CN115569091B - Millettia speciosa and noni enzyme facial cleanser - Google Patents
Millettia speciosa and noni enzyme facial cleanser Download PDFInfo
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- CN115569091B CN115569091B CN202110688906.7A CN202110688906A CN115569091B CN 115569091 B CN115569091 B CN 115569091B CN 202110688906 A CN202110688906 A CN 202110688906A CN 115569091 B CN115569091 B CN 115569091B
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- NJKOMDUNNDKEAI-UHFFFAOYSA-N beta-sitosterol Natural products CCC(CCC(C)C1CCC2(C)C3CC=C4CC(O)CCC4C3CCC12C)C(C)C NJKOMDUNNDKEAI-UHFFFAOYSA-N 0.000 description 1
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- FWYIBGHGBOVPNL-UHFFFAOYSA-N scopoletin Natural products COC=1C=C2C=CC(OC2=C(C1)O)=O FWYIBGHGBOVPNL-UHFFFAOYSA-N 0.000 description 1
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- KZJWDPNRJALLNS-VJSFXXLFSA-N sitosterol Chemical compound C1C=C2C[C@@H](O)CC[C@]2(C)[C@@H]2[C@@H]1[C@@H]1CC[C@H]([C@H](C)CC[C@@H](CC)C(C)C)[C@@]1(C)CC2 KZJWDPNRJALLNS-VJSFXXLFSA-N 0.000 description 1
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- 239000011734 sodium Substances 0.000 description 1
- 229910052708 sodium Inorganic materials 0.000 description 1
- NZTBZLYGWJBIJE-UHFFFAOYSA-M sodium 1-oxododecane-1-sulfonate Chemical compound [Na+].CCCCCCCCCCCC(=O)S([O-])(=O)=O NZTBZLYGWJBIJE-UHFFFAOYSA-M 0.000 description 1
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- YIBXWXOYFGZLRU-UHFFFAOYSA-N syringic aldehyde Natural products CC12CCC(C3(CCC(=O)C(C)(C)C3CC=3)C)C=3C1(C)CCC2C1COC(C)(C)C(O)C(O)C1 YIBXWXOYFGZLRU-UHFFFAOYSA-N 0.000 description 1
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- VZCYOOQTPOCHFL-UHFFFAOYSA-N trans-butenedioic acid Natural products OC(=O)C=CC(O)=O VZCYOOQTPOCHFL-UHFFFAOYSA-N 0.000 description 1
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Classifications
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9789—Magnoliopsida [dicotyledons]
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q1/00—Make-up preparations; Body powders; Preparations for removing make-up
- A61Q1/14—Preparations for removing make-up
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/10—Washing or bathing preparations
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/59—Mixtures
- A61K2800/592—Mixtures of compounds complementing their respective functions
- A61K2800/5922—At least two compounds being classified in the same subclass of A61K8/18
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/80—Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
- A61K2800/85—Products or compounds obtained by fermentation, e.g. yoghurt, beer, wine
Landscapes
- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Veterinary Medicine (AREA)
- Public Health (AREA)
- General Health & Medical Sciences (AREA)
- Animal Behavior & Ethology (AREA)
- Botany (AREA)
- Birds (AREA)
- Epidemiology (AREA)
- Mycology (AREA)
- Microbiology (AREA)
- Biotechnology (AREA)
- Engineering & Computer Science (AREA)
- Dermatology (AREA)
- Cosmetics (AREA)
Abstract
The invention relates to a millettia speciosa champ facial cleanser. The noni enzyme facial cleanser, the millettia speciosa fruit enzyme facial cleanser and the millettia speciosa enzyme facial cleanser disclosed by the invention are in cream yellow paste, have light fragrance, are uniform and fine in texture, have no tight feel on the skin after being used, have good cleansing and cleansing capability, heat resistance, cold resistance, stability and neutral pH, and accord with QB/T29680-2013.
Description
Technical Field
The invention belongs to the field of daily chemicals, and particularly relates to a millettia speciosa champ facial cleanser.
Background
Radix et rhizoma Rhei (Millettia Speciose Champ), also known as radix Ardisiae Japonicae, jin Zhonggen, herba Ardisiae Japonicae, radix et rhizoma Gaultheriae Yunnanensis, rhizoma Nelumbinis, radix et rhizoma Gaultheriae Yunnanensis, radix et rhizoma Solani Tuber osi, and herba seu radix Kadsurae Longipedunculatae, belonging to plant kingdom, seed plant, dicotyledonous plant, and dried root of herba Adianti of genus Adianti of family Leguminosae [1] . The cattle are mainly grown on roadsides, valleys, wild fields, forests or bushes, the main planting places of China are Guangdong, guangxi, fujian, hunan, hainan, guizhou, yunnan and other places, and the Guangdong province is mainly distributed in the west, south and middle areas of the Guangdong [2] . The main place of production is Vietnam abroad.
