CN115397801A - 纯化(甲基)丙烯酸的方法 - Google Patents

纯化(甲基)丙烯酸的方法 Download PDF

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Publication number
CN115397801A
CN115397801A CN202180025573.8A CN202180025573A CN115397801A CN 115397801 A CN115397801 A CN 115397801A CN 202180025573 A CN202180025573 A CN 202180025573A CN 115397801 A CN115397801 A CN 115397801A
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CN
China
Prior art keywords
column
stream
acrylic acid
less
dehydration
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN202180025573.8A
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English (en)
Chinese (zh)
Inventor
S.特雷特贾克
A.胡韦
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Arkema France SA
Original Assignee
Arkema France SA
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Arkema France SA filed Critical Arkema France SA
Publication of CN115397801A publication Critical patent/CN115397801A/zh
Pending legal-status Critical Current

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    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C57/00—Unsaturated compounds having carboxyl groups bound to acyclic carbon atoms
    • C07C57/02—Unsaturated compounds having carboxyl groups bound to acyclic carbon atoms with only carbon-to-carbon double bonds as unsaturation
    • C07C57/03—Monocarboxylic acids
    • C07C57/04—Acrylic acid; Methacrylic acid
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D3/00—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
    • B01D3/14—Fractional distillation or use of a fractionation or rectification column
    • B01D3/143—Fractional distillation or use of a fractionation or rectification column by two or more of a fractionation, separation or rectification step
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D3/00—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
    • B01D3/34—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping with one or more auxiliary substances
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D3/00—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
    • B01D3/42—Regulation; Control
    • B01D3/4205—Reflux ratio control splitter
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/42—Separation; Purification; Stabilisation; Use of additives
    • C07C51/43—Separation; Purification; Stabilisation; Use of additives by change of the physical state, e.g. crystallisation
    • C07C51/44—Separation; Purification; Stabilisation; Use of additives by change of the physical state, e.g. crystallisation by distillation
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/42—Separation; Purification; Stabilisation; Use of additives
    • C07C51/43—Separation; Purification; Stabilisation; Use of additives by change of the physical state, e.g. crystallisation
    • C07C51/44—Separation; Purification; Stabilisation; Use of additives by change of the physical state, e.g. crystallisation by distillation
    • C07C51/46—Separation; Purification; Stabilisation; Use of additives by change of the physical state, e.g. crystallisation by distillation by azeotropic distillation

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
CN202180025573.8A 2020-04-06 2021-03-23 纯化(甲基)丙烯酸的方法 Pending CN115397801A (zh)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
FRFR2003402 2020-04-06
FR2003402A FR3108906B1 (fr) 2020-04-06 2020-04-06 Procede de purification d’acide (meth)acrylique
PCT/FR2021/050490 WO2021205090A1 (fr) 2020-04-06 2021-03-23 Procede de purification d'acide (meth)acrylique

Publications (1)

Publication Number Publication Date
CN115397801A true CN115397801A (zh) 2022-11-25

Family

ID=71094530

Family Applications (1)

Application Number Title Priority Date Filing Date
CN202180025573.8A Pending CN115397801A (zh) 2020-04-06 2021-03-23 纯化(甲基)丙烯酸的方法

Country Status (8)

Country Link
US (1) US12116339B2 (https=)
EP (1) EP4132898B8 (https=)
JP (1) JP2023520711A (https=)
KR (1) KR20220164564A (https=)
CN (1) CN115397801A (https=)
BR (1) BR112022018198A2 (https=)
FR (1) FR3108906B1 (https=)
WO (1) WO2021205090A1 (https=)

Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP1484309A1 (en) * 2003-06-05 2004-12-08 Nippon Shokubai Co.,Ltd. Method for production of acrylic acid
US20090253934A1 (en) * 2006-09-15 2009-10-08 Fungau Ho Process for Producing Acrylic Acid
CN106061934A (zh) * 2014-02-20 2016-10-26 阿科玛股份有限公司 用于生产丙烯酸的方法和系统
CN107428659A (zh) * 2015-03-12 2017-12-01 阿肯马法国公司 改进的(甲基)丙烯酸制备方法
CN108137469A (zh) * 2015-10-06 2018-06-08 阿肯马法国公司 改进的用于制备聚合物级的(甲基)丙烯酸的方法
CN110461811A (zh) * 2017-04-04 2019-11-15 阿科玛法国公司 包括具有分隔壁的蒸馏塔的纯化(甲基)丙烯酸的方法

Family Cites Families (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3725208A (en) 1971-08-20 1973-04-03 Nippon Kayaku Kk Process for purification of acrylic acid from aldehydes by distillation with a reagent
JPS6054939B2 (ja) * 1977-08-04 1985-12-03 住友化学工業株式会社 粗製アクリル酸の精製方法
TW305830B (https=) 1993-03-26 1997-05-21 Sulzer Chemtech Ag
JP3991873B2 (ja) * 2002-01-29 2007-10-17 三菱化学株式会社 （メタ）アクリル酸の製造方法
US7393976B2 (en) 2003-11-26 2008-07-01 Rohm And Haas Company Process for manufacturing reduced water content (meth)acrylic acid
FR2948365B1 (fr) 2009-07-22 2011-09-09 Arkema France Procede de fabrication d'acide acrylique bio-ressource a partir de glycerol
FR3094716B1 (fr) 2019-04-02 2021-06-04 Arkema France Production d’acide acrylique de grade polymere

Patent Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP1484309A1 (en) * 2003-06-05 2004-12-08 Nippon Shokubai Co.,Ltd. Method for production of acrylic acid
US20090253934A1 (en) * 2006-09-15 2009-10-08 Fungau Ho Process for Producing Acrylic Acid
CN106061934A (zh) * 2014-02-20 2016-10-26 阿科玛股份有限公司 用于生产丙烯酸的方法和系统
CN107428659A (zh) * 2015-03-12 2017-12-01 阿肯马法国公司 改进的(甲基)丙烯酸制备方法
CN108137469A (zh) * 2015-10-06 2018-06-08 阿肯马法国公司 改进的用于制备聚合物级的(甲基)丙烯酸的方法
CN110461811A (zh) * 2017-04-04 2019-11-15 阿科玛法国公司 包括具有分隔壁的蒸馏塔的纯化(甲基)丙烯酸的方法

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
大连理工大学编: "《化工原理 下》", 31 December 2002, 高等教育出版社, pages: 49 - 50 *

Also Published As

Publication number Publication date
FR3108906B1 (fr) 2022-03-04
US12116339B2 (en) 2024-10-15
EP4132898B1 (fr) 2025-04-23
KR20220164564A (ko) 2022-12-13
EP4132898A1 (fr) 2023-02-15
FR3108906A1 (fr) 2021-10-08
WO2021205090A1 (fr) 2021-10-14
BR112022018198A2 (pt) 2022-10-25
US20230109749A1 (en) 2023-04-13
EP4132898B8 (fr) 2025-10-22
JP2023520711A (ja) 2023-05-18

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