CN115569091A - Millettia speciosa and noni enzyme facial cleanser - Google Patents
Millettia speciosa and noni enzyme facial cleanser Download PDFInfo
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- CN115569091A CN115569091A CN202110688906.7A CN202110688906A CN115569091A CN 115569091 A CN115569091 A CN 115569091A CN 202110688906 A CN202110688906 A CN 202110688906A CN 115569091 A CN115569091 A CN 115569091A
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- facial cleanser
- ferment
- beautiful millettia
- noni
- millettia root
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Images
Classifications
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9789—Magnoliopsida [dicotyledons]
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q1/00—Make-up preparations; Body powders; Preparations for removing make-up
- A61Q1/14—Preparations for removing make-up
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/10—Washing or bathing preparations
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/59—Mixtures
- A61K2800/592—Mixtures of compounds complementing their respective functions
- A61K2800/5922—At least two compounds being classified in the same subclass of A61K8/18
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/80—Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
- A61K2800/85—Products or compounds obtained by fermentation, e.g. yoghurt, beer, wine
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- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Veterinary Medicine (AREA)
- Public Health (AREA)
- General Health & Medical Sciences (AREA)
- Animal Behavior & Ethology (AREA)
- Botany (AREA)
- Birds (AREA)
- Epidemiology (AREA)
- Mycology (AREA)
- Microbiology (AREA)
- Biotechnology (AREA)
- Engineering & Computer Science (AREA)
- Dermatology (AREA)
- Cosmetics (AREA)
Abstract
The invention relates to beautiful millettia root noni enzyme facial cleanser. The noni enzyme facial cleanser, the beautiful millettia root fruit enzyme facial cleanser and the beautiful millettia root enzyme facial cleanser disclosed by the invention are cream yellow pastes, have light faint scent, are uniform and fine in texture, have no tightness to skin when being used, have good dirt-removing and makeup-removing capacity, heat resistance, cold resistance and stability, have neutral pH value, and meet QB/T29680-2013.
Description
Technical Field
The invention belongs to the field of daily chemicals, and particularly relates to beautiful millettia root noni ferment facial cleanser.
Background
Millettia speciosa (Millettia speciosa Champ), also known as Tilapia kok, radix Stephaniae Sinicae, radix seu caulis Arctii, radix Chimonanthi Praecocis, rhizoma Nelumbinis, radix Millettiae Speciosae, radix Ipomoeae, and radix Stephaniae Tetrandrae, belonging to the plant kingdom, the seed plant, and the dicotyledon, is the dried root of Millettia speciosa (L.) C.A. Merr. Of Millettia of Leguminosae) [1] . Beautiful millettia root is mainly developed and grown in roadside, valley, wilderness, open forest or bush, china has the main planting producing areas of Guangdong, guangxi, fujian, hunan, hainan, guizhou, yunnan and the like, and Guangdong province is mainly distributed in the west of GuangdongSouth and middle regions [2] . The main production place abroad is Vietnam.
The beautiful millettia root and the chemical components thereof are researched a lot at home and abroad, the beautiful millettia root is taken as a health food material in the Ming dynasty of China, and the medical history can be traced back to the records of ' Luchuan herbal medicine ' and ' raw herb medicine property reserve essences [3] . In the experiment of research progress of chemical components and pharmacological effects of beautiful millettia root, the beautiful millettia root is found to contain various chemical components such as various flavonoids, lignins, polysaccharides, triterpenes, alkaloid compounds and the like [3] . In addition, radix Millettiae Speciosae contains a large amount of organic acids, such as syringic acid, gentisic acid, maleic acid, echinocandic acid, linoleic acid, etc [4] . Grass of Fangcao, etc [5] In different places of production, the beautiful millettia root contains a large amount of protein, starch, amino acid, total dietary fiber, vitamin B2, saccharide and vitamin C. The research results of a plurality of pharmacological actions of beautiful millettia root show that the chemical components contained in the beautiful millettia root have obvious inoxidizability, anti-inflammation, anti-tumor property, fatigue resistance, anti-stress property, the function of enhancing immunoregulation, the efficacies of eliminating phlegm, relieving cough, relieving asthma and protecting liver and the like [6-9] . Chen Rongrong and the like [10] Experiments show that the water extract and the alcohol extract of the beautiful millettia root have certain lipid peroxidation resisting and free radical removing effects, the effect of the water extract of the beautiful millettia root is better than that of the alcohol extract, but the effects of the crude polysaccharide on resisting oxidation and removing free radicals are the weakest. Chen Xiaobai and the like [11] Pharmacological experiment results show that the beautiful millettia root has the effect of radiation resistance.