The research on the millettia speciosa and the chemical components of the millettia speciosa is very great at home and abroad, the millettia speciosa is recorded as a health-care food material in the open-cut generation of China, and the medical history can be traced back to the records of the Chinese herbal medicine and the Chinese herbal medicine preparation [3] . In the experiment of researching and developing the chemical composition and pharmacological action of the Oriental millettia root, the Oriental millettia root is found to contain various chemical compositions such as various flavonoids, lignin, polysaccharides, triterpenes, alkaloid compounds and the like [3] . In addition, oriental millettia contains a large amount of organic acids such as syringic acid, gentisic acid, maleic acid, pyracanthc acid, linoleic acid, etc [4] . Herb of Fangcao and the like [5] Among the different producing places of the millettia speciosa champ, it was identified that the millettia speciosa champ contains a large amount of proteins, starches, amino acids, total dietary fibers, vitamin B2, sugars, vitamin C. In many research knots on pharmacological actions of radix et rhizoma RheiThe results show that the chemical components contained in the millettia speciosa champ have obvious effects of resisting oxidation, inflammation, tumor, fatigue and stress, enhancing the immunoregulation, eliminating phlegm, relieving cough, relieving asthma, protecting liver and the like [6-9] . Chen Rongrong, etc [10] Through experiments, the in-vitro antioxidant activity of different components of the millettia speciosa champ is detected, and the experimental results show that the aqueous extract and the alcohol extract of the millettia speciosa champ have certain lipid peroxidation resistance and free radical removal effects, the effect of the aqueous extract of the millettia speciosa champ is better than that of the alcohol extract, but the crude polysaccharide has the weakest antioxidant and free radical removal effects. Chen Xiaobai, etc [11] Pharmacological experiment results show that the millettia speciosa champ has the effect of resisting radiation.
Noni (Morinda citrifolia Linn), also known as Noni, morinda citrifolia, is of the family Rubiaceae. Mainly distributed in subtropical and tropical regions such as Indonesia, australia, hawaiian islands, etc., and the noni regions mainly planted in China have Sisha islands, hainan islands, etc [12] . Noni contains abundant nutrients including 5 kinds of essential nutrients required for human body, and contains abundant effective nutrients such as carbohydrate, mineral, vitamins, amino acids, proteins, microelements, polysaccharide, phenols, methylcoumarin, beta-sitosterol, saponin, antioxidant substances, alizarin, flavonoids, anthraquinone and scopoletin bioactive substances [13] 。
Noni has antibacterial effect, and has been shown by research and experiment results to have an inhibitory effect on the growth of specific microorganisms, such as Shigella, salmonella, escherichia coli, helicobacter pylori, pseudomonas aeruginosa, bacillus subtilis, staphylococcus aureus, etc [13] 。
Noni has oxidation resistance, and related experimental researchers test and evaluate the oxidation resistance of n-butanol extract of noni fruits and the monomer compounds extracted from noni fruits through five oxidation resistance experimental methods such as ABTS free radical scavenging rate, hydroxyl free radical scavenging rate, DPPH free radical scavenging rate, copper ion reducing power and total reducing power [14] 。
Noni has antiinflammatory and analgesic effects, and has been found by students to be effective in treating inflammation-induced problems due to local severe inflammatory reaction caused by high inflammatory agent, and has certain antiinflammatory effect [15] . Zhang Weimin, etc [16] By acting on mice with noni root extract, experimental results show that noni root extract has remarkable analgesic and sedative effects on mice, while noni extract is nontoxic and has no side effects.
The ferment is mainly an edible product which is beneficial to human body by fermenting available medicinal materials and fruits and vegetables under certain conditions through edible strains [17] . The ferment can be taken properly by human body to delay the aging of the organism and prolong the life of people [18] . Enzymes (enzymes) refer to various active substances and enzymes produced by the enzyme microorganisms during their activities, also collectively referred to as enzymes [19] . Because the microbial enzyme is produced by natural ferment bacteria, the microbial enzyme has no side effect and is favored by people, especially female groups [20,21] . For different types of Chinese medicinal materials, the Chinese medicinal materials have different effects, and researches show that some Chinese medicinal materials can effectively promote metabolism of cells and delay aging of skin [22] 。
In the cosmetic industry, facial cleanser is favored by people for moisturizing, decontaminating, and removing oil. However, as the economic level of China is increasingly improved, the living standard of people is continuously improved, and the requirements of people on beauty and skin care are also higher and higher. People are continuously aware that a certain potential safety hazard exists when the facial cleanser containing the chemical is used for a long time. Therefore, more and more people will choose facial cleanser containing traditional Chinese medicine components. Compared with chemical cosmetics, the traditional Chinese medicine type cosmetics have the characteristics of small side effect, high safety performance, nature, no toxicity, small side effect and the like [23] 。
Based on the above, the applicant's prior patent applications (application numbers CN202110562491.9, CN 202110556369.0) prepared noni ferment, millettia-fruit composite ferment, millettia-noni composite ferment and related sun-screening products, the invention further discloses a facial cleanser containing noni ferment, millettia-fruit composite ferment and millettia-noni composite ferment. And the related measurement is carried out on the aspects of moisturizing activity, water loss rate, deoiling property, detergency, cleansing ability, stability of the facial cleanser and the like of the facial cleanser, so that the composite enzyme has good development prospect in the field of cosmetics.
