CN115645311B - Grease composition with repairing and cooling effects and application thereof - Google Patents
Grease composition with repairing and cooling effects and application thereof Download PDFInfo
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- CN115645311B CN115645311B CN202211414863.4A CN202211414863A CN115645311B CN 115645311 B CN115645311 B CN 115645311B CN 202211414863 A CN202211414863 A CN 202211414863A CN 115645311 B CN115645311 B CN 115645311B
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Abstract
The invention relates to a grease composition with repairing and cooling effects and application thereof, wherein the grease composition with repairing and cooling effects comprises white pool flower seed oil, prinsepia utilis royle oil, squalane, stearyl heptanoate, phytosterol canola oil glycerides and jojoba oil. The grease composition composed of the six components has the effects of keeping moisture, reducing temperature, resisting allergy, removing red blood streaks and nourishing skin and repairing, can be applied to preparation of various cosmetics, and is mild and free of irritation.
Description
Technical Field
The invention belongs to the technical field of cosmetics, relates to a grease composition with repairing and cooling effects and application thereof, and in particular relates to a grease composition with repairing and cooling effects and application thereof in cosmetics.
Background
In recent years, the public is increasingly concerned about "sensitive muscle care". Skin sensitivity is mainly due to two reasons: endogenous injuries such as natural aging, chronic inflammation, sleep, stress, diet, etc.; exogenous damage such as environmental pollution, ultraviolet irradiation, improper use of cosmetics, and mechanical pulling damage. The main manifestations of sensitive skin groups are discomfort such as burning, stinging, itching and tightness of the facial skin, lasting minutes or hours, and general cosmetics cannot be tolerated. In recent years, the proportion of skin care products aiming at 'sensitive muscle' repair is continuously increased, and the repair efficacy of the products is expected to be more greatly improved by the masses.
Cosmetic products with repairing effects have been reported in the prior art, for example, CN112315882A discloses a repairing and moisturizing facial cream and a preparation method thereof, wherein the facial cream is mainly prepared by compounding bisabolol, 4-tert-butylcyclohexanol, plant soothing components, a skin conditioning agent and a humectant, and the plant soothing components and the bisabolol have instant itching relieving and anti-inflammatory effects; the 4-tert-butylcyclohexanol immediately reduces burning and stinging feel, and the skin conditioner repairs skin; the humectant has effects of keeping moisture and moistening, and can soften skin and lock skin moisture. The cream is mild, does not irritate, is safe, has no toxic or side effect, can effectively preserve moisture, repair red and repair, and is suitable for people with partial sensitive skin.
For example, CN104173261a discloses an anti-allergy soothing repair emulsion and a method for preparing the same, said emulsion comprising: sweet almond oil, macadamia nut oil, wheat germ oil, evening primrose oil, omnipotent simple emulsifier, water-soluble jojoba oil, water-soluble Ve, biological polysaccharide gum, cell activating agent, amino acid humectant, trehalose, stevia leaf extract, hibiscus leaf extract, gentian extract, ligusticum wallichii root extract, honey, distilled water, glycerol, 1, 2-propylene glycol, ethylparaben and essence. Compared with the existing emulsion, the emulsion is mild and non-irritating, has obvious effect of relieving and repairing, has the most mild moisturizing effect of active ingredients in natural vegetable oil on skin, has the functions of moisturizing and activating cells to keep the skin moist, and has the effects of calming and relieving the skin, promoting blood circulation, keeping moist, endowing the cells with vitality and enabling the skin to emit light from inside to outside.
However, the repairing mechanism of the existing cosmetics is relatively one-sided, the effect is not long-lasting, or the preparation raw materials are excessive, and the process cost is relatively high. Therefore, it is highly necessary to develop more products with significant repair efficacy.
Disclosure of Invention
Aiming at the defects of the prior art, the invention aims to provide a grease composition with repairing and cooling effects and application thereof, in particular to a grease composition with repairing and cooling effects and application thereof in cosmetics.
In order to achieve the aim of the invention, the invention adopts the following technical scheme:
the invention relates to a grease composition with repairing and cooling effects, which comprises white pool flower seed oil, prinsepia utilis royle oil, squalane, stearyl heptanoate, phytosterol canola oil glycerides and jojoba oil.