Noni (Morinda citrifolia Linn), also known as Noni, morinda citrifolia, rubiaceae. Mainly distributed in subtropical zone and tropical zone, such as Indonesia, australia, hawaii island, etc., and in the noni region of China, there are Xisha island, hainan island, etc [12] . The noni fruit contains abundant nutrients, including 5 essential nutrients, and abundant effective nutrients such as carbohydrate and mineralSubstances, vitamins, amino acids, proteins, trace elements, polysaccharide, phenols, methylcoumarin, beta-sitosterol, saponin, antioxidant, alizarin, flavonoids, anthraquinone, scopoletin bioactive substances, etc [13] 。
Noni has antibacterial activity, and research and experiment results show that certain phenolic substances contained in noni can inhibit the growth of certain specific microorganisms, such as shigella, salmonella, escherichia coli, helicobacter pylori, pseudomonas aeruginosa, bacillus subtilis, staphylococcus aureus and the like [13] 。
Noni has oxidation resistance, and related experimental researchers test and evaluate n-butanol extract of noni and extract monomer compounds from noni with oxidation resistance by five oxidation resistance experimental methods such as ABTS free radical clearance, hydroxyl free radical clearance, DPPH free radical clearance, copper ion reducing power, total reducing power and the like [14] 。
Noni has anti-inflammatory and analgesic effects, and the scholars find that noni extract can effectively solve the problems caused by inflammation and has certain anti-inflammatory effect in treating local severe inflammatory reaction caused by high inflammatory agents [15] . Zhang Weimin and the like [16] The experiment result shows that the extract of the root of the noni has obvious pain relieving and calming effects on the mice by acting the extract of the root of the noni on the mice, and meanwhile, the noni extracting solution is nontoxic and has no side effect.
The ferment is a food which is beneficial to human body and is prepared by fermenting available medicinal materials, fruits and vegetables with edible strains under certain conditions [17] . Proper intake of enzyme by human body can delay aging and prolong life of people [18] . Enzymes (enzymes) refer to various active substances and enzymes produced by enzyme bacteria during their activity, and are also collectively referred to as enzymes [19] . Because the natural enzyme bacteria produce the enzyme, the enzyme has no side effect, and is popular with people, especially women [20,21] . Different types of traditional Chinese medicinal materials have different efficacies, and researches show that some traditional Chinese medicinal materials can effectively promote cellsMetabolism of the skin and delaying aging of the skin [22] 。
In the cosmetic industry, facial cleanser is popular among people because of having the effects of moisturizing, decontaminating, removing oil and the like. However, as the economic level of China is gradually improved, the living standard of people is also continuously improved, and the requirements of people on beauty and skin care are higher and higher. People are continuously aware that certain potential safety hazards exist in the long-term use of facial cleanser containing chemicals. Therefore, more and more people will choose the facial cleanser containing the traditional Chinese medicine components. Compared with chemical cosmetics, the traditional Chinese medicine cosmetics have the characteristics of small side effect, high safety performance, natural non-toxicity, small side effect and the like [23] 。
Based on the above, the applicant previously applied patent applications (application numbers CN202110562491.9 and CN 202110556369.0) to prepare morinda citrifolia ferment, beautiful millettia root-fruit complex ferment, beautiful millettia root-noni complex ferment and related sunscreen products, and the present invention further discloses a facial cleanser containing the morinda citrifolia ferment, beautiful millettia root-fruit complex ferment and beautiful millettia root-noni complex ferment. And the in-vitro moisturizing activity, the water loss rate, the oil removal performance, the detergency, the makeup removing capability, the stability of the facial cleanser and other aspects of the facial cleanser are subjected to related determination, so that the beautiful millettia root compound enzyme has a good development prospect in the field of cosmetics.
Disclosure of Invention
The invention provides an enzyme facial cleanser, which is characterized by comprising the following components in parts by weight:
the ferment is selected from one or more of noni ferment, beautiful millettia root-fruit composite ferment and beautiful millettia root-noni composite ferment.
Another embodiment of the present invention provides the enzyme facial cleanser, which is prepared by the following steps: heating to 85-95 ℃ according to the proportion of the formula, preparing phase A, keeping the temperature, stirring for 40-60min, adding phase B which is preheated and dissolved uniformly, stirring uniformly, stopping heating, adding phase C which is prepared in advance, continuing stirring until no bubbles exist on the liquid level, cooling to 50 ℃, adding phase D which is prepared in advance, stirring uniformly, reducing the stirring speed, continuing stirring until the temperature is reduced to 45 ℃, adding phase E which is prepared in advance, continuing stirring until the stirring speed is unchanged until the temperature is lower than 37 ℃, discharging to obtain a flowable paste, and standing the paste at room temperature for 1-2 days to obtain the final product of the ferment facial cleanser.