Disclosure of Invention
The invention provides an enzyme facial cleanser, which is characterized by comprising the following components in percentage by weight:
the ferment is selected from one or more of noni ferment, oriental-fruit composite ferment and Oriental-noni composite ferment.
Another embodiment of the present invention provides the ferment facial cleanser, which is characterized by being prepared according to the following method: heating the phase A at the temperature of 85-95 ℃ according to the formula proportion, stirring for 40-60min, adding the phase B which is preheated and dissolved uniformly, stirring uniformly, stopping heating, adding the phase C which is prepared in advance, continuing stirring until the liquid level is bubble-free, adding the phase D which is prepared in advance under high-speed stirring when the temperature is reduced to 50 ℃, stirring uniformly, reducing the stirring speed, continuing stirring until the temperature is reduced to 45 ℃, adding the phase E which is prepared in advance, stirring continuously at the stirring speed until the temperature is lower than 37 ℃, discharging, obtaining the flowable paste after discharging, and standing the paste at room temperature for 1-2 days to form the enzyme facial cleanser.
The B phase which is preheated and dissolved uniformly can be selected from the B phase components which are dissolved and mixed uniformly under the temperature condition of above the melting point temperature (preferably 85-95 ℃).
The high-speed stirring is selected from stirring speeds of 400-600rpm, and the stirring speed is reduced to 100-200rpm.
Another embodiment of the present invention provides a method for preparing the ferment facial cleanser, which is characterized by comprising the following steps: heating the phase A at the temperature of 85-95 ℃ according to the formula proportion, stirring for 40-60min, adding the phase B which is preheated and dissolved uniformly, stirring uniformly, stopping heating, adding the phase C which is prepared in advance, continuing stirring until the liquid level is bubble-free, adding the phase D which is prepared in advance under high-speed stirring when the temperature is reduced to 50 ℃, stirring uniformly, reducing the stirring speed, continuing stirring until the temperature is reduced to 45 ℃, adding the phase E which is prepared in advance, stirring continuously at the stirring speed until the temperature is lower than 37 ℃, discharging, obtaining the flowable paste after discharging, and standing the paste at room temperature for 1-2 days to form the enzyme facial cleanser.
The B phase which is preheated and dissolved uniformly can be selected from the B phase components which are dissolved and mixed uniformly under the temperature condition of above the melting point temperature (preferably 85-95 ℃).
The high-speed stirring is selected from stirring speeds of 400-600rpm, and the stirring speed is reduced to 100-200rpm.
Another embodiment of the invention provides an application of the ferment facial cleanser in preparing daily necessities for degreasing and/or cleansing.
Another embodiment of the invention provides the use of noni ferment, millettia speciosa champ-fruit composite ferment, millettia speciosa champ-noni composite ferment in the preparation of degreasing and/or makeup-removing daily chemicals. The daily chemical product for removing greasy dirt and/or cleansing is preferably a hand cleanser, a facial cleanser, cleansing water and the like. The formula of the degreasing and/or cleansing daily chemical product is as follows:
the preparation method comprises the following steps: heating the phase A at the temperature of 85-95 ℃ according to the formula proportion, stirring for 40-60min, adding the phase B which is preheated and dissolved uniformly, stirring uniformly, stopping heating, adding the phase C which is prepared in advance, continuing stirring until the liquid level is bubble-free, adding the phase D which is prepared in advance under high-speed stirring when the temperature is reduced to 50 ℃, stirring uniformly, reducing the stirring speed, continuing stirring until the temperature is reduced to 45 ℃, adding the phase E which is prepared in advance, stirring continuously at the stirring speed until the temperature is lower than 37 ℃, discharging, obtaining the flowable paste after discharging, and standing the paste at room temperature for 1-2 days to form the enzyme facial cleanser.
The B phase which is preheated and dissolved uniformly can be selected from the B phase components which are dissolved and mixed uniformly under the temperature condition of above the melting point temperature (preferably 85-95 ℃).
The high-speed stirring is selected from stirring speeds of 400-600rpm, and the stirring speed is reduced to 100-200rpm.
The noni ferment, the millettia speciosa-fruit composite ferment and the millettia speciosa-noni composite ferment are prepared by the method of the previous Chinese patent application No. CN202110562491.9 and CN202110556369.0 (in particular the method of the preparation examples 1-5 in the example 1).