The invention creatively discovers that the grease composition composed of six components of the white pool flower seed oil, the prinsepia utilis royle oil, the squalane, the stearyl heptanoate, the phytosterol canola oil glyceride and the jojoba oil has excellent effects of moisturizing, cooling, resisting allergy, removing red blood streaks and nourishing skin and repairing, can be applied to preparation of various cosmetics, and is mild and non-irritating. Wherein stearyl alcohol heptanoate, phytosterol canola oil glycerides and jojoba oil have potential interactions, positively influence each other, and have synergistic effects on the above efficacy which are unexpected to those skilled in the art.
Preferably, the grease composition with repairing and cooling effects comprises, by mass, 1-10 parts of white pool flower seed oil, 1-5 parts of prinsepia utilis royle oil, 1-20 parts of squalane, 1-15 parts of stearyl heptanoate, 1-10 parts of phytosterol canola oil glycerides and 1-20 parts of jojoba oil.
When the six components in the oil composition are combined according to the specific mass ratio, the effects of moisture preservation, temperature reduction, allergy resistance, red blood streak removal and skin care restoration can be maximized.
The mass parts of the white pond flower seed oil can be 1 part, 2 parts, 3 parts, 4 parts, 5 parts, 6 parts, 7 parts, 8 parts, 9 parts, 10 parts and the like.
The prinsepia utilis royle oil can be selected from 1 part, 2 parts, 3 parts, 4 parts, 5 parts and the like by mass.
The squalane may be selected from 1 part, 3 parts, 5 parts, 7 parts, 10 parts, 12 parts, 15 parts, 16 parts, 18 parts, 20 parts, etc.
The weight parts of the stearyl alcohol heptanoate can be 1 part, 3 parts, 5 parts, 7 parts, 10 parts, 12 parts, 15 parts and the like.
The mass parts of the phytosterol canola oil glyceride can be 1 part, 2 parts, 3 parts, 4 parts, 5 parts, 6 parts, 7 parts, 8 parts, 9 parts, 10 parts and the like.
The mass parts of jojoba oil can be 1 part, 3 parts, 5 parts, 7 parts, 10 parts, 12 parts, 15 parts, 16 parts, 18 parts, 20 parts and the like.
Other specific point values in the numerical ranges are selectable, and will not be described in detail herein.
Preferably, the grease composition with repairing and cooling effects is obtained by uniformly and physically mixing all the preparation raw materials.
In a second aspect, the invention provides an application of the oil composition with repairing and cooling effects in preparing cosmetics.
Preferably, the cosmetic comprises an emulsion, a face cream, a face mask, a sun cream, an essence and a cleansing oil.
Preferably, the weight percentage of the oil composition with repairing and cooling effects in the cosmetic is 10-40%, for example 10%, 15%, 20%, 25%, 30%, 35%, 40%, etc., and other specific values within the numerical range are selectable, so that no further description is given here.
In a third aspect, the invention provides an emulsion with repairing and cooling effects, which comprises the oil composition with repairing and cooling effects, an emulsifying agent, a thickening agent, a humectant, an antioxidant and water.
The emulsion product has the effects of excellent moisturizing, cooling, anti-allergy, red blood streak removal and skin care restoration, and has good system stability and high safety.
Preferably, the emulsion with repairing and cooling effects comprises, by mass, 10-40% of the oil composition with repairing and cooling effects of the first aspect, 1-10% of an emulsifying agent, 0.1-2% of a thickening agent, 3-15% of a humectant, 0.2-1% of an antioxidant and water.
The mass percentage of the grease composition can be 10%, 15%, 20%, 25%, 30%, 35%, 40% and the like.
The mass percentage of the emulsifier can be 1%, 2%, 3%, 4%, 5%, 6%, 7%, 8%, 9%, 10% and the like.
The mass percentage of the thickener can be selected from 0.1%, 0.3%, 0.5%, 0.8%, 1%, 1.2%, 1.5%, 1.6%, 1.8%, 2% and the like.
The humectant can be selected from 3%, 4%, 5%, 6%, 7%, 8%, 9%, 10%, 12%, 15% and the like by mass.
The antioxidant can be selected from 0.2%, 0.3%, 0.5%, 0.8%, 1% by mass, etc. Other specific point values within the above numerical ranges are selectable, and will not be described in detail herein.
Preferably, the emulsion with repairing and cooling effects further comprises a plant extract, wherein the plant extract comprises centella asiatica extract, chamomile extract and flaxseed extract.
The invention also creatively discovers that the addition of the centella asiatica extract, the chamomile extract and the flaxseed extract in the emulsion product can further improve the cooling and repairing effects of the product, and the centella asiatica extract, the chamomile extract and the flaxseed extract also have a certain synergistic effect on the effects.
