blacking pouch powder comprises the following steps:
s1: adding the components in the powder phase into a batching pot respectively, stirring at a high speed at a rotating speed of 3500-4000r/min, and uniformly mixing;
s2: stirring and dissolving all components in the water phase in a container in advance, uniformly mixing, adding into a batching pan, and uniformly stirring at the rotating speed of 2800-3800 r/min;
s3: mixing the components in the oil phase uniformly, then putting into a batching pot, stirring uniformly at a high speed of 2500-3500r/min, taking out of the pot, sampling and inspecting to obtain the blackened eye bag removing powder.
Through adopting above-mentioned technical scheme, adopt specific rotational speed to cooperate specific component to prepare the blacking pouch powder again for silica parcel mountain cloth dead leaf extract, kava leaf/root/stem extract, hundred vein root seed extract, chrysanthemum potato root juice ground is more even, is difficult for appearing because the powder can not wrap up the aqueous phase and leads to wrapping up uneven phenomenon, so that blacking pouch powder has the effect of improving eye microcirculation, alleviate eye tired, and blacking pouch powder's gas permeability is good, has obvious dustproof effect, will blacking pouch powder smear on the eye also can not influence the discharge of sweat, has good experience.
In summary, the present application includes at least one of the following beneficial technical effects:
1. the kava leaf/root/stem extract, the Baimai root seed extract and the chrysanthemum juice are added to be matched with the mountain withered leaf extract in a synergistic way, meanwhile, silica is added into the powder phase, and the mountain withered leaf extract, the kava leaf/root/stem extract, the Baimai root seed extract and the chrysanthemum juice in the water phase are wrapped in the powder phase by utilizing the special structure of the silica, so that the mountain withered leaf extract has no irritation to skin, has the effect of obviously removing black eye bags, has the effect of improving the black eye circles and the eye bags for a long time and is not easy to relapse, and further has the effects of good wrinkle resistance and firm eye skin.
2. The mountain sheath blight leaf extract, the kava pepper leaf/root/stem extract, the lotus seed extract and the chrysanthemum root juice are matched with the silica according to a specific proportion, so that the silica better wraps the mountain sheath blight leaf extract, the kava pepper leaf/root/stem extract, the lotus seed extract and the chrysanthemum root juice, and the wrapping failure is not easy to occur, thereby enabling the blackened eye bag removing powder to achieve the purposes of better removing the eye bags and increasing the skin elasticity.
3. The black eye bag removing powder is prepared by adopting a specific rotating speed and matching with specific components, so that silica is used for wrapping mountain withered leaf extract, kava leaf/root/stem extract, lotus seed extract and chrysanthemum potato root juice more uniformly, the phenomenon of uneven wrapping caused by the fact that powder cannot wrap water phase is difficult to occur, the black eye bag removing powder has the effects of improving eye microcirculation and relieving eye fatigue, and the black eye bag removing powder is good in air permeability, has an obvious dustproof effect, does not influence the discharge of sweat when being smeared on eyes, and has good experience.
Detailed Description
The present application is described in further detail below with reference to examples.
Example 1
The blacking eye pouch powder comprises the following components:
an oil phase: a humectant; phenoxyethanol; ethylhexyl glycerol; an emollient;
aqueous phase: water; a mountain burley leaf extract; kava leaf/root/stem extract; an extract of Baimai root seed; the chrysanthemum potato root juice;
powder phase: titanium dioxide; silica; methyl methacrylate cross-linked polymer; CI 77499; triethoxy octyl silane; CI 77492; CI 77491.
A preparation process of blacking pouch powder comprises the following steps:
s1: adding the components in the powder phase into a batching pot respectively, stirring at high speed at 3500r/min, and mixing uniformly;
s2: stirring and dissolving all components in the water phase in a container in advance, uniformly mixing at the rotating speed of 1500r/min, adding into a batching pan, and uniformly stirring at the rotating speed of 2800 r/min;
s3: mixing the components in the oil phase uniformly, then putting the mixture into a batching pot, stirring the mixture uniformly at a high speed of 2500r/min, taking out of the pot, sampling and inspecting the mixture, and obtaining the blackened eye bag removing powder.