Drawings
Fig. 1 is an in vitro moisture retention plot for each sample with rh=43%;
fig. 2 is a graph of relative humidity rh=84% in vitro moisture retention of each sample;
fig. 3 is a graph of relative humidity rh=43% water loss for each sample;
fig. 4 is a graph of relative humidity rh=84% water loss for each sample;
FIG. 5 is a plot of the smear before the experiment;
fig. 6 is a graph of the smear after the experiment.
Detailed Description
2.1 laboratory apparatus, reagents and raw materials
2.1.1 instruments
Table 1 meter for instrument
2.1.2 reagents
Hondu PCP 30 (potassium cocoyl hydrolyzed oat protein); hondu LT-40 (sodium lauroyl sulfonate); hondu LS-30 (sodium lauroyl aminoacid); HC-10PLUS (disodium lauryl sulfosuccinate); the above reagents were obtained from Guangzhou Hongall fine chemical Co.
MP (methyl paraben); SF-1 (acrylate copolymer emulsion); protectol PES (phenoxyethanol), the above agents were sourced from Guangzhou Bano cosmetic Co., ltd.
Glycerol (glycerol); tetradecanoic acid; dodecanoic acid; naCl; EDTA-2Na, the above reagents were derived from the materialization laboratory.
2.2 preparation of facial cleanser
Preparation of 100g of substrate facial cleanser sample
Table 2 substrate facial cleanser formulation
The general preparation method comprises the following steps: heating the phase A at the temperature of 85-95 ℃ according to the formula proportion, stirring for 40-60min, adding the phase B which is preheated and dissolved uniformly, stirring uniformly, stopping heating, adding the phase C which is prepared in advance, continuing stirring until the liquid level is bubble-free, adding the phase D which is prepared in advance under high-speed stirring when the temperature is reduced to 50 ℃, stirring uniformly, reducing the stirring speed, continuing stirring until the temperature is reduced to 45 ℃, adding the phase E which is prepared in advance, stirring continuously at the stirring speed until the temperature is lower than 37 ℃, discharging, obtaining the flowable paste after discharging, and standing the paste at room temperature for 1-2 days to form the enzyme facial cleanser. The B phase which is preheated and dissolved uniformly can be selected from the B phase components which are dissolved and mixed uniformly under the temperature condition of above the melting point temperature (preferably 85-95 ℃). The high-speed stirring is selected from stirring speeds of 400-600rpm, and the stirring speed is reduced to 100-200rpm.
And respectively taking noni enzyme, millettia speciosa champ-fruit composite enzyme and millettia speciosa-noni composite enzyme prepared in the previous patent methods of the applicant, and preparing corresponding facial cleanser according to the general method, wherein the noni enzyme facial cleanser is referred to as a sample A, the millettia speciosa champ is referred to as a sample B, the millettia speciosa-fruit composite enzyme facial cleanser is referred to as a sample C and the millettia speciosa-noni composite enzyme facial cleanser is referred to as a sample D. The commercial beauty Befei milk facial cleanser was designated as commercial facial cleanser 1, and the commercial one-leaf facial cleanser was designated as commercial facial cleanser 2.
2.4 in vitro moisture Performance determination
At room temperature (24 ℃) 1.5g of self-made facial cleanser, one leaf facial cleanser sold in the market and one face cleanser sold in the market are weighed, two medical breathable adhesive tapes (3M adhesive tapes) are adhered to dry and clean glass slides to simulate skin tissues of a human body, the facial cleanser is uniformly smeared on the treated glass slides, and the glass slides are respectively placed in two dryers, wherein the relative humidity of one dryer is RH=43% (saturated calcium chloride solution) and the relative humidity of the other dryer is RH=84% (saturated ammonium sulfate solution). The quality of the weighing bottle is changed at 20,40, 60, 80, 100, 120, 140, 160 and 180min, and the quality of the facial cleanser before being placed is m 0 (g) The quality of the placed facial cleanser is m n (g) A. The invention relates to a method for producing a fibre-reinforced plastic composite The moisture retention was calculated according to equation (1).
Moisture retention= (m) n /m 0 )×100％ (1)
2.5 determination of Water loss
At room temperature (24 ℃) 2g of self-made facial cleanser with different formulations, one leaf facial cleanser sold in the market and one body facial cleanser sold in the market are weighed into weighing bottles, the weighing bottles are respectively placed into two dryers, the relative humidity of one dryer is RH=43% (saturated calcium chloride solution), and the relative humidity of the other dryer is RH=84% (saturated calcium chloride solution)And ammonium sulfate solution). Measuring the change of the quality of the weighing bottle at 2,4, 6, 8, 10, 12, 24, 48, 72, 96 and 120 hours, and accurately measuring the quality of the facial cleanser before being placed to be m 0 (g) The quality of the placed facial cleanser is m n (g) A. The invention relates to a method for producing a fibre-reinforced plastic composite The water loss rate was calculated according to formula (2).