Preferably, the emulsion with repairing and cooling effects further comprises any one or a combination of at least two of whitening effect active substances, antioxidant effect active substances or anti-saccharification effect active substances.
The whitening active is selected from common whitening ingredients which can be added into cosmetic products, such as vitamin C, nicotinamide, arbutin, kojic acid, fruit acid, etc.
The antioxidant active is selected from common antioxidant ingredients which can be added into cosmetic products, such as glutathione, vitamin E, ubiquinone, grape polyphenols, astaxanthin, etc.
The anti-glycation efficacy active is selected from the commonly used ingredients with anti-glycation efficacy that can be added to cosmetic products, such as carnosine, albizia bark extract, red sage extract, pomegranate extract, etc.
Preferably, the emulsion with repairing and cooling effects further comprises any one or a combination of at least two of a preservative, a pH regulator, a chelating agent and a flavoring agent.
Preferably, the emulsifier comprises any one or a combination of at least two of glycerol stearate, C12-20 alkyl glucoside, coco glucoside, polyglycerol-3 methyl glucose distearate, sucrose stearate, or hydrogenated lecithin.
Preferably, the thickener comprises any one or a combination of at least two of carbomers, tara gum, ammonium acryloyldimethyl taurate/behenate polyether-25 methacrylate cross-linked poly, acrylic acid (esters) and C10-30 alkanol acrylate cross-linked polymer, sclerotium gum or pectin.
Preferably, the humectant comprises any one or a combination of at least two of glycerol, butylene glycol, propylene glycol, sodium hyaluronate, erythritol, trehalose, or dextran; more preferred is a combination of glycerol, sodium hyaluronate and erythritol.
The present invention has also creatively found that when a combination of glycerin, sodium hyaluronate and erythritol is selected as the humectant component, the moisturizing effect of the product can be amplified, and the manifestation of the moisturizing effect of the oil composition can be further promoted.
Preferably, the antioxidant comprises tocopheryl acetate.
In a fourth aspect, the present invention provides a method for preparing the emulsion with repairing and cooling effects according to the third aspect, the method comprising:
(1) Mixing the oil composition, the antioxidant and the emulsifier to obtain an oil phase; mixing thickener and humectant water to obtain water phase;
(2) Mixing the water phase and the oil phase obtained in the step (1) and emulsifying to obtain the water-phase-oil emulsion.
Preferably, the oil phase is prepared by heating to 70-85deg.C, such as 70deg.C, 72deg.C, 75deg.C, 78deg.C, 80deg.C, 82 deg.C, 84 deg.C, 85deg.C, etc.; the aqueous phase is prepared by heating to 80-90deg.C, such as 80deg.C, 82 deg.C, 85 deg.C, 88 deg.C, 90 deg.C, etc.
Preferably, the emulsification is performed at 70-90deg.C (e.g., 70deg.C, 72deg.C, 75deg.C, 78deg.C, 80deg.C, 82 deg.C, 85deg.C, 90deg.C, etc.) for 5-15min (e.g., 5min, 8min, 10min, 12min, 15min, etc.).
Preferably, the emulsified mixture further comprises mixing with any one or a combination of at least two of plant extracts, whitening efficacy actives, antioxidant efficacy actives, anti-glycation efficacy actives, preservatives, pH adjusters, chelating agents or fragrances.
Compared with the prior art, the invention has the following beneficial effects:
the invention creatively discovers that the grease composition composed of the six components of the white pool flower seed oil, the prinsepia utilis royle oil, the squalane, the stearyl heptanoate, the phytosterol canola oil glyceride and the jojoba oil has the effects of keeping moisture, cooling and calming, resisting allergy, removing red blood streaks and nourishing skin and repairing, can be applied to the preparation of various cosmetics, and is mild and not stimulated. Wherein stearyl alcohol heptanoate, phytosterol canola oil glycerides and jojoba oil have potential interactions, positively influence each other, and have synergistic effects on the above efficacy which are unexpected to those skilled in the art.
Detailed Description
In order to further describe the technical means adopted by the present invention and the effects thereof, the following describes the technical scheme of the present invention in combination with the preferred embodiments of the present invention, but the present invention is not limited to the scope of the embodiments.