The B phase which is preheated and dissolved uniformly can be selected from the B phase component to be dissolved and mixed uniformly under the temperature condition of the melting point temperature of the B phase component (preferably 85-95 ℃).
The high-speed stirring is selected from the stirring speed of 400-600rpm, and the stirring speed is reduced to 100-200rpm.
Another embodiment of the present invention provides a method for preparing the ferment facial cleanser, which comprises the following steps: heating to 85-95 ℃ according to a formula proportion, preparing phase A, keeping the temperature, stirring for 40-60min, adding phase B which is preheated and dissolved uniformly, stirring uniformly, stopping heating, adding phase C prepared in advance, continuing stirring until the liquid level has no bubbles, cooling to 50 ℃, adding phase D prepared in advance, stirring uniformly, reducing the stirring speed, continuing stirring until the temperature is reduced to 45 ℃, adding phase E prepared in advance, continuing stirring until the stirring speed is unchanged until the temperature is lower than 37 ℃, discharging to obtain a flowable paste, and standing the paste at room temperature for 1-2 days to obtain the enzyme facial cleanser.
The B phase which is preheated and dissolved uniformly can be selected from the B phase component to be dissolved and mixed uniformly under the temperature condition of the melting point temperature of the B phase component (preferably 85-95 ℃).
The high-speed stirring is selected from the stirring speed of 400-600rpm, and the stirring speed is reduced to 100-200rpm.
The invention further provides application of the ferment facial cleanser in preparation of daily chemical products for removing oil stains and or makeup.
Another embodiment of the present invention provides the use of noni ferment, beautiful millettia root-fruit complex ferment and beautiful millettia root-noni complex ferment in the preparation of daily chemical products for degreasing and/or makeup removal. The degreasing and/or makeup removing daily chemical product is preferably a hand sanitizer, a facial cleanser, makeup removing water and the like. The formula of the degreasing and/or makeup removing daily chemical product is as follows:
the preparation method comprises the following steps: heating to 85-95 ℃ according to the proportion of the formula, preparing phase A, keeping the temperature, stirring for 40-60min, adding phase B which is preheated and dissolved uniformly, stirring uniformly, stopping heating, adding phase C which is prepared in advance, continuing stirring until no bubbles exist on the liquid level, cooling to 50 ℃, adding phase D which is prepared in advance, stirring uniformly, reducing the stirring speed, continuing stirring until the temperature is reduced to 45 ℃, adding phase E which is prepared in advance, continuing stirring until the stirring speed is unchanged until the temperature is lower than 37 ℃, discharging to obtain a flowable paste, and standing the paste at room temperature for 1-2 days to obtain the final product of the ferment facial cleanser.
The B phase which is preheated and dissolved uniformly can be selected from the B phase component to be dissolved and mixed uniformly under the temperature condition of the melting point temperature of the B phase component (preferably 85-95 ℃).
The high-speed stirring is selected from the stirring speed of 400-600rpm, and the stirring speed is reduced to 100-200rpm.
The noni enzyme, the beautiful millettia root-fruit complex enzyme and the beautiful millettia root-noni complex enzyme are prepared by the methods of the previous Chinese patent application numbers CN202110562491.9 and CN202110556369.0 of the applicant (specifically, the methods of the preparation examples 1 to 5 in the example 1).
Drawings
Fig. 1 is a graph of in vitro moisture retention for each sample RH = 43%;
fig. 2 is a graph of relative humidity RH =84% in vitro moisturization rate for each sample;
fig. 3 is a graph of the water loss for each sample with relative humidity RH = 43%;
fig. 4 is a graph of relative humidity RH =84% water loss for each sample;
FIG. 5 is a graph of smear traces before the experiment;
fig. 6 is a graph of smear traces after the experiment.
Detailed Description
2.1 laboratory instruments, reagents and raw materials
2.1.1 instruments
TABLE 1 Instrument table
2.1.2 reagents
Hondu PCP 30 (potassium cocoyl-hydrolyzed avenin); hondu LT-40 (sodium lauroyl sulfonate); hondu LS-30 (sodium lauroyl amide); HC-10PLUS (disodium lauryl sulfosuccinate); the above reagents are available from Guangzhou Hongdu Fine chemical Co., ltd.
MP (methylparaben); SF-1 (acrylate copolymer emulsion); protectol PES (phenoxyethanol), which is prepared from Beino cosmetics, inc. of Guangzhou.
Glycerol (glycerin); myristic acid; dodecanoic acid; naCl; EDTA-2Na, and the above reagents are from physicochemical laboratories.