Example 2
The difference from example 1 is that:
a preparation process of blacking pouch powder comprises the following steps:
s1: adding the components in the powder phase into a batching pot respectively, stirring at a high speed at a rotating speed of 4000r/min, and uniformly mixing;
s2: stirring and dissolving all components in the water phase in a container in advance, uniformly mixing at the rotating speed of 2000r/min, adding into a batching pan, and uniformly stirring at the rotating speed of 3800 r/min;
s3: mixing the components in the oil phase uniformly, then putting the mixture into a batching pot, stirring the mixture uniformly at a high speed of 3500r/min, taking out of the pot, sampling and inspecting the mixture, and obtaining the blackened eye bag removing powder.
Examples 3 to 4
The difference from example 2 is that: the components and the dosage are different.
Example 5
The difference from example 4 is that: the mass ratio of the mountain burley leaf extract, the kava leaf/root/stem extract, the Baimai root seed extract, the chrysanthemum potato root juice and the silica is 3:2:3:1:4.
the components and amounts of the components used in examples 1 to 5 are shown in Table 1, the amounts of the components used in Table 1 being in kg.
TABLE 1
Example 6
The difference from example 5 is that: the water phase also comprises 1kg of corn starch, 1kg of soybean lecithin, 2kg of panthenol, 0.5kg of maltodextrin, 1kg of nicotinamide, 0.1kg of butanediol, 0.08kg of acetyl tetrapeptide-5 and 0.5kg of betaine, and the water is 21.52kg.
Example 7
The difference from example 5 is that: the water phase also comprises corn starch 0.2kg, soybean lecithin 0.2kg, panthenol 1kg, maltodextrin 1kg, nicotinamide 2kg, butanediol 0.5kg, acetyl tetrapeptide-5.1 kg, betaine 2kg, and water 20.7kg.
Example 8
The difference from example 5 is that: the stirring speed of the aqueous phase and the powder phase in S2 is 4000r/min.
Example 9
The difference from example 5 is that: in S3, the stirring speed of the oil phase and the powder phase and the water phase is 4000r/min.
Comparative example 1
The difference from example 5 is that: the aqueous phase is not added with the extract of the mountain sheath blight leaves.
Comparative example 2
The difference from example 5 is that: the water phase is not added with kava leaf/root/stem extract.
Comparative example 3
The difference from example 5 is that: the water phase is not added with the extract of the seed of the radix platyphyllae.
Comparative example 4
The difference from example 5 is that: the water phase is not added with the chrysanthemum potato root juice.
Comparative example 5
The difference from example 5 is that: no silica was added to the powder phase.
Comparative example 6
The difference from example 5 is that: the amounts of mountain sheath blight leaf extract, kava leaf/root/stem extract, passion fruit seed extract, chrysanthemum potato root juice and silica used were all different from those of example 5, namely 6kg, 7kg and 5kg of mountain sheath blight leaf extract, kava leaf/root/stem extract, passion fruit seed extract, chrysanthemum potato root juice and silica used, respectively.
Experiment 1 skin patch test
The number of the tested persons is 50, and all the tested persons accord with the standard of the test subjects. The blacking eye bag powder prepared in examples 1 to 9 and comparative examples 1 to 6 was placed in each of plaque test cells in an amount of about 0.020g to 0.025g. The control wells were blank (without any substance) and the plaque test with the test substance was applied to the back or forearm side of the subject with hypoallergenic tape and gently pressed with the palm to apply it uniformly to the skin for 24 hours. Skin reactions were observed according to the following table criteria for 30min (after the disappearance of the indentations) and 24h after removal of the subject plaque tester, respectively, and the observations were recorded. The results were recorded according to the skin reaction classification criteria in cosmetic safety Specification 2015, which is shown in Table 2.