The sources of the functional components contained in the products related to the following examples, comparative examples, application examples and comparative application examples are as follows (only the functional components are represented, and the essential auxiliary material components contained in other commercial raw materials are not described in detail):
the white pool seed oil was obtained from Charkit Chemical Company under the trade name Meadowfoam Seed Oil TM Is a product of (a);
prinsepia utilis royle oil is derived from a product commercially available from Rock Arras under the trade name Rock Arras Prinsepia utilis royle oil;
squalane is derived from a product available from NIPPON SURFACTANT INDUSTRIES co., ltd. Company under the trade designation NIKKOL SUGAR SQUALANE;
stearyl alcohol heptanoate was commercially available from Evonik-Personal Care under the trade nameSH products;
the phytosterol canola oil glycerides are derived from the company AAK AB under the trade designation Lipex cell TM Is a product of (a);
jojoba Oil is available from OLVEA under the trade name Jojoba Oil;
centella asiatica extract is available from Inc. under the trade name MultiEX BSASM from DKSH North America TM Is a product of (a);
the chamomile extract was obtained from a product available from makingconsets inc. Under the trade name Helichrysum Extract;
the flaxseed extract was obtained from AQIA Qui mica Inovativa under the trade name SEMI DI LINO AQ AQUEOUS EXTRACT;
sodium hyaluronate is available under the trade name Hybloom from Kaxi Biotech Co., ltd TM Sodium hyaluronate product;
CoCo Glucoside was obtained from Spec-Chem Industry Inc. under the trade name CoCo Glucoside (C8-14 Fatty Alcohol Glycoside,SpecSufc) TM APG 0814);
polyglycerol-3 methyl glucose distearate was obtained from Evonik-Personal Care under the trade nameCare 450MB product.
Example 1
The embodiment provides a grease composition with repairing and cooling effects, which comprises the following components in parts by mass: 3 parts of white pool flower seed oil, 2 parts of prinsepia utilis royle oil, 5 parts of squalane, 5 parts of stearyl heptanoate, 5 parts of phytosterol canola oil glyceride and 5 parts of jojoba oil.
Example 2
The embodiment provides a grease composition with repairing and cooling effects, which comprises the following components in parts by mass: 8 parts of white pool flower seed oil, 1 part of prinsepia utilis royle oil, 1 part of squalane, 6 parts of stearyl heptanoate, 2 parts of phytosterol canola oil glyceride and 7 parts of jojoba oil.
Example 3
The embodiment provides a grease composition with repairing and cooling effects, which comprises the following components in parts by mass: 1 part of white pool flower seed oil, 2 parts of prinsepia utilis royle oil, 7 parts of squalane, 2 parts of stearyl heptanoate, 6 parts of phytosterol canola oil glyceride and 7 parts of jojoba oil.
Comparative example 1
This comparative example provides a composition which differs from example 1 only in that: 5 parts of stearyl alcohol heptanoate, 5 parts of plant sterol canola oil glycerides and 5 parts of jojoba oil are replaced by 7.5 parts of plant sterol canola oil glycerides and 7.5 parts of jojoba oil, and other components and contents are kept unchanged.
Comparative example 2
This comparative example provides a composition which differs from example 1 only in that: the stearyl alcohol heptanoate 5 parts, the phytosterol canola oil glycerides 5 parts and the jojoba oil 5 parts are replaced by stearyl alcohol heptanoate 7.5 parts and jojoba oil 7.5 parts, and other components and contents are kept unchanged.
Comparative example 3
This comparative example provides a composition which differs from example 1 only in that: the stearyl alcohol heptanoate 5 parts, the phytosterol canola oil glycerides 5 parts and the jojoba oil 5 parts are replaced by the stearyl alcohol heptanoate 7.5 parts and the phytosterol canola oil glycerides 7.5 parts, and other components and contents are kept unchanged.
Comparative example 4
This comparative example provides a composition which differs from example 1 only in that: 5 parts of stearyl alcohol heptanoate, 5 parts of phytosterol canola oil glycerides and 5 parts of jojoba oil are replaced by 15 parts of stearyl alcohol heptanoate, and other components and contents remain unchanged.
Comparative example 5
This comparative example provides a composition which differs from example 1 only in that: 5 parts of stearyl alcohol heptanoate, 5 parts of phytosterol canola oil glycerides and 5 parts of jojoba oil are replaced by 15 parts of phytosterol canola oil glycerides, and other components and contents remain unchanged.