2.2 preparation of facial cleanser
100g of matrix facial cleanser samples were prepared
TABLE 2 formula of facial cleanser with base
The general preparation method comprises the following steps: heating to 85-95 ℃ according to a formula proportion, preparing phase A, keeping the temperature, stirring for 40-60min, adding phase B which is preheated and dissolved uniformly, stirring uniformly, stopping heating, adding phase C prepared in advance, continuing stirring until the liquid level has no bubbles, cooling to 50 ℃, adding phase D prepared in advance, stirring uniformly, reducing the stirring speed, continuing stirring until the temperature is reduced to 45 ℃, adding phase E prepared in advance, continuing stirring until the stirring speed is unchanged until the temperature is lower than 37 ℃, discharging to obtain a flowable paste, and standing the paste at room temperature for 1-2 days to obtain the enzyme facial cleanser. The B phase which is preheated and dissolved uniformly can be selected from the B phase component to be dissolved and uniformly mixed under the temperature condition that the melting point temperature of the B phase component is higher (preferably 85-95 ℃). The high-speed stirring is selected from the stirring speed of 400-600rpm, and the stirring speed is reduced to 100-200rpm.
The noni enzyme, the beautiful millettia root-fruit composite enzyme and the beautiful millettia root-noni composite enzyme which are prepared by the previous patent methods of the applicant are respectively taken to prepare the corresponding facial cleanser according to the general method, wherein the noni enzyme facial cleanser is called sample A for short, the beautiful millettia root enzyme facial cleanser is called sample B for short, the beautiful millettia root-fruit composite enzyme facial cleanser is called sample C for short, and the beautiful millettia root-noni composite enzyme facial cleanser is called sample D for short. The commercially available facial cleanser with mupeifei milk was designated as market facial cleanser 1, and the commercially available one-leaf facial cleanser was designated as market facial cleanser 2.
2.4 in vitro Wet keeping Performance measurement
Weighing 1.5g of self-made facial cleanser with different formulas, one leaf facial cleanser sold in the market and MEIREIFEIMIAN facial cleanser sold in the market at room temperature (24 deg.C), sticking medical air permeable adhesive tape (3M adhesive tape) on dry and clean glass slide to simulate skin tissue of human body, and uniformly smearing the facial cleanser on the treated glass slideThe tablets were placed in two dryers, one dryer having a relative humidity of RH =43% (saturated calcium chloride solution) and the other dryer having a relative humidity of RH =84% (saturated ammonium sulfate solution). Weighing the weighing bottles at 20,40, 60, 80, 100, 120, 140, 160 and 180min to obtain a facial cleanser with mass m before standing 0 (g) The quality of the facial cleanser after placement is m n (g) In that respect The moisture retention rate was calculated according to the formula (1).
Moisture retention rate = (m) n /m 0 )×100％ (1)
2.5 Water loss measurement
Two portions of each of 2g of homemade facial cleanser, commercial one-leaf facial cleanser and commercial meriliner milk facial cleanser of different formulations were weighed into weighing bottles at room temperature (24 ℃), and the weighing bottles were placed in two dryers, respectively, one dryer having a relative humidity of RH =43% (saturated calcium chloride solution) and the other dryer having a relative humidity of RH =84% (saturated ammonium sulfate solution). Measuring the change of the quality of the weighing bottle at 2,4, 6, 8, 10, 12, 24, 48, 72, 96 and 120h, and accurately measuring the quality m of the facial cleanser before placing 0 (g) The quality of the facial cleanser after placement is m n (g) In that respect And (3) calculating the water loss rate according to the formula (2).
Water loss rate = [ (m) 0 -m n )/m 0 ]×100％ (2)
2.6 measurement of oil-removing Properties
Determination of oil removal capacity: reference to the literature [24] The method is properly adjusted, 1g of facial cleanser sample is weighed, 10g of water is added to dissolve the facial cleanser sample into 10% diluted solution, vegetable oil is dripped into the diluted solution at 25 ℃ to dissolve the vegetable oil until the vegetable oil is not dissolved in the solution, and the weight of the consumed vegetable oil is weighed when the last drop just reaches a saturated state.
Oil removal capacity at different temperatures: weighing 1g of facial cleanser sample, adding 10g of water to dissolve and dilute the facial cleanser sample into 10% solution, respectively placing the solution containing 10% in 35 ℃,40 ℃,45 ℃ and 50 ℃ water bath pots to heat for 5min, dropwise adding vegetable oil into the diluted solution to dissolve the vegetable oil until the solution does not dissolve the vegetable oil, and weighing the last drop of the facial cleanser sample to be just the mass of the consumed vegetable oil in a saturated state.
2.7 measurement of Makeup removing ability
The medical adhesive tape is attached to a glass slide to imitate human skin, a rectangular area of 1 x 4cm is selected to be marked on the medical adhesive tape, and lipstick is uniformly coated in the rectangular area. And (3) coating 0.04g of sample on the medical adhesive tape coated with the lipstick, slightly kneading for 2min, then cleaning with tap water, and comparing the trace of the lipstick before and after cleaning. The comparative experiment was performed by applying an equal amount of makeup remover water (commercially available clean soft makeup remover water), and the blank experiment was performed by applying an equal amount of water.