Water loss = [ (m) 0 -m n )/m 0 ]×100％ (2)
2.6 determination of deoiling Properties
Determination of oil removal Capacity: reference is made to the literature [24] The method is properly adjusted, 1g of facial cleanser sample is weighed, 10g of water is added to dissolve and dilute the facial cleanser sample into 10% solution, vegetable oil is dripped into the diluted solution at 25 ℃ to dissolve the vegetable oil until the vegetable oil is not dissolved in the solution, and the mass of the vegetable oil consumed when the last drop just reaches a saturated state is weighed.
Determination of degreasing ability at different temperatures: 1g of facial cleanser sample is weighed, 10g of water is added to dissolve and dilute the facial cleanser sample into 10% solution, the 10% solution is respectively placed in water baths at 35, 40, 45 and 50 ℃ and heated for 5min, vegetable oil is added dropwise into the diluted solution to dissolve the vegetable oil until the solution is not dissolved, and the mass of the vegetable oil consumed by the last drop just reaching the saturated state is weighed.
2.7 determination of make-up removal Capacity
The medical adhesive tape is stuck on a glass slide to imitate human skin, a rectangular area with the length of 1 cm or 4cm is selected on the medical adhesive tape to be marked, and lipstick is uniformly smeared in the rectangular area. And (3) smearing 0.04g of sample on the medical adhesive tape smeared with lipstick, slightly kneading for 2min, cleaning with tap water, and comparing the marks of lipstick marks before and after cleaning. The comparative experiment was performed with an equal amount of makeup remover (clean and soft makeup remover available on the market) and the blank experiment was performed with an equal amount of water.
2.8 measurement of surface tension
2.0g of facial cleanser is weighed under the environment of 25 ℃ and diluted into 40mL of 5% diluted solution, and the surface tension of samples with different concentrations is measured according to the volume ratio of the samples to water of 1:9, 2:8, 3:7, 4:6, 5:5 and 6:4 respectively and marked as 1-6 respectively.
The surface tension instrument container and capillary tube are cleaned and dried, and whether the instrument leaks air is checked. Distilled water is added dropwise to the surface tensiometer and the liquid level is adjusted so that it is tangential to the capillary [25]. And (3) adjusting the air extraction speed to make the air bubbles at the opening of the air bubble capillary uniformly emerge, recording the maximum pressure difference, continuously measuring for three times, and taking an average value.
Distilled water in the surface tensiometer was taken out. Firstly, a sample is used for washing a surface tension meter, samples 1, 2, 3 and 4, a commercially available facial cleanser 1 and a commercially available facial cleanser 2 are respectively added, the maximum pressure difference is measured, three times of continuous measurement are carried out, and the average value is obtained.
2.9 determination of foamability and bubble stability
2g of facial cleanser was dissolved in water to give a 10% diluted solution, which was then added to a 250mL cylinder with a piston, and the cylinder was shaken up and down 10 times with even force, and the height of the highest air bubbles was recorded. Standing for 10min, and comparing the heights of the bubbles after standing. Three parallel experiments were performed and the average value was determined.
2.10 organoleptic index and physicochemical Standard detection
2.10.1 sensory index detection
2.0g of facial cleanser is weighed and placed on a clean and dry surface dish, and the appearance of the facial cleanser is observed to have fragrance. Then 0.5g of facial cleanser is weighed and evenly smeared on the back of the hand to feel the fineness of the facial cleanser.
2.10.2 physical and chemical Properties detection
Cold resistance experiment: 2.0g of facial cleanser is weighed and placed in a dry weighing bottle, placed in a condition of minus 12+/-2 ℃, kept stand for 24 hours, taken out, and restored to room temperature, and whether the sample has obvious difference from the sample before the experiment is observed in the period.
Heat resistance experiment: 2.0g of facial cleanser is weighed and placed in a dry weighing bottle, placed in a condition of 42+/-2 ℃, kept stand for 24 hours, taken out, and restored to room temperature, and whether the sample has obvious difference from the sample before the experiment is observed in the period.
Centrifugal stability: weighing a certain amount of facial cleanser, centrifuging at 3500r/min for 30min, taking out, and observing whether the sample has delamination phenomenon and water precipitation.
Determination of pH: 1.0g of facial cleanser is accurately weighed by a dilution method, 10.0g of distilled water is placed in a small beaker, the solution is continuously stirred until the solution is uniform, the pH of the solution is measured by a pH meter for three times, and the average value is obtained.
3 experimental results and discussion
3.1 moisture retention
Table 3 rh=43% in vitro moisture retention for each sample
In vitro moisturizing experiments were performed for 180min in an environment with rh=43%, as can be seen from table 3, fig. 1: the moisturizing rate of each facial cleanser is kept above 90% after 180min, wherein the market facial cleanser used in the experiment has stronger moisturizing capability. In the self-made facial cleanser, the sample D, namely the oregano enzyme facial cleanser, has good moisture retention, and the moisture retention rate can reach 93.69% after 180 minutes. In this in vitro moisturizing experiment, the overall trend of the moisturizing ability is as follows: commercially available facial cleanser 2> commercially available facial cleanser 1> sample D > sample A > sample C > sample B, i.e., oregano enzyme facial cleanser > noni enzyme facial cleanser > oregano fruit enzyme facial cleanser > oregano enzyme facial cleanser.