Comparative example 6
This comparative example provides a composition which differs from example 1 only in that: 5 parts of stearyl alcohol heptanoate, 5 parts of phytosterin canola oil glycerides and 5 parts of jojoba oil are replaced by 15 parts of jojoba oil, and other components and contents are kept unchanged.
Application example 1
The application example provides an emulsion with repairing and cooling effects, which comprises the following formula:
the preparation method comprises the following steps:
(1) Mixing the oil composition, the antioxidant and the emulsifier, heating to 80 ℃, uniformly stirring, and preserving heat for 5min to obtain an oil phase; mixing thickener, humectant and water, heating to 85deg.C, stirring, and maintaining the temperature for 15min to obtain water phase;
(2) After the heat preservation is finished, mixing the water phase and the oil phase obtained in the step (1), stirring under vacuum to emulsify for 15min, and preserving heat for 5min;
(3) Cooling to 45deg.C, adding pH regulator, and homogenizing for 1min;
(4) Continuously cooling to 40 ℃, adding the preservative and the chelating agent, and uniformly stirring to obtain the product.
Application examples 2 to 3
The present application example provides two emulsions with repairing and cooling effects, and the formulation of the emulsions is different from that of application example 1 only in that the oil composition of example 1 is replaced by the oil compositions of examples 2 and 3 in equal amounts, and the other components and contents are kept unchanged. The preparation method is described in application example 1.
Comparative application examples 1 to 6
The present comparative application example provides six emulsions, the formulation of which differs from that of application example 1 only in that the oil and fat compositions of example 1 are replaced with the oil and fat compositions of comparative examples 1 to 6, respectively, in equal amounts, with the other ingredients and contents remaining unchanged. The preparation method is described in application example 1.
Application example 4
The present application example provides an emulsion with repairing and cooling effects, the formulation of which is different from that of application example 1 only in that the humectant is different in formulation, no glycerin is contained, and the reduced mass thereof is proportionally distributed to the mass of sodium hyaluronate and erythritol. The other components and the content remain unchanged. The preparation method is described in application example 1.
Application example 5
The present application example provides an emulsion with repairing and cooling effects, the formulation of which is different from that of application example 1 only in that the humectant is different in formulation, sodium hyaluronate is not contained, and the reduced mass thereof is proportionally distributed to the mass of glycerin and erythritol. The other components and the content remain unchanged. The preparation method is described in application example 1.
Application example 6
The present application example provides an emulsion with repairing and cooling effects, the formulation of which is different from that of application example 1 only in that the humectant is different in formulation, erythritol is not contained, and the reduced mass thereof is proportionally distributed to the mass of glycerin and sodium hyaluronate. The other components and the content remain unchanged. The preparation method is described in application example 1.
Application example 7
The application example provides an emulsion with repairing and cooling effects, which comprises the following formula:
the preparation method comprises the following steps:
(1) Mixing the oil composition, the antioxidant and the emulsifier, heating to 80 ℃, uniformly stirring, and preserving heat for 5min to obtain an oil phase; mixing thickener, humectant and water, heating to 85deg.C, stirring, and maintaining the temperature for 15min to obtain water phase;
(2) After the heat preservation is finished, mixing the water phase and the oil phase obtained in the step (1), stirring under vacuum to emulsify for 15min, and preserving heat for 5min;
(3) Cooling to 45deg.C, adding pH regulator, and homogenizing for 1min;
(4) Continuously cooling to 40deg.C, adding antiseptic, chelating agent and plant extract, and stirring.
Application example 8
The application example provides an emulsion with repairing and cooling effects, the formula of the emulsion is different from that of application example 7 only in that the plant extract is different in formula, the emulsion does not contain centella asiatica extract, and the reduced mass of the emulsion is distributed to the mass of the chamomile extract and the flaxseed extract in proportion. The other components and the content remain unchanged. The preparation method is described in application example 7.
Application example 9
The application example provides an emulsion with repairing and cooling effects, the formula of the emulsion is different from that of application example 7 only in that the plant extract is different in formula, the emulsion does not contain the chamomile extract, and the reduced mass of the emulsion is distributed on the mass of the centella extract and the flaxseed extract in proportion. The other components and the content remain unchanged. The preparation method is described in application example 7.
Application example 10
The present application example provides an emulsion with repairing and cooling effects, the formulation of which is different from that of application example 7 only in that the formulation of the plant extract is different, no linseed extract is contained, and the reduced mass thereof is proportionally distributed on the mass of centella asiatica extract and chamomile extract. The other components and the content remain unchanged. The preparation method is described in application example 7.