TABLE 2 skin seal Patch test skin response grading criteria
Experiment 2 pouch removal Effect
1. Test instrument: the rapid three-dimensional imaging system of skin PRIMOS, canfield, usa;
2. the test principle is as follows: obtaining a digital three-dimensional image of the surface of the skin to be tested by testing the position change of stripe light irradiated to the surface of the skin and the gray values of all image points, and analyzing by system software to obtain the volume of the eye bag;
3. test sample: examples 1 to 9 and comparative examples 1 to 6;
4. the testing method comprises the following steps: 150 subjects were selected, 10 in each group, meeting the subject criteria. The rapid three-dimensional imaging system PRIMOS of the skin is adopted to shoot the pouch images of the subject before and after the use of the blacking pouch powder, and the pouch volume value is obtained through analysis, the pouch volume is obviously reduced after the use compared with that before the use, which indicates that the blacking pouch powder has the effect of improving the pouch after long-term use.
The test indexes are as follows: rate of change = (post-use measurement-pre-use measurement)/pre-use measurement x 100%.
The results of the above experiments are shown in Table 3.
TABLE 3 Table 3
According to the comparison of comparative examples 1 to 5 in Table 3 with example 5, respectively, the comparative example 1 was free from the addition of the extract of mountain sheath blight leaves, the black pouch removed powder did not cause irritation to the skin, the comparative example 2 was free from the addition of the extract of kava pepper leaves/roots/stems, the comparative example 3 was free from the addition of the extract of Baimai roots, the comparative example 4 was free from the addition of the juice of Ju potato roots, and the comparative examples 2 to 4 caused a certain irritation to the skin, because the comparative examples 2 to 4 were both added with the extract of mountain sheath blight leaves, and the extract of mountain sheath blight leaves caused a certain irritation to the skin; in comparative example 5, the kava leaf/root/stem extract, the Baimai root seed extract, the Ju potato root juice and the mountain area leaf extract are added at the same time, and the skin reaction grade is reduced, which shows that the kava leaf/root/stem extract, the Baimai root seed extract, the Ju potato root juice and the mountain area leaf extract are added to cooperate, thereby being beneficial to reducing the irritation of the mountain area leaf extract to the skin.
Example 5 was also added with silica on the basis of comparative example 5, and the skin reaction grade was reduced, demonstrating that the addition of silica synergistically acted with the mountain bureau leaf extract, the kava leaf/root/stem extract, the Baimai root seed extract, and the jujuba root juice, so that the mountain bureau leaf extract was not irritating to the skin, since the mountain bureau leaf extract, the kava leaf/root/stem extract, the Baimai root seed extract, and the jujuba root juice in the aqueous phase were enclosed therein by the special structure of silica, so that the mountain bureau leaf extract was not irritating to the skin.
In summary, silica is adopted to wrap the mountain bureau leaf extract, the kava leaf/root/stem extract, the Baimai root seed extract and the Ju potato root juice, so that the irritation of the mountain bureau leaf extract to the skin is greatly reduced, and people have comfortable experience. The absence of any of silica and burley leaf extract, kava leaf/root/stem extract, cranberry seed extract, and chrysanthemum juice does not achieve the results of the present application.
According to the comparison of comparative example 6 and example 5 in Table 3, the dosages of the mountain withered leaf extract, the kava leaf/root/stem extract, the Baimai root seed extract, the Ju potato root juice and the silica in comparative example 6 are not within the scope protected by the application, and the change rate after 28 days of using the blackeye removing bag is increased, which indicates that the dosages of the mountain withered leaf extract, the kava leaf/root/stem extract, the Baimai root seed extract, the Ju potato root juice and the silica are not within the scope protected by the application, and the eye bag is easy to relapse. Therefore, the dosage of the mountain burley leaf extract, the kava leaf/root/stem extract, the baimai root seed extract, the chrysanthemum potato root juice and the silica is only within the scope of protection of the application, so that the mountain burley leaf extract, the kava leaf/root/stem extract, the baimai root seed extract, the chrysanthemum potato root juice and the silica have better effect of removing the eye bags, and are not easy to relapse after long-term use. Not all the proportions can achieve the effect of the application.