Table 4 RH =84% in vitro moisture retention of each sample
In vitro moisturizing experiments were performed for 180min in an environment with rh=84%, as can be seen from table 4, fig. 2: after 180min, the moisture retention rate of the facial cleanser is kept above 94%, wherein the market facial cleanser used in the experiment shows strong moisture absorption capacity; in the self-made facial cleanser, the sample D, namely the Dali noni enzyme facial cleanser, has good moisturizing property, and the moisturizing rate after 180 minutes can reach 96.47 percent. In this in vitro moisturizing experiment, the overall trend of the moisturizing ability is as follows: commercially available facial cleanser 2> commercially available facial cleanser 1> sample D > sample A > sample C > sample B, i.e., oregano enzyme facial cleanser > noni enzyme facial cleanser > oregano fruit enzyme facial cleanser > oregano enzyme facial cleanser.
3.2 Water loss Rate
Table 5 RH =43% water loss rate for each sample
As can be seen from table 5 and fig. 3, the water loss measurement was performed for 120 hours in the environment of rh=43%: the water loss rate of the self-made facial cleanser after 120 hours is kept above 40%, wherein the water loss rate of the market facial cleanser used in the experiment is 26.56% and 16.57% respectively, and the water loss capability is weaker. The water loss rate of the self-made facial cleanser after 120 hours can reach 45.85 percent at most. In the water loss experiment, the total trend of the water loss capacity of each facial cleanser is as follows: sample C > sample B > sample A > sample D > market-available facial cleanser 1> market-available facial cleanser 2, i.e., dali fruit ferment facial cleanser > Dali ferment facial cleanser > noni ferment facial cleanser > Dali noni ferment facial cleanser.
Table 6 RH =84% water loss rate for each sample
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As can be seen from table 6 and fig. 4, the water loss experimental measurement was performed for 120 hours in the environment of rh=84%: the water loss rate of the self-made facial cleanser after 120 hours is kept above 10%, wherein the market facial cleanser used in the experiment has the characteristic of moisture absorption and has weaker water loss capability. The water loss rate of the self-made facial cleanser after 120 hours can reach 20.64 percent at most. In the water loss experiment, the total trend of the water loss capacity of each facial cleanser is as follows: sample B > sample C > sample a > sample D > market-available facial cleanser 1> market-available facial cleanser 2, i.e., oregano ferment facial cleanser > oregano ferment facial cleanser.
3.3 deoiling Activity
3.3.1 evaluation of oil removal ability
TABLE 7 quality of the dissolved oil for each sample
Experimental results show that the noni enzyme facial cleanser, the Dali fruit enzyme facial cleanser and the Dali noni enzyme facial cleanser all have certain degreasing capability. As can be seen from Table 7, sample A, namely noni enzyme facial cleanser, has the strongest degreasing ability at room temperature; the sample C with the weakest degreasing capability is the milk cleanser with the enzyme of the Dahurian fruits; the four different ferment facial washes have stronger degreasing capability than the commercially available facial washes of the 2 nd facial washes of the same type, the facial washes of the 4 formulations of the homemade type.
3.3.2 deoiling ability at different temperatures
TABLE 8 quality of the dissolved oil for each sample
As is clear from Table 8, the facial cleanser used in the present experiment had different degreasing capabilities at different temperatures, and the mass of the facial cleanser dissolved oil increased as the temperature increased. The degreasing capacity at the same temperature is as follows: sample a > sample D > sample B > sample C > market-ready facial cleanser 1> market-ready facial cleanser 2, i.e., noni enzyme facial cleanser > orexin fruit enzyme facial cleanser > market-ready facial cleanser 1> market-ready facial cleanser 2.
3.4 evaluation of Makeup removal ability
It is found from fig. 5 and 6 that the noni enzyme facial cleanser, the millettia speciosa champ and the millettia speciosa champ have a certain makeup removing capability through a blank control experiment, wherein the sample A, i.e. the noni enzyme facial cleanser and the sample D, i.e. the millettia speciosa champ, have a makeup removing capability which is higher than that of a commercially available facial cleanser and a clean and soft makeup removing capability which is higher than that of a commercially available clean and soft makeup removing water, and the sample C, i.e. the millettia speciosa champ, and the sample B, i.e. the makeup removing capability of the millettia speciosa champ, have no obvious difference. In the test of the makeup removing capability, the 3M medical adhesive tape which uses the makeup removing water to gently simulate the human skin is found to have a large amount of burrs, while the four self-made facial washes have little or no burrs, and experiments show that the self-made facial washes are more mild than the clean and soft makeup removing water.