Test example 1
And (3) testing cooling and repairing efficacy:
after 80 volunteers uniformly clean the left forearm and the right forearm on the curved side, 10 ginseng samples are added to each group of samples after the water is gently sucked by paper towels, 3 areas with the area of 4cm multiplied by 4cm are marked as test areas for each group of samples, at least 2cm is arranged between each area, and the test results are counted as average values. The volunteers were tested for 5min of thermal stimulation with a hot air blower before using the samples, and then the test areas were smeared with the appropriate amounts of the emulsion samples of application examples 1-10 and comparative application examples 1-6, and the control group was not smeared with any samples. Recording the skin temperature change (C., by testing the skin epidermis temperature with an infrared thermometer, including the temperature change before and after use and in the control group), as shown in Table 1; the change of the heme content of the skin (%), the method is that the data acquisition of the subjects is arranged before using the sample and after 10min, 20min and 30min, each time the skin parameter acquisition is carried out by using a skin testing instrument (CK multifunctional skin testing instrument CK-MPA 10), the heme content of the skin is counted, the change of the heme content of the skin after different smearing times is calculated, and the heme content = (heme content after n minutes/heme content before use) ×100% is shown in the table 2:
TABLE 1
TABLE 2
| Group of | 0min | 10min | 20min | 30min |
| Application example 1 | 100％ | 68％ | 45％ | 20％ |
| Application example 2 | 100％ | 70％ | 50％ | 30％ |
| Application example 3 | 100％ | 71％ | 51％ | 29％ |
| Application example 4 | 100％ | 69％ | 53％ | 28％ |
| Application example 5 | 100％ | 67％ | 45％ | 22％ |
| Application example 6 | 100％ | 68％ | 42％ | 21％ |
| Application example 7 | 100％ | 50％ | 35％ | 12％ |
| Application example 8 | 100％ | 61％ | 40％ | 21％ |
| Application example 9 | 100％ | 62％ | 42％ | 20％ |
| Application example 10 | 100％ | 58％ | 35％ | 15％ |
| Comparative application example 1 | 100％ | 82％ | 74％ | 70％ |
| Comparative application example 2 | 100％ | 88％ | 77％ | 70％ |
| Comparative application example 3 | 100％ | 83％ | 71％ | 69％ |
| Comparative application example 4 | 100％ | 91％ | 82％ | 76％ |
| Comparative application example 5 | 100％ | 94％ | 81％ | 79％ |
| Comparative application example 6 | 100％ | 92％ | 80％ | 75％ |
| Control group | 100％ | 95％ | 82％ | 81％ |
As can be seen from the data in tables 1 and 2: the oil composition and the cosmetic containing the oil composition have excellent effects of cooling and removing red blood streaks, and can calm the skin quickly and effectively. And the stearyl heptanoate, the phytosterol, the canola oil glyceride and the jojoba oil in the grease composition have a synergistic effect on the effects. Meanwhile, the plant extract is further added into the product, so that the effect can be promoted.
Test example 2
Moisture efficacy test:
after 80 volunteers uniformly clean the left forearm and the right forearm on the curved side, 10 ginseng samples are added to each group of samples after the water is gently sucked by paper towels, 3 areas with the area of 4cm multiplied by 4cm are marked as test areas for each group of samples, at least 2cm is arranged between each area, and the test results are counted as average values. The test areas were smeared with an appropriate amount of equal amounts of emulsion samples of application examples 1-10 and comparative application examples 1-6. Subject data collection was scheduled before and after 2 hours and 4 hours of use of the sample, each time skin parameter collection was performed using a skin test instrument (Corneometer CM 825), and the skin stratum corneum moisture content increase rate (%) was counted, the increase rate= (moisture content after n hours of use-moisture content before use)/moisture content before use. The results are shown in Table 3.