According to comparison of example 8 and example 5 in Table 3, the stirring speed of the aqueous phase and the powder phase in example 8 was 4000r/min, and the rotating speed silica under the stirring speed was not good enough to encapsulate the mountain sheath and leaf extract, kava leaf/root/stem extract, baimai root seed extract and Ju potato root juice therein, so that the blacking eye powder was stimulated to the skin, and the blacking eye powder's eyebag removing effect was also affected.
According to comparison of example 9 and example 5 in Table 3, the stirring speed of the oil phase and the powder phase in example 9 was 4000r/min, and the rotation speed under the conditions was such that the silica could not encapsulate the mountain sheath blight leaf extract, the kava leaf/root/stem extract, the Baimai root seed extract and the Ju potato root juice more uniformly, and the uneven encapsulation was likely to occur, thereby affecting the performance of the blackened pouch powder.
Therefore, only when the rotating speed of the application is used for coating the mountain withered leaf extract, the kava leaf/root/stem extract, the Baimai root seed extract and the Ju potato root juice in the mountain withered leaf extract, the kava leaf/root/stem extract and the Baimai root seed extract, the black eye bag can be obviously removed, and meanwhile, the black eye ring and the black eye bag are improved for a long time and are not easy to relapse.
Experiment 3 subject use feeling test
The temperature of the test environment is 20-22 ℃, the humidity is 40-60%, and real-time dynamic monitoring is carried out. The subjects were 18-45 years old, 30 subjects were numbered separately, and each subject was coated on the face and neck using the same method as the blackened pouch powder prepared in examples 1-9 and comparative examples 1-6.
Preparation before testing: any product (cosmetic or topical medicine) cannot be used 2-3 days before testing the tested part, and water cannot be contacted for 1-3 hours. Prior to testing, subjects were required to uniformly clean the face and neck, and were wiped clean with dry facial tissues. After cleaning, the face and neck of the subject are marked with measurement areas. Before formal test, the test bed should sit still for 30min in a room meeting the standard, can not drink water, and is placed in a test state to be kept relaxed.
The testing steps are as follows: in the experiment, the face and neck were marked with 2cm x 2cm test areas, and the face and neck were marked with multiple areas at 1cm intervals. The plurality of regions are evenly distributed over the face and neck. Subjects were respectively smeared with the black pouch powder and the blank, and the test samples were tested according to (3.00.1）mg/cm 2 The test product was uniformly coated in the test area using latex fingerstall, and each sample was applied for each week in the morning and evening, respectively.
After application, 30 volunteers were scored for skin hydration, skin elasticity, and wrinkle change, respectively (0-100 points).
The scoring criteria for the above items are shown in Table 4:
TABLE 4 Table 4
The moisture retention and water supplementing effect of the blacking eye pouch powder can be obtained by scoring the moisture degree of the skin by a subject; the anti-wrinkle effect of the black pouch removing powder can be obtained by scoring the change of wrinkles and the skin elasticity of the skin of the subject. The experimental results are shown in Table 5.
TABLE 5
According to the comparison of comparative examples 1-5 in Table 5 with examples 1-5, respectively, the extract of Bu-tui leaf, the extract of kava leaf/root/stem, the extract of Baimai root seed, the juice of Ju-potato root and silica are used in examples 1-5 to make the powder for removing black eye bag have better effect of removing eye bag, and make the powder for removing black eye bag have better effects of moisturizing, moisturizing and anti-wrinkle.
The foregoing are all preferred embodiments of the present application, and are not intended to limit the scope of the present application in any way, therefore: all equivalent changes in structure, shape and principle of this application should be covered in the protection scope of this application.