2.8 measurement of surface tension
2.0g of facial cleanser is weighed in an environment at 25 ℃ and diluted into 40mL of 5% diluted solution, solutions of 1:9, 2:8, 3:7, 4:6, 5:5 and 6:4 are respectively marked as No. 1-6 according to the volume ratio of the sample to water, and the surface tensions of the samples with different concentrations are respectively measured.
Firstly, cleaning and drying the surface tension instrument container and the capillary, and checking whether the instrument is air-leaked. Distilled water is dropped into the surface tension meter and the level is adjusted to be tangent to the capillary [25]. Adjusting the air pumping speed to make the bubbles at the bubble capillary port uniformly emerge, recording the maximum pressure difference, continuously measuring for three times, and taking the average value.
The distilled water in the surface tension meter was taken out. Firstly, a surface tension meter is rinsed by using samples, the samples 1, 2, 3 and 4, the commercially available facial cleanser 1 and the commercially available facial cleanser 2 are respectively added, the maximum pressure difference is measured, the measurement is continuously carried out for three times, and the average value is obtained.
2.9 measurement of foamability and bubble stability
Dissolving 2g of facial cleanser in water to obtain 10% diluted solution, adding into 250mL measuring cylinder with piston, shaking the measuring cylinder with uniform force up and down for 10 times, and recording the height of the highest bubble. Then, the mixture is kept still for 10min, and the height of the bubbles after the mixture is kept still is compared. Three replicates were run and the average was determined.
2.10 detection of sensory index and physicochemical Standard
2.10.1 sensory index detection
2.0g of facial cleanser was weighed and placed on a clean and dry watch glass, and the appearance was observed for presence or absence of fragrance. Then 0.5g of facial cleanser is weighed and evenly smeared on the back of the hand to feel the fineness of the hand.
2.10.2 physicochemical Properties detection
Cold resistance test: weighing 2.0g of facial cleanser, placing in a dry weighing bottle, placing in a condition of-12 + -2 deg.C, standing for 24h, taking out, recovering to room temperature, and observing whether the sample has obvious difference with the sample before the experiment.
Heat resistance test: weighing 2.0g of facial cleanser, placing in a dry weighing bottle, placing in a condition of 42 +/-2 ℃, standing for 24h, taking out, recovering to room temperature, and observing whether the sample has obvious difference with the sample before the experiment during the period.
Centrifugal stability: weighing a certain amount of facial cleanser, centrifuging for 30min at 3500r/min, taking out, and observing whether the sample has layering phenomenon and whether water exists or not.
Measurement of pH: measuring by dilution method, accurately weighing 1.0g of facial cleanser, placing 10.0g of distilled water in a small beaker, continuously stirring the solution until the solution is uniform, measuring the pH value of the solution by using a pH meter respectively, measuring for three times, and taking an average value.
3 Experimental results and discussion
3.1 moisture retention rate
TABLE 3RH =43% in vitro moisture retention of each sample
In vitro moisture retention test was performed for 180min under RH =43%, and it can be found from table 3 and fig. 1: the moisture retention rate of each facial cleanser is kept above 90% after 180min, wherein the market facial cleanser used in the experiment has strong moisture retention capacity. In the self-made facial cleanser, the sample D, namely the noni ferment facial cleanser, has good moisturizing performance, and the moisturizing rate can reach 93.69% after 180 min. In the in vitro moisturizing experiment, the total trend of the moisturizing ability is as follows: the market sold facial cleanser 2, the market sold facial cleanser 1, the sample D, the sample A, the sample C and the sample B are named as the beautiful millettia root ferment facial cleanser, the beautiful millettia root fruit ferment facial cleanser and the beautiful millettia root ferment facial cleanser.
Table 4 rh =84% in vitro moisture retention rate of each sample
In vitro moisture retention test was performed for 180min under RH =84%, and it can be found from table 4 and fig. 2 that: after 180min, the moisture retention of the facial cleanser is kept above 94%, wherein the market facial cleanser used in the experiment has strong moisture absorption capacity; in the self-made facial cleanser, the sample D, namely the beautiful millettia root morinda citrifolia ferment facial cleanser has better moisture retention, and the moisture retention rate after 180min can reach 96.47%. In the in vitro moisturizing experiment, the total trend of the moisturizing ability is as follows: the market sold facial cleanser 2, the market sold facial cleanser 1, the sample D, the sample A, the sample C and the sample B are shown in the specification, namely the beautiful millettia root ferment facial cleanser, the beautiful millettia root fruit ferment facial cleanser and the beautiful millettia root ferment facial cleanser.