3.5 surface tension
TABLE 9 surface tension of various samples
As can be seen from Table 9, the surface tension of each sample decreases with increasing sample concentration, and when the concentration reaches 60%, the surface tension of sample A (noni enzyme facial cleanser) is 2.167X 10-2 (N/m); the surface tension at the same concentration is as follows: market facial cleanser 1> sample B > market facial cleanser 2> sample C > sample D > sample a, i.e., market facial cleanser 1> oregano ferment facial cleanser > market facial cleanser 2> oregano ferment facial cleanser.
The concentration has a great influence on the surface tension, and the smaller the surface tension, the more wetting ability to an object is enhanced, and the greater the penetration to stains, the more easily dissolved [25]. That is, the facial cleanser containing noni enzyme alone has the minimum surface tension, and the higher the surface tension, the poorer the wetting ability against stains, that is, the poorer the detergency.
3.6 foamability and foam stability evaluation
Table 10 foaming and foam stability properties of each sample
Table 10 shows that the four types of facial washes prepared by the laboratory have a certain foaming capacity and are stronger than two types of commercially available facial washes used in the experiment. The foaming capacity is as follows: sample a > sample B > sample D > sample C > market facial cleanser 2> market facial cleanser 1, i.e., noni enzyme facial cleanser > orexin fruit enzyme facial cleanser > market sold facial cleanser 2; in combination with tables 8 and 9, fig. 5 and 6 show that the degreasing and cleansing ability of the facial cleanser is not necessarily linked to the foaming ability of the facial cleanser.
After 10 minutes, the volume of the foam is recorded, and the heights of bubbles of the four types of facial cleanser prepared by a laboratory are still higher than those of two types of commercially available facial cleanser used in the experiment, wherein the foam height of the sample A, namely noni enzyme facial cleanser, is highest, and the foam height of the sample B, namely Dahurian enzyme is lowest; after 10min, the market facial cleanser 2 with the largest difference in foam height from the original foam height was designated as market facial cleanser 2, and the sample C with the smallest difference in foam height was designated as Dahurian fruit ferment. The sequence of the change values is as follows: market facial cleanser 2> sample B > sample a > market facial cleanser 1> sample D > sample C, i.e., market facial cleanser 2> oregano ferment facial cleanser > noni ferment facial cleanser > market facial cleanser 1> oregano ferment facial cleanser > oregano ferment fruit ferment facial cleanser.
3.7 sensory index evaluation
Table 11 sensory indices of each sample
The results in Table 11 show that the four self-made facial washes are milky yellow uniform pastes with light fragrance, while the two commercially available facial washes used in the experiment are milky white uniform pastes, one with milky fragrance and the other with fragrance; the six types of facial cleanser find that the skin is smooth and smooth without tightening after use.
3.8 evaluation of physicochemical Properties
Table 12 stability properties of each sample
The results in Table 12 show that the millettia speciosa champ, the noni speciosa champ, and the millettia speciosa champ have better heat resistance and cold resistance. In addition, after the six types of facial washes were centrifuged at 3500r/min for 20min, each of the six types of facial washes was found to have no delamination phenomenon and was analyzed without water. In summary, the analysis shows that all four facial washes prepared by the laboratory have good stability.
Sample A, sample B, sample D, namely noni ferment facial cleanser, millettia speciosa champ ferment facial cleanser, the dilute solution of millettia speciosa champ ferment facial cleanser is weak acid, sample C, namely the dilute solution of millettia speciosa champ ferment is neutral, the dilute solutions of two commercially available facial cleansers used in the experiment are weak alkaline; compared with the commercial flour, the noni ferment facial cleanser, the millettia speciosa ferment facial cleanser and the millettia speciosa ferment facial cleanser are nearly neutral, are mild in use and are easy to maintain skin.
4. Summary
The experimental study is to improve the traditional facial cleanser and add ferment containing traditional Chinese medicine components. Noni enzyme facial cleanser, millettia speciosa fruit enzyme facial cleanser, millettia speciosa enzyme facial cleanser are prepared respectively, and cleansing ability, moisturizing ability, foaming ability, bubble stability and the like of the millettia speciosa enzyme facial cleanser are detected respectively.
Experimental results show that the noni enzyme facial cleanser, the millettia speciosa champ fruit facial cleanser and the millettia speciosa champ have certain makeup removal and moisturizing activities; the size sequence of the cleansing and degreasing capabilities is as follows: noni ferment facial cleanser > oregano ferment facial cleanser and oregano ferment facial cleanser, and oregano ferment facial cleanser have no clear difference, wherein noni ferment facial cleanser has the best moisturizing effect. Therefore, the application of the millettia speciosa and noni enzymes in cosmetics has a certain development potential.