TABLE 3 Table 3
| Group of | 2h | 4h |
| Application example 1 | 55.3％ | 43.6％ |
| Application example 2 | 52.2％ | 39.1％ |
| Application example 3 | 51.2％ | 38.4％ |
| Application example 4 | 50.8％ | 37.9％ |
| Application example 5 | 50.9％ | 38.5％ |
| Application example 6 | 49.5％ | 36.4％ |
| Application example 7 | 54.2％ | 43.8％ |
| Application example 8 | 54.9％ | 42.6％ |
| Application example 9 | 55.1％ | 42.9％ |
| Application example 10 | 54.6％ | 43.5％ |
| Comparative application example 1 | 23.3％ | 15.5％ |
| Comparative application example 2 | 29.5％ | 18.1％ |
| Comparative application example 3 | 21.8％ | 12.1％ |
| Comparative application example 4 | 14.2％ | 5.1％ |
| Comparative application example 5 | 13.8％ | 3.5％ |
| Comparative application example 6 | 17.4％ | 8.1％ |
As can be seen from the data in table 3: the oil and fat composition and the cosmetic containing the same according to the present invention have excellent moisturizing effects and can maintain the moisture content of the skin horny layer for a long period of time. And the stearyl heptanoate, the phytosterol, the canola oil glyceride and the jojoba oil in the grease composition have a synergistic effect on the effects. Meanwhile, the formula of the humectant also has a certain influence on the moisturizing effect.
Test example 3
Skin irritation experiments:
skin irritation measurement was performed by taking the emulsions of application examples 1 to 10. 50 subjects were selected, and a patch test tape containing 0.03mL of the sample was applied to normal skin of the left and right forearms of the subjects, and the test was performed according to CTFA guidelines (1981) for 6 times within half an hour after the patch was uncovered, and additional tests were performed for the purpose of observing a delayed reaction on the 6 th day after the skin was applied, and the identification criteria are shown in Table 4, and the results are shown in Table 5.
TABLE 4 Table 4
| Grade | (symbol) | Authentication criteria |
| 0 | - | Negative reaction: no irritation and erythema |
| 1 | ± | Suspicious reaction: mild erythema |
| 2 | + | Weak positive reaction: erythema (red spot) |
| 3 | ++ | Strong positive reaction: erythema (red spot)Pimple and blister |
| 4 | +++ | Very positive reaction: severe edema, large foam |
TABLE 5
From the above data results, it can be seen that: the grease composition and the cosmetic containing the grease composition have no stimulation to skin, no positive reaction and mild and no stimulation effects.
The applicant states that the present invention is described by way of the above examples as an oil and fat composition with repairing and cooling effects and its application, but the present invention is not limited to the above examples, i.e. it is not meant that the present invention must be practiced by relying on the above examples. It should be apparent to those skilled in the art that any modification of the present invention, equivalent substitution of raw materials for the product of the present invention, addition of auxiliary components, selection of specific modes, etc., falls within the scope of the present invention and the scope of disclosure.
The preferred embodiments of the present invention have been described in detail above, but the present invention is not limited to the specific details of the above embodiments, and various simple modifications can be made to the technical solution of the present invention within the scope of the technical concept of the present invention, and all the simple modifications belong to the protection scope of the present invention.
In addition, the specific features described in the above embodiments may be combined in any suitable manner, and in order to avoid unnecessary repetition, various possible combinations are not described further.
Claims (18)
1. A grease composition with repairing and cooling effects is characterized in that,
the preparation raw materials of the grease composition with repairing and cooling effects comprise, by mass, 1-10 parts of white pool flower seed oil, 1-5 parts of prinsepia utilis royle oil, 1-20 parts of squalane, 1-15 parts of stearyl heptanoate, 1-10 parts of phytosterol canola oil glyceride and 1-20 parts of jojoba oil.
2. The oil and fat composition with repairing and cooling effects according to claim 1, wherein the oil and fat composition with repairing and cooling effects is obtained by physically and uniformly mixing all the preparation raw materials.
3. Use of the oil and fat composition with repairing and cooling effects according to any one of claims 1-2 in the preparation of cosmetics.
4. The use according to claim 3, wherein the cosmetic is an emulsion, a face cream, a face mask, a sun cream, an essence, a make-up remover.
5. The use according to claim 3, wherein the oil and fat composition having the efficacy of repairing and cooling is contained in the cosmetic in an amount of 10 to 40% by mass.
6. An emulsion with repairing and cooling effects is characterized by comprising, by mass, 10-40% of the grease composition with repairing and cooling effects described in any one of claims 1-2, 1-10% of an emulsifying agent, 0.1-2% of a thickening agent, 3-15% of a humectant, 0.2-1% of an antioxidant and water.
7. The emulsion with repairing and cooling effects according to claim 6, further comprising a plant extract, wherein the plant extract comprises centella asiatica extract, chamomile extract and flaxseed extract.
8. The emulsion with repair cooling effect according to claim 6, further comprising any one or a combination of at least two of a whitening effect active, an antioxidant effect active or an anti-glycation effect active.