3.2 Water loss Rate
Table 5 rh =43% water loss rate of each sample
The water loss was measured for 120 hours in an environment of RH =43%, and it was found from table 5 and fig. 3 that: the water loss rate of the self-made facial cleanser after 120h is kept above 40%, wherein the water loss rates of the market facial cleansers used in the experiment are respectively 26.56% and 16.57%, and the self-made facial cleanser has weak water loss capacity. The highest water loss rate of the self-made facial cleanser after 120 hours can reach 45.85%. In the water loss test, the general trend of the water loss capacity of each facial cleanser is as follows: sample C, sample B, sample a, sample D, market-sold facial cleanser 1, market-sold facial cleanser 2, i.e., beautiful millettia root fruit ferment facial cleanser, beautiful millettia root ferment facial cleanser, noni ferment facial cleanser, beautiful millettia root ferment facial cleanser.
Table 6 rh =84% water loss rate of each sample
The water loss test measurement was performed for 120 hours in an environment with RH =84%, and it can be found from table 6 and fig. 4 that: the water loss rate of the self-made facial cleanser is kept above 10% after 120h, wherein the market facial cleanser used in the experiment has the characteristic of moisture absorption and has weaker water loss capacity. The water loss rate of the self-made facial cleanser after 120 hours can reach 20.64 percent at most. In the water loss test, the general trend of the water loss capacity of each facial cleanser is as follows: sample B, sample C, sample a, sample D, market-sold facial cleanser 1, market-sold facial cleanser 2, that is, beautiful millettia root ferment facial cleanser, noni ferment facial cleanser, beautiful millettia root ferment facial cleanser.
3.3 De-oiling Activity
3.3.1 evaluation of oil-removing ability
TABLE 7 quality of the dissolved oil for each sample
The experimental results show that the noni ferment facial cleanser, the beautiful millettia root fruit ferment facial cleanser and the beautiful millettia root ferment facial cleanser have certain oil removal capability. From table 7, it can be seen that the sample a, i.e., noni ferment facial cleanser, has the strongest oil removal capability at room temperature; the weakest oil removing ability is sample C, namely the beautiful millettia root fruit ferment facial cleanser; compared with the commercially available facial cleanser, the facial cleansers prepared by the four different enzymes have stronger oil removing capability than the facial cleansers prepared by the commercially available facial cleanser 2.
3.3.2 oil removal Capacity at different temperatures
TABLE 8 quality of dissolved oil for each sample
It can be seen from table 8 that the cleansing milk used in this experiment has different oil removing ability at different temperatures, and the quality of the cleansing milk dissolved oil increases when the temperature rises. The oil removal capacity at the same temperature is in the following order: sample a > sample D > sample B > sample C > market facial cleanser 1> market facial cleanser 2, i.e. noni ferment facial cleanser > beautiful millettia root ferment facial cleanser > market facial cleanser 1> market facial cleanser 2.
3.4 evaluation of cleansing ability
The blank comparison experiments show that the noni enzyme facial cleanser, the beautiful millettia root fruit enzyme facial cleanser and the beautiful millettia root enzyme facial cleanser have certain makeup removing capability through the blank comparison experiments shown in the figures 5 and 6, wherein the sample A, namely the noni enzyme facial cleanser and the sample D, namely the beautiful millettia root enzyme facial cleanser, has the makeup removing capability higher than that of the commercially available facial cleanser and the makeup removing capability higher than that of the commercially available clean soft makeup remover, and the sample C, namely the beautiful millettia root fruit enzyme and the sample B, namely the beautiful millettia root fruit enzyme facial cleanser have no obvious difference in the makeup removing capability. The 3M medical adhesive tape for simulating the human skin and slightly softening the cleansing water is found to have a large amount of rough edges in the cleansing capability test, and the four self-made facial cleansers have a small amount of rough edges or even no rough edges, and the experiment shows that the mildness of the self-made facial cleanser is stronger than that of clean and soft cleansing water.
3.5 surface tension
TABLE 9 surface tension of each sample
From Table 9, it can be found that the surface tension of each sample decreases as the concentration of the sample increases, and when the concentration reaches 60%, the surface tension of sample A (facial cleanser of noni ferment) is 2.167 × 10^ -2 (N/m); the surface tension at the same concentration is as follows: market facial cleanser 1, sample B, market facial cleanser 2, sample C, sample D and sample A, namely market facial cleanser 1, beautiful millettia root ferment facial cleanser, market facial cleanser 2, beautiful millettia root fruit ferment, beautiful millettia root ferment facial cleanser and beautiful millettia root ferment facial cleanser.