The noni enzyme facial cleanser, the millettia speciosa enzyme facial cleanser and the millettia speciosa fruit enzyme facial cleanser prepared by the experiment are in cream yellow paste, have light fragrance, are uniform and fine in texture, have no tight feel when being used, have good cleansing capability, heat resistance, cold resistance, stability and neutral pH, and accord with the execution standard data QB/T29680-2013 of the light industrial facial cleanser of the people's republic of China.
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Claims (6)
1. The ferment facial cleanser is characterized by comprising the following components in percentage by weight:
the ferment is selected from noni ferment; the ferment facial cleanser is prepared according to the following method: heating the phase A at the temperature of 85-95 ℃ according to the formula proportion, stirring for 40-60min, adding the phase B which is preheated and dissolved uniformly, stirring uniformly, stopping heating, adding the phase C which is prepared in advance, continuing stirring until the liquid level is bubble-free, adding the phase D which is prepared in advance under high-speed stirring when the temperature is reduced to 50 ℃, stirring uniformly, reducing the stirring speed, continuing stirring until the temperature is reduced to 45 ℃, adding the phase E which is prepared in advance, stirring continuously at the stirring speed until the temperature is lower than 37 ℃, discharging, obtaining the flowable paste after discharging, and standing the paste at room temperature for 1-2 days to form the enzyme facial cleanser.
2. The ferment facial cleanser of claim 1, characterized in that the phase B component which is preheated and dissolved uniformly is dissolved and mixed uniformly at a temperature of 85-95 ℃.
3. The ferment facial cleanser according to claim 1, characterized in that the high-speed stirring is selected from stirring speeds of preferably 400-600rpm, and the stirring speed is reduced, preferably adjusted to 100-200rpm.
4. The preparation method of the ferment facial cleanser of claim 1, which is characterized by comprising the following steps: heating the phase A at the temperature of 85-95 ℃ according to the formula proportion, stirring for 40-60min, adding the phase B which is preheated and dissolved uniformly, stirring uniformly, stopping heating, adding the phase C which is prepared in advance, continuing stirring until the liquid level is bubble-free, adding the phase D which is prepared in advance under high-speed stirring when the temperature is reduced to 50 ℃, stirring uniformly, reducing the stirring speed, continuing stirring until the temperature is reduced to 45 ℃, adding the phase E which is prepared in advance, stirring continuously at the stirring speed until the temperature is lower than 37 ℃, discharging, obtaining the flowable paste after discharging, and standing the paste at room temperature for 1-2 days to form the enzyme facial cleanser.
5. Use of the ferment facial cleanser according to any one of claims 1 to 3 for the preparation of degreasing and/or cleansing daily chemical products.
6. The use according to claim 5, wherein said degreasing and/or cleansing daily chemical product is preferably a hand cleanser, a facial cleanser or a cleansing water.
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| CN109364007A (en) * | 2018-12-04 | 2019-02-22 | 天津尚美化妆品有限公司 | Plant enzyme face cleaning condensation |
| CN109401869A (en) * | 2018-11-09 | 2019-03-01 | 广州宏度精细化工有限公司 | Liquid cleansing composition and its preparation method and application |
| CN109984960A (en) * | 2019-05-07 | 2019-07-09 | 海南师范大学 | A kind of beautiful essential oil facial cleanser of promise and preparation method thereof |
| KR102017132B1 (en) * | 2018-10-11 | 2019-09-03 | 임승호 | Cosmetic composition comprising a mixed fermentation extract of cinnamomum verum and angelica dahurica |
| CN111514072A (en) * | 2020-05-17 | 2020-08-11 | 海南师范大学 | Millettia speciosa-noni composite enzyme, preparation method thereof and application of millettia speciosa-noni composite enzyme in preparation of facial mask |
| CN112494342A (en) * | 2020-12-28 | 2021-03-16 | 广州天翼化妆品有限公司 | Liquid crystal amino acid facial cleanser and preparation method thereof |
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Patent Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| KR102017132B1 (en) * | 2018-10-11 | 2019-09-03 | 임승호 | Cosmetic composition comprising a mixed fermentation extract of cinnamomum verum and angelica dahurica |
| CN109401869A (en) * | 2018-11-09 | 2019-03-01 | 广州宏度精细化工有限公司 | Liquid cleansing composition and its preparation method and application |
| CN109364007A (en) * | 2018-12-04 | 2019-02-22 | 天津尚美化妆品有限公司 | Plant enzyme face cleaning condensation |
| CN109984960A (en) * | 2019-05-07 | 2019-07-09 | 海南师范大学 | A kind of beautiful essential oil facial cleanser of promise and preparation method thereof |
| CN111514072A (en) * | 2020-05-17 | 2020-08-11 | 海南师范大学 | Millettia speciosa-noni composite enzyme, preparation method thereof and application of millettia speciosa-noni composite enzyme in preparation of facial mask |
| CN112494342A (en) * | 2020-12-28 | 2021-03-16 | 广州天翼化妆品有限公司 | Liquid crystal amino acid facial cleanser and preparation method thereof |
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