9. The emulsion with repairing and cooling effects according to claim 6, further comprising any one or a combination of at least two of a preservative, a pH adjuster, a chelating agent and a fragrance.
10. The emulsion with repairing and cooling effects according to claim 6, wherein the emulsifier is selected from any one or a combination of at least two of glycerol stearate, C12-20 alkyl glucoside, coco glucoside, polyglycerol-3 methyl glucose distearate, sucrose stearate or hydrogenated lecithin.
11. The emulsion with repairing and cooling effects according to claim 6, wherein the thickener is selected from any one or a combination of at least two of carbomers, tara gum, ammonium acryloyldimethyl taurate/behenate polyether-25 methacrylate cross-linked polymer, acrylic acid (esters) type/C10-30 alkanol acrylate cross-linked polymer, sclerotium gum or pectin.
12. The emulsion with repairing and cooling effects according to claim 6, wherein the humectant is selected from any one or a combination of at least two of glycerin, butylene glycol, propylene glycol, sodium hyaluronate, erythritol, trehalose, or dextran.
13. The emulsion with repairing and cooling effects according to claim 12, wherein the humectant is a combination of glycerin, sodium hyaluronate and erythritol.
14. The emulsion having a repairing and cooling effect according to claim 6, wherein the antioxidant is selected from the group consisting of ethyl tocopheryl acetate.
15. The method for preparing an emulsion with repairing and cooling effects according to any one of claims 6 to 14, wherein the preparation method comprises:
(1) Mixing the oil composition, the antioxidant and the emulsifier to obtain an oil phase; mixing a thickener, a humectant and water to obtain a water phase;
(2) Mixing the water phase and the oil phase obtained in the step (1) and emulsifying to obtain the water-phase-oil emulsion.
16. The method for preparing an emulsion with repairing and cooling effects according to claim 15, wherein the oil phase is heated to 70-85 ℃; the aqueous phase is prepared by heating to 80-90 ℃.
17. The method for preparing an emulsion with repairing and cooling effects according to claim 15, wherein the emulsification is performed at 70-90 ℃ for 5-15 min.
18. The method of claim 15, further comprising mixing the emulsified emulsion with any one or a combination of at least two of a plant extract, a whitening active, an antioxidant active, an anti-glycation active, a preservative, a pH adjuster, a chelating agent, and a fragrance.
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| CN202211414863.4A CN115645311B (en) | 2022-11-11 | 2022-11-11 | Grease composition with repairing and cooling effects and application thereof |
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Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105411865A (en) * | 2015-12-11 | 2016-03-23 | 诺斯贝尔化妆品股份有限公司 | Multi-effect moisturizing microemulsion essence containing multiple vegetable oil and fat |
| CN107661226A (en) * | 2017-08-24 | 2018-02-06 | 广州神采化妆品有限公司 | It is a kind of to smear water outlet cream changed and cooled rapidly and preparation method thereof |
| CN108379124A (en) * | 2018-04-13 | 2018-08-10 | 珠海伊斯佳科技股份有限公司 | Essential oils and its preparation method and application for preventing and repairing skin barrier damage |
| CN111067832A (en) * | 2020-01-08 | 2020-04-28 | 澳宝化妆品（惠州）有限公司 | Facial care product for repairing sensitive skin and resisting premature senility |
| CN111700826A (en) * | 2020-06-19 | 2020-09-25 | 泉后(广州)生物科技研究院有限公司 | Composition for repairing skin barrier and preparation method and application thereof |
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Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105411865A (en) * | 2015-12-11 | 2016-03-23 | 诺斯贝尔化妆品股份有限公司 | Multi-effect moisturizing microemulsion essence containing multiple vegetable oil and fat |
| CN107661226A (en) * | 2017-08-24 | 2018-02-06 | 广州神采化妆品有限公司 | It is a kind of to smear water outlet cream changed and cooled rapidly and preparation method thereof |
| CN108379124A (en) * | 2018-04-13 | 2018-08-10 | 珠海伊斯佳科技股份有限公司 | Essential oils and its preparation method and application for preventing and repairing skin barrier damage |
| CN111067832A (en) * | 2020-01-08 | 2020-04-28 | 澳宝化妆品（惠州）有限公司 | Facial care product for repairing sensitive skin and resisting premature senility |
| CN111700826A (en) * | 2020-06-19 | 2020-09-25 | 泉后(广州)生物科技研究院有限公司 | Composition for repairing skin barrier and preparation method and application thereof |
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