The effect of concentration on surface tension is large, the smaller the surface tension, the greater the wetting ability on objects and the greater the penetration of stains and thus the more soluble [25]. That is, the facial cleanser containing only noni ferment has the smallest surface tension, and the larger the surface tension, the poorer the wetting ability to stains, i.e., the poorer the detergency.
3.6 evaluation of foamability and foam stability
TABLE 10 foaming Properties and foam stability Properties of the samples
From table 10, it is known that four kinds of facial cleansers prepared by the laboratory have certain foaming ability, and both are stronger than two kinds of facial cleansers sold in the market used in the experiment. The foaming capacity is as follows: sample A, sample B, sample D, sample C, market facial cleanser 2, market facial cleanser 1, namely noni ferment facial cleanser, beautiful millettia root ferment facial cleanser, beautiful millettia fruit ferment facial cleanser, market already sold facial cleanser 2 and market already sold facial cleanser 2; in combination with tables 8 and 9, fig. 5 and 6 show that the cleansing cream has no necessary relationship between the cleansing cream degreasing and makeup removing abilities and the cleansing cream foaming ability.
The volume after recording the foam after 10min is found that the height of the four kinds of facial cleanser bubbles prepared by a laboratory is still higher than that of two kinds of facial cleansers sold in the market used in the experiment, wherein the foam height of the sample A, namely noni ferment facial cleanser is the highest, and the foam height of the sample B, namely beautiful cow ferment is the lowest; after 10min, the largest difference from the initial foam height is the market facial cleanser 2, and the smallest difference is the sample C, namely the beautiful millettia root fruit enzyme. The order of the change values is: market facial cleanser 2, sample B, sample A, market facial cleanser 1, sample D and sample C, namely market facial cleanser 2, beautiful millettia root ferment facial cleanser, noni ferment facial cleanser, market facial cleanser 1, beautiful millettia root ferment facial cleanser and beautiful millettia root fruit ferment facial cleanser.
3.7 sensory index evaluation
TABLE 11 sensory indices of the samples
The results in table 11 indicate that the four self-made facial cleansers are cream-yellow uniform cream bodies with light faint scent, while the two commercially available facial cleansers used in the experiment are milky uniform cream bodies, one has milk fragrance, and the other has faint scent; by using the six facial cleansers, the skin is not tight and is fine and smooth after the facial cleansers are used.
3.8 evaluation of physicochemical Properties
TABLE 12 stability Properties of the samples
The results in table 12 show that the beautiful millettia root ferment facial cleanser, the noni ferment facial cleanser and the beautiful millettia root ferment facial cleanser have better heat resistance and cold resistance. In addition, after the six kinds of facial cleanser were respectively centrifuged for 20min at a centrifugal machine of 3500r/min, no layering phenomenon was found in any of the six kinds of facial cleanser, and no water was separated out. By combining the above, analysis shows that four kinds of facial cleanser made by a laboratory have good stability.
Dilute solutions of a sample A, a sample B and a sample D, namely noni enzyme facial cleanser, beautiful millettia root enzyme facial cleanser and beautiful millettia root enzyme facial cleanser, are weakly acidic, dilute solutions of a sample C, namely beautiful millettia root fruit enzyme, are neutral, and dilute solutions of two commercially available facial cleansers used in the experiment are weakly alkaline; compared with the commercially available noodles, the noni enzyme facial cleanser, the beautiful millettia root enzyme facial cleanser and the beautiful millettia root enzyme facial cleanser are nearly neutral, are mild in use and are easy to maintain the skin.
4. Summary of the invention
The experimental study is an improvement on the basis of the traditional facial cleanser, and the enzyme containing the traditional Chinese medicine components is added. Respectively preparing noni ferment facial cleanser, beautiful millettia root fruit ferment facial cleanser and beautiful millettia root ferment facial cleanser, and respectively detecting the makeup removing capability, the moisturizing capability, the foaming capability, the bubble stability and the like.
The experimental results show that the noni enzyme facial cleanser, the beautiful millettia root fruit enzyme facial cleanser and the beautiful millettia root enzyme facial cleanser have certain makeup removing and oil removing capabilities and moisturizing activities; the makeup removing and oil removing capacity is as follows: the noni enzyme facial cleanser is prepared from the beautiful millettia root and noni enzyme, the beautiful millettia root and noni fruit enzyme facial cleanser and has no obvious difference from the beautiful millettia root and noni fruit enzyme facial cleanser, and the noni enzyme facial cleanser has the best moisturizing effect. Therefore, the application of beautiful millettia root and noni ferment in cosmetics has certain development potential.
The noni enzyme facial cleanser, the beautiful millettia root enzyme facial cleanser and the beautiful millettia root fruit enzyme facial cleanser prepared by the experiment are creamy yellow paste, have light faint scent, uniform and fine texture, have no tight feeling on skin when used, have good dirt-removing and makeup-removing capacity, heat resistance, cold resistance, stability and neutral pH value, and meet the QB/T29680-2013 of the light industrial facial cleanser execution standard of the people's republic of China.