Claims (5)
1. The blacking eye pouch powder is characterized in that: comprises the following components in percentage by mass:
an oil phase: 20-50% of humectant; 0.5-1% of phenoxyethanol; 0.05-0.1% of ethylhexyl glycerol; 2-10% of an emollient;
aqueous phase: 20-45% of water; 0.4-5% of mountain burley leaf extract; 0.5-5% of kava leaf/root/stem extract; 0.6-5% of a Baimai root seed extract; 1-3% of chrysanthemum potato root juice;
powder phase: 1-10% of titanium dioxide; 1-8% of silica; 1-10% of methyl methacrylate cross-linked polymer; CI 77499 0-1%; 0.01-0.05% of triethoxy octyl silane; CI 77492 0-2%; CI 77491 0-1%;
the total mass percentage is 100 percent;
the humectant is the compounding of glycerin, propylene glycol and butanediol;
the emollient comprises the combination of octyl glycol, ethylhexyl glycerol, hydrogenated polyisobutene and polydimethylsiloxane;
the preparation process of the blacking eye pouch powder comprises the following steps:
s1: adding the components in the powder phase into a batching pot respectively, stirring at a high speed at a rotating speed of 3500-4000r/min, and uniformly mixing;
s2: stirring and dissolving all components in the water phase in a container in advance, uniformly mixing, adding into a batching pan, and uniformly stirring at the rotating speed of 2800-3800 r/min;
s3: mixing the components in the oil phase uniformly, then putting into a batching pot, stirring uniformly at a high speed of 2500-3500r/min, taking out of the pot, sampling and inspecting to obtain the blackened eye bag removing powder.
2. The blacking eye bag powder according to claim 1, wherein: the blacking eye pouch powder comprises the following components in percentage by mass:
an oil phase: 30-40% of humectant; 0.6 to 0.7 percent of phenoxyethanol; 0.06-0.08% of ethylhexyl glycerol; 5-7% of an emollient;
aqueous phase: 22-35% of water; 2-4% of a mountain burley leaf extract; kava leaf/root/stem extract 1-3%; 2-4% of a Baimai root seed extract; 1-2% of chrysanthemum potato root juice;
powder phase: 4-6% of titanium dioxide; 3-5% of silica; 6-8% of methyl methacrylate cross-linked polymer; CI 77499 0.07-0.1%; 0.01-0.02% of triethoxy octyl silane; CI 77492 1-2%; CI 77491 is 0.2-0.4%;
the total mass percentage is 100%.
3. A blacking eye bag powder according to any one of claims 1-2, characterized in that: the mass ratio of the mountain burley leaf extract, the kava leaf/root/stem extract, the hundred vein root seed extract, the chrysanthemum potato root juice and the silica is 3:2:3:1:4.
4. a blacking eye bag powder according to any one of claims 1-2, characterized in that: the water phase also comprises corn starch, soybean lecithin, panthenol, maltodextrin, nicotinamide, butanediol, acetyl tetrapeptide-5, and betaine.
5. The blacking eye bag powder according to claim 4, wherein: the water phase also comprises the following components in percentage by mass:
corn starch 0.2-1%;
0.2-1% of soybean lecithin;
1-2% of panthenol;
maltodextrin 0.5-1%;
1-2% of nicotinamide;
0.1-0.5% of butanediol;
acetyl tetrapeptide-5.08-0.1%;
betaine 0.5-2%.
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| FR2980362B1 (en) * | 2011-09-27 | 2013-10-04 | Sederma Sa | NOVEL COSMETIC USE OF ALBIZIA JULIBRISSIN EXTRACT AND CORRESPONDING TOPICAL COMPOSITION |
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| CN106176298A (en) * | 2016-07-08 | 2016-12-07 | 珍尔姿（广州）化妆品有限公司 | One dispels black-eyed compositions |
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