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Claims (10)
1. The ferment facial cleanser is characterized by comprising the following formula:
2. the ferment facial cleanser according to claim 1, wherein the ferment is selected from one or more of morinda citrifolia ferment, millettia speciosa-fruit complex ferment and millettia speciosa-noni complex ferment.
3. The ferment facial cleanser according to any one of claims 1 to 2, characterized by being prepared according to the following method: heating to 85-95 ℃ according to the proportion of the formula, preparing phase A, keeping the temperature, stirring for 40-60min, adding phase B which is preheated and dissolved uniformly, stirring uniformly, stopping heating, adding phase C which is prepared in advance, continuing stirring until no bubbles exist on the liquid level, cooling to 50 ℃, adding phase D which is prepared in advance, stirring uniformly, reducing the stirring speed, continuing stirring until the temperature is reduced to 45 ℃, adding phase E which is prepared in advance, continuing stirring until the stirring speed is unchanged until the temperature is lower than 37 ℃, discharging to obtain a flowable paste, and standing the paste at room temperature for 1-2 days to obtain the final product of the ferment facial cleanser.
4. The ferment facial cleanser according to claim 3, wherein the preheated and uniformly dissolved B phase can be selected from B phase components which are uniformly dissolved at a temperature higher than the melting point (preferably 85-95 ℃).
5. The ferment facial cleanser according to any one of claims 3 to 4, characterized in that the high speed stirring is selected from stirring speeds of 400 to 600rpm, and the stirring speed is reduced preferably to 100 to 200rpm.
6. The method for preparing an enzymatic facial cleanser according to any one of claims 1 to 4, comprising the steps of any one of claims 1 to 4.
7. Use of the enzymatic facial cleanser according to any one of claims 1 to 4 for the preparation of degreasing and or makeup removing daily chemical products.
8. Application of noni ferment, beautiful millettia root-fruit composite ferment and beautiful millettia root-fruit composite ferment in preparing daily chemical products for degreasing and/or makeup removal.
9. Use according to claim 8, characterized in that the degreasing and/or makeup-removing commodity is preferably a hand sanitizer, a facial cleanser, a makeup remover or the like.
10. Use according to any one of claims 8 to 9, characterized in that the formulation of said degreasing and or makeup removing commodity is as follows:
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| CN109364007A (en) * | 2018-12-04 | 2019-02-22 | 天津尚美化妆品有限公司 | Plant enzyme face cleaning condensation |
| CN109401869A (en) * | 2018-11-09 | 2019-03-01 | 广州宏度精细化工有限公司 | Liquid cleansing composition and its preparation method and application |
| CN109984960A (en) * | 2019-05-07 | 2019-07-09 | 海南师范大学 | A kind of beautiful essential oil facial cleanser of promise and preparation method thereof |
| KR102017132B1 (en) * | 2018-10-11 | 2019-09-03 | 임승호 | Cosmetic composition comprising a mixed fermentation extract of cinnamomum verum and angelica dahurica |
| CN111514072A (en) * | 2020-05-17 | 2020-08-11 | 海南师范大学 | Millettia speciosa-noni composite enzyme, preparation method thereof and application of millettia speciosa-noni composite enzyme in preparation of facial mask |
| CN112494342A (en) * | 2020-12-28 | 2021-03-16 | 广州天翼化妆品有限公司 | Liquid crystal amino acid facial cleanser and preparation method thereof |
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Patent Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| KR102017132B1 (en) * | 2018-10-11 | 2019-09-03 | 임승호 | Cosmetic composition comprising a mixed fermentation extract of cinnamomum verum and angelica dahurica |
| CN109401869A (en) * | 2018-11-09 | 2019-03-01 | 广州宏度精细化工有限公司 | Liquid cleansing composition and its preparation method and application |
| CN109364007A (en) * | 2018-12-04 | 2019-02-22 | 天津尚美化妆品有限公司 | Plant enzyme face cleaning condensation |
| CN109984960A (en) * | 2019-05-07 | 2019-07-09 | 海南师范大学 | A kind of beautiful essential oil facial cleanser of promise and preparation method thereof |
| CN111514072A (en) * | 2020-05-17 | 2020-08-11 | 海南师范大学 | Millettia speciosa-noni composite enzyme, preparation method thereof and application of millettia speciosa-noni composite enzyme in preparation of facial mask |
| CN112494342A (en) * | 2020-12-28 | 2021-03-16 | 广州天翼化妆品有限公司 | Liquid crystal amino acid facial cleanser and preparation method thereof